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41.
研究了淬火前不同冷变形量对LY12铝合金挤压小棒组织和性能的影响.结果表明:不同的冷拉拔量对LY12铝合金组织和性能有明显的影响;适当的冷变形量能减少或消除该合金挤压棒材的粗晶环.作者还对粗晶环的形成原因及其消除方法进行了讨论. 相似文献
42.
胡太忠 《中国科学技术大学学报》1993,23(4):375-381
研究了二维正态分布矩形区域概率质量当矩形区域中心沿某特定方向平移时的局部单调性。同时给出了一簇矩形区域,其中任一矩形区域的概率质量对正态分布相关系数的绝对值具有局部单调性。 相似文献
44.
The formation of the identical slope surface and the method of construction are discussed. On the basement of building the
parameter equation of variable-radius circle family envelope, the frequently used parameter equation of the identical slope
surface of the top of taper moving along column helix, horizental arc and line is built. The equation can be used to construct
the identical slope surface’s contours, gradient lines and three dimensional figures correctly.
Biography: Hu Jian-guo(1953-), male, Professor, research direction: CG and CAD. 相似文献
45.
Toshiki Kono Toshikazo Sakaguchi Yanming Hu Masashi Shiotsuki Fumio Sanda Toshio Masuda 《Journal of polymer science. Part A, Polymer chemistry》2006,44(20):5943-5953
Phenylacetylene (PA) derivatives having two polar groups (ester, 2a – d ; amide, 4) or one cyclic polar group (imide, 5a – c ) were polymerized using (nbd)Rh+[(η6‐C6H5)B?(C6H5)3] catalyst to afford high molecular weight polymers (~1 × 106 – 4 × 106). The hydrolysis of ester‐containing poly(PA), poly( 2a) , provided poly(3,4‐dicarboxyPA) [poly ( 3 )], which could not be obtained directly by the polymerization of the corresponding monomer. The solubility properties of the present polymers were different from those of poly(PA) having no polar group; that is, poly( 2a )–poly( 2d ) dissolved in ethyl acetate and poly( 4 ) dissolved in N,N‐dimethylformamide, while poly(PA) was insoluble in such solvents. Ester‐group‐containing polymers [poly( 2a )–poly( 2d )] afforded free‐standing membranes by casting from THF solutions. The membrane of poly( 2a ) showed high carbon dioxide permselectivity against nitrogen (PCO2/PN2 = 62). © 2006 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 44: 5943–5953, 2006 相似文献
46.
Mikaru Ikedo Masanobu Mori Kazumasa Kurachi Wenzhi Hu Kazuhiko Tanaka 《Analytical sciences》2006,22(1):117-121
The selective and simultaneous ion-exclusion chromatography (IEC) with UV-detection on a weakly acidic cation-exchange resin column in the H+ -form (TSKgel Super IC-A/C) was developed and applied for the simultaneous determination of phosphate and silicate ions as the water quality parameters required for optimizing the water-leaching process for ceramics glaze raw materials of natural origin including feldspar, woods-ash, and straw-ash. Phosphate and silicate ions in these water-leaching process water samples were separated selectively from the coexisting anions such as sulfate, chloride, nitrate and carbonate ions, based on the ion-exclusion separation mechanism. They were detected selectively and simultaneously by a postcolumn derivatization with molybdenum-yellow using the UV-detector. Under the optimized separation and detection conditions (eluent, 0-1 mM sulfuric acid; reactant, 10 mM sodium molybdate-25 mM sulfuric acid; detector, UV at 370 nm; temperature, 45 degrees C), the linearity of calibration was in the range 0.1 - 10 ppm for both phosphate and silicate ions, and the detection limits at S/N = 3 were 2.58 ppb for silicate ions and 4.75 ppb for phosphate ions. The effectiveness of this method was demonstrated in practical applications to the water-leaching process for some ceramics glaze raw materials. 相似文献
47.
Solid-phase extraction (SPE) procedure for cleanup followed by HPLC-UV method has been investigated for the determination of pyraflufen-ethyl residues in soil. The pesticide is extracted from the sample with acetone-water (80:20, v/v) and the extract is loaded onto an octadecyl (C(18)) column. The pesticide is eluted with acetonitrile and determined by HPLC with a UV detector. Using an acetone-water extraction followed by a C(18) cleanup, this method is characterized by recovery >90.1%, precision <5.8% RSD and sensitivity of 0.01 mg/kg. The proposed method has been successfully employed for the determination of the degradation dynamics of pyraflufen-ethyl in four agricultural soil samples under laboratory conditions. 相似文献
48.
Enantioselective catalytic trimethylsilylcyanations of aldehydes with 48% to 92% e.e. have been studied using the novel Ti-chiral Schiff base complexes. We have found that the catalyst led to high enantoselectivity when the molar ratio of the Schiff base 1 to Ti(O-i-Pr)4 was 2:1. 相似文献
49.
切削刀具倒棱刃口挤压力的理论计算 总被引:1,自引:0,他引:1
根据试验观察.揭出了刀具刃口带负倒棱时的切削模型。在此模型中,刀具刃口 存在一个“金属死区”。以新模型为基础.采用能量法,对高温、高应变率下刀具刃 口的挤压力进行了理论计算。所做工作的特点是:1)在材料变形分析中计入了挤压 层金属绕过刀具刃口时的过剩变形;2)进行有关材料变形与物理特性的计算时,考 虑了温度与应变率的影响。利用新研制的压电式切削测力仪进行验证试验,其结果表 明,理论计算值与实测数据较好一致。 相似文献
50.