全文获取类型
收费全文 | 11841篇 |
免费 | 1417篇 |
国内免费 | 838篇 |
专业分类
化学 | 5803篇 |
晶体学 | 87篇 |
力学 | 509篇 |
综合类 | 44篇 |
数学 | 998篇 |
物理学 | 3187篇 |
综合类 | 3468篇 |
出版年
2024年 | 40篇 |
2023年 | 197篇 |
2022年 | 339篇 |
2021年 | 385篇 |
2020年 | 407篇 |
2019年 | 323篇 |
2018年 | 289篇 |
2017年 | 288篇 |
2016年 | 466篇 |
2015年 | 513篇 |
2014年 | 582篇 |
2013年 | 707篇 |
2012年 | 891篇 |
2011年 | 862篇 |
2010年 | 651篇 |
2009年 | 622篇 |
2008年 | 711篇 |
2007年 | 545篇 |
2006年 | 557篇 |
2005年 | 461篇 |
2004年 | 344篇 |
2003年 | 300篇 |
2002年 | 258篇 |
2001年 | 227篇 |
2000年 | 241篇 |
1999年 | 353篇 |
1998年 | 319篇 |
1997年 | 280篇 |
1996年 | 275篇 |
1995年 | 254篇 |
1994年 | 243篇 |
1993年 | 176篇 |
1992年 | 179篇 |
1991年 | 160篇 |
1990年 | 125篇 |
1989年 | 107篇 |
1988年 | 95篇 |
1987年 | 75篇 |
1986年 | 51篇 |
1985年 | 30篇 |
1984年 | 22篇 |
1983年 | 20篇 |
1982年 | 9篇 |
1981年 | 14篇 |
1980年 | 9篇 |
1977年 | 6篇 |
1976年 | 10篇 |
1975年 | 9篇 |
1973年 | 8篇 |
1972年 | 6篇 |
排序方式: 共有10000条查询结果,搜索用时 8 毫秒
11.
12.
Least-squares finite difference (LSFD) method, one of mesh-free methods, is used to solve slider air bearings problem through discritizing the generalized Reynolds equation into nonlinear systems of algebraic equations. Two approximation schemes for the linearization of these equations are presented and compared. And, some new techniques to search supporting points for the reference node in the mesh-free method were proposed and explored. Therefore, these improvements eliminate some potential limitation of the LSFD method previously published and further facilitate its employment in complex slider models. Advanced step slider as an example of negative pressure sliders is simulated and verified using the improved LSFD mesh-free method in head disk systems. 相似文献
13.
Peng Xu Haitao Wang Rui Lv Qiangguo Du Wei Zhong Yuliang Yang 《Journal of polymer science. Part A, Polymer chemistry》2006,44(12):3911-3920
A novel microphase‐inversion method was proposed for the preparation of TiO2–SiO2/poly(methyl methacrylate) core–shell nanocomposite particles. The inorganic–polymer nanocomposites were first synthesized via a free‐radical copolymerization in a tetrahydrofuran solution, and the poor solvent was added slowly to induce the microphase separation of the nanocomposite and result in the formation of nanoparticles. The average particle sizes of the microspheres ranged from 70 to 1000 nm, depending on the reaction conditions. Transmission electron microscopy and scanning electron microscopy indicated a core–shell morphology for the obtained microspheres. Thermogravimetric analysis and X‐ray photoelectron spectroscopy measurements confirmed that the surface of the nanocomposite microspheres was polymer‐rich, and this was consistent with the core–shell morphology. The influence of the synthetic conditions, such as the inorganic composition and the content of the crosslinking monomer, on the particle properties was studied in detail. © 2006 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 44: 3911–3920, 2006 相似文献
14.
A simple and sensitive method was conducted for the determination of trace amounts of proteins with benzeneazo-8-acetylamino-1-naphthol-3,6-disulfonic acid sodium salt (azophloxine, AP) using a Rayleigh light-scattering (RLS) technique. At pH 2.60 and in the presence of an emulsifier OP microemulsion, the RLS of AP can be greatly enhanced by proteins, owing to the interaction between AP and protein. The enhanced intensity is proportional to the concentration of proteins. Four proteins, including bovine serum albumin (BSA), human serum albumin (HSA), lysozyme (Lys) and gamma globulin (gamma-G) have been tested. For example, the linear range of BSA was 0 - 0.06 microg mL(-1) with detection limits of 2.38 ng mL(-1). The method was applied to the analysis of protein in human urine and penicillin samples with satisfactory results. The relative standard deviation was in all instances less than 4.0%, and the recovery was in the range of 97.5 - 104%. 相似文献
15.
介绍了针对油藏流体及其注气体系的相态及物性的预测而开发的DGPVT软件包功能、模型及特点。基于实验数据对DGPVT软件包的预测准确性进行了检验,并与石油界知名的商用油气相态及物性计算软件包STATPACK进行了比较。 相似文献
16.
面向对象的二叉树装配模型研究 总被引:1,自引:1,他引:0
文章研究可装配性设计中的产品装配建模,提出一种以装配体为对象并能充分反映装配过程特点的二叉树装配模型。应用面向对象技术,建立了相应的数据结构及应用框架,为可装配性评价奠定了基础,也可做为通用的产品装配模型应用于CAPP等领域。 相似文献
17.
18.
解决我国城市生活垃圾问题的出路 总被引:2,自引:0,他引:2
杜学成 《佛山科学技术学院学报(自然科学版)》1998,16(3):69-75
对目前国内垃圾主要处理方法进行了评价,认为要从根本上解决我国城市生活垃圾问题必须建立健全垃圾减量与处理的双重机制。提出了“清洁生活”的概念,指出了城市生活垃圾的减量要建立在“清洁生活”战略指导思想的基础上;建立城市生活垃圾多级、低熵分选处理体系是符合我国国情的有效处理垃圾的最佳选择。 相似文献
19.
Dušan J. Radanović Zoran D. Matović Gustavo Ponticelli Paola Scano Inessa A. Efimenko 《Transition Metal Chemistry》1994,19(6):646-650
Summary The synthesis and characterization of AuIII complexes with several heterocyclic ligands are reported. The compounds have general formula [AuX3(L)], where L =N-methylimidazole (N-MeIz),N-ethylimidazole (N-EtIz),N-propylimidazole (N-PrIz), benzoxazole (BO), 2-methylbenzoxazole (2-MeBO), 2,5-dimethylbenzoxazole (2,5-diMeBO), 2-amino-pyrimidine (2-APm), 4(6) -hydroxy-pyrimidine [4(6)-hydrPm] or hypoxanthine (Hypox) and X = Cl or Br. Elemental analysis, conductivity measurements and spectral studies were used for the characterization of the complexes. A square-planar geometry withN-bonded heterocyclic ligands is suggested. 相似文献
20.
The complexes of the rare earth metals with 2-phenyltrifluoroacetone in the presence of TX-100 are reported. The characteristic absorbances of neodymium, holmium and erbium complexes can be increased by factors of 8.5, 31 and 15 respectively, compared to those of the cholrides. The third-derivative spectra have been used to eliminate the interference of cerium, and the sensitivities are increased again by factors of 7.4, 5.5 and 6.5. A method for the direct determination of neodymium, erbium and holmium in rare earth mixtures is proposed. 相似文献