Interfacial effects on stress distribution in model composites

Raman mechanical spectroscopy was used to examine interfacial effects on the stress distribution in model polydiacetylene fiber/epoxy composites. Epoxy release agents were coated on fiber surfaces to modify the interfacial adhesion properties. The modified fiber surfaces were then characterized by scanning electron microscopy and x-ray photoelectron spectroscopy as well as optical microscopy. No difference in the maximum stress value or stress distribution was observed for the two types of fibers, coated or uncoated, used in composites. This suggests that adhesion properties at the composite interface do not affect tensile stress transfer efficiency nor, therefore, the composite tensile modulus along the fiber axis direction in uniaxial composites. Experimental data were also compared with theoretical calculations assuming perfect bonding between fiber and matrix, and idealized frictional force transfer mechanism at the fiber–matrix interface.     

论我国商业秘密的立法完善

商业秘密是企业重要的无形资产,实践中商业秘密被侵害的纠纷也屡屡发生.着重探讨现阶段我国对商业秘密的保护在立法、司法等方面存在的缺陷,指出完善商业秘密的立法保护的重要性,并提出完善商业秘密立法的一些看法.     

基于Web的学生工作管理系统的JSP设计与实现

阐述了咸宁学院学生工作管理系统的主要功能,针对本院学生工作管理的特点,采用JSP网页技术进行开发.介绍了系统所有模块的数据项和数据结构,并对部分系统具体实现给出了代码说明.该系统运行结果表明,它提高了学生管理工作的工作效率和管理水平.     

粘合衬对服装舒适性影响的研究

探讨了粘合衬与粘合工艺对服装透气性、透湿性及透水性影响的规律。得出服装的舒适性虽由面料决定,但辅料(粘合衬)的影响也不可忽视。粘合衬的涂胶种类,粘合衬本身的透气性与透湿性,以及非织造粘合衬底布的单位重量,机织粘合衬底布的覆盖系数等,均对服装舒适性有影响,从而为衬料的选择,以及粘合工艺参数的设定,提供了依据。     

两个组合恒等式的概率证明

给出了两个组合恒等式的概率证明，扩展了已知的结果。     

含有纯滞后对象的控制方法

评述纯滞后对象控制的两种典型方法─—大林算法和纯滞后补偿法的原理、优缺点、设计要求及存在问题，并讨论了两者的联系。     

三角形速度场解析平面变形辊拔与辊挤

文章对平面变形辊拔与辊挤问题建立了运动许可的三角形速度场并获得上界解析解。该解与 Avitzur 以连续速度场得到的上界解进行比较表明,有时本文解法可得到更低的上界值。     

Dialdehyde starch‐crosslinked chitosan films and their antimicrobial effects

For improved mechanical and water‐swelling properties of chitosan films, a series of transparent films were prepared with dialdehyde starch as a crosslinking agent. Fourier transform infrared and X‐ray analysis results demonstrated that the formation of Schiff's base disturbed the crystallization of chitosan. The mechanical properties and water‐swelling properties of the films were significantly improved. The best values of the tensile strength and breaking elongation were 113.1 MPa and 27.0%, respectively, when the dialdehyde starch content was 5%. All the crosslinked films still retained obvious antimicrobial effects toward S. aureus and E. coli, and they showed potential for biomedical applications. © 2003 Wiley Periodicals, Inc. J Polym Sci Part B: Polym Phys 41: 993–997, 2003     

Crystallographic report: Bis[bis(N,N‐dibenzyldithiocarbamato)cadmium(II)]

The centrosymmetric structure of {Cd[S₂CN(CH₂Ph)₂]₂}₂ features both bridging and chelating dithiocarbamate ligands so that a square pyramidal S₅ coordination geometry results. Copyright © 2004 John Wiley & Sons, Ltd.     

Flow-injection spectrophotometric determination of sulfadiazine and sulfamethoxazole in pharmaceuticals and urine.

A rapid and sensitive flow-injection spectrophotometric method is proposed for the determination of sulfadiazine and sulfamethoxazole. This method is based on the diazotization of sulfonamide with sodium nitrite, and a coupling reaction of the diazo-compound with alpha-naphthylamine. The optimum experimental conditions are obtained by using the controlled and weighted centroid simplex method. The linear ranges for the determination of sulfadiazine and sulfamethoxazole are 0.2-20 microg ml(-1) and 0.1-20 microg ml(-1), and their detection limits are 0.06 microg ml(-1) and 0.05 microg ml(-1), respectively, and the sampling frequency is 130 samples per hour. The method has been used to determine sulfadiazine and sulfamethoxazole in pharmaceuticals and urine without separation. The results are in agreement with those obtained by a high-performance liquid chromatograph technique at the 95% confidence level.