流动注射原子吸收光谱法测定富硒天麻、葡萄及大米中的硒

建立了流动注射氢化物发生-原子吸收光谱法测定富硒天麻、葡萄及大米中硒的方法。测定硒的线性范围为0．33μg/L-50μg/L，相对标准偏差小于3％，加标回收率为93％-106％。方法已广泛应用于实际样品中微量硒的测定。     

STUDIES ON HYPERFINE STRUCTURE AND ISOTOPE SHIFT OF SOME EXCITED STATES IN Yb AND Tm ATOMS

The hyperfine structures and isotope shifts in some excited states of Yb and Tm have been measured using laser-atomic beam interaction, stepwise excitation and fluorescence detection techniques. From the experimental results, magnetic dipole hyperfine constants A and electric quadrupole hyperfine constants B have been derived. So for as we know, the A factor of [4f¹²5d6s6p]9/2 level in Tm is given for the first time.     

Electronic Structure and Magnetic Properties of SmCo7-xZrx

The electronic structure and magnetism of SmCo_7-xZr_x alloy are investigated using the spin-polarized MS-X. method. The results show that a few of electrons are transferred to the Sm(5d⁰) orbital due to orbital hybridization between Sm and Co atoms. The exchange interactions between 3d and 5d electrons are more important than the polarization effects of the conductive electrons, thus it is the main reason resulting in the long-range ferromagnetic order in SmCo_7-xZr_x. The Curie temperature of SmCo_7-xZr_x is generally lower than that of corresponding pure Co, which may be explained by the weaker average coupling strength between Co lattices due to some negative couplings mainly occurring of 2e site. The calculated results for the Sm₅Co₃₂Zr₂ cluster may lead to a better understanding of why SmCo_7-xZr_x is stable phase. Since the spin-up DOS peak of d electrons at E_F arises and the bonding of electrons at E_F strengthens with increasing Zr concentration, which results in the internal energy of the system decrease, the stable ferromagnetic order forms in SmCo_7-xZr_x.     

陆生植物黑麦草(Lolium multiflorum)对富营养化水体修复的围隔实验研究——氨氮的净化效应及其动态过程

采用浮床黑麦草（Lolium multi florum）对畜禽养殖富营养水体氨氮的净化效应及动态过程进行了研究．结果表明：浮床黑麦草对富营养水体中的氨氮具有明显的净化效果．当覆盖率30％时，对氨氮的去除率最高可达到95．89％．对其去除水体氨氮的动态过程拟合表明符合三次方程曲线．该研究为冬季陆生植物修复富营养水体提供重要依据．     

护环成型技术及质量控制的新进展

回顾了近年来在发电机护环各制造环节研究中所取得的主要成果,简要介绍了原材料冶炼、热成形制坯、强化性能三个关键工序攻关中取得的最新进展.针对当前生产中的难题和沿用工艺的缺点,开发的电渣熔铸坯料、包套冲挤(扩挤)热成形制坯新技术,能够解决热锻开裂、变形不均匀的难题,并可缩短工艺流程,提高产品质量与生产效益.研究的内增压或外增压液压胀形强化新方法,可以提高工艺过程的可控制性,并能扩大液压胀形的应用范围.     

Syntheses and Vasodilatory Activities of New Pyrazolo [ 4,3-d ] pyrimidin-7-ones

IntroductionAdenosine 3′,5′-cyclic monophosphate (cAMP)and guanosine 3′,5′-cyclic monophosphate(cGMP) areubiquitous second messengers that mediate biologicalresponses to a variety of extracellular cues, includinghormones, neurotransmitters, chemokines…     

自集成透镜InGaAsP／InPDHLED及其离子束铣技术

本文报道在国内首次采用离子束铣技术研制自集成透镜InGaAsP/InP DH LED的实验结果。采用烘烤正性光致抗蚀剂来形成球状掩膜适合于离子束铣,且重复性很好。为了获得光洁的刻蚀表面,刻蚀条件均已最优化。     

论微观辨证

探讨了在中、西医理论不同的前提下，如何合理选择应用现代检测项目作为辩证的指标，并提出微观辩证的新概念。     

合肥光源二分割三角型光位置检测器的研制

介绍了一种用于合肥光源的二分割三角型光位置检测器的研制,对其主要性能(如灵敏度和线性范围)进行了理论分析和实际测量,测量结果与理论分析相当吻合.文中还给出了光位置测量系统的组成     

基于3S技术的土地利用动态变化研究

3S技术是研究土地利用动态变化的重要技术手段，具有传统方法无法比拟的优越性。本文以秦皇岛市为例，定量分析了区域内土地利用动态变化。针对区域土地利用程度及生态环境可能产生的影响进行了简要的评价，揭示了研究区土地利用变化规律，为秦皇岛市实现生态环境目标提供决策依据。