Stability control of the electrooptic effect with new maleimide copolymers containing photoreactive tricyanopyrrolidene‐based chromophores

New photocrosslinkable maleimide copolymers have been synthesized by the attachment of a tricyanopyrrolidene‐based chromophore. The 2‐(3‐cyano‐4‐(2‐{4‐[hexyl‐(6‐hydroxy‐hexyl)‐amino]‐phenyl}‐vinyl)‐5‐oxo‐1‐{4‐[4‐(3‐oxo‐3‐phenyl‐propenyl)‐ phenoxy]‐butyl}‐1,5‐dihydro‐pyrrol‐2‐ylidene)‐malononitrile chromophore exhibits nonlinear optical activity and contains a chalcone moiety that is sensitive to UV light (λ = 330–360 nm) for crosslink formation. The maleimide monomers have also been functionalized with chalcone moieties. The resultant copolymers exhibit great processability, and one of them shows a maximum electrooptic coefficient of 90 pm/V at 1300 nm. We could control the thermal stability of the electrooptic coefficient with the newly synthesized photoreactive copolymers successfully. © 2006 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 45: 531–542, 2007     

A study of ion exchange selectivity coefficient by cyclic voltammetric measurement

An equation to express ion exchange selectivity coefficient was derived and used for calculating that of PPY film with the results obtained by cyclic voltammetric measurement. PPY film was synthesized by electrochemical method in aqueous solution using K₄Fe(CN)₆ as supporting electrolyte, and the anions were doped into the film. Ion exchange behaviour of doped Fe (CN)₆^3-/4- in the PPY film with Cl^?, NO₃^? or F^? ions in solution has been studied, and the corresponding ion exchange selectivity coefficients were determined.     

Mbius群的离散性(英文)

利用一个固定的抛物型M bius变换作为检验性元素来检验扩充复平面上的非初等M bius群的离散性 ,文中给出的结果改进了由Jrgensen所建立的判别准则     

Riding on Tyvek-A Case Study about How a New Material Invented by Western Multinational Company Enters China

This paper is a case study about how a new product developed by Western multinational company enters new market ?the Mainland China. In this study, a new fabric ?DuPont's hi-technical Tyvek?PU Coating, is fashionized and developed into a new fashionable and functional casual-rainwear, using the approach of new product development method ( idea generation; screening; business analysis; development; evaluation and testing; commercialization).     

Validation of a method for predicting the precision, limit of detection and range of quantitation in competitive ELISA.

The mathematical model for predicting the precision, limit of detection (LOD) and range of quantitation (ROQ) in a competitive enzyme-linked immunosorbent assay (ELISA) proposed by Hayashi et al. (Anal. Chem., 2004, 76, 1295) was validated. The model describes the relative standard deviation (RSD) of concentration estimates by the RSDs of pipetting volumes of analyte, enzyme-conjugated antigen, antibody and substrate solutions, and the standard deviation (SD) of inherent absorbances between the wells in an ELISA plate. For 6 kinds of direct competitive ELISA kits, the LOD and ROQ predicted by the model agreed well with those obtained by experiments with real samples. It was also confirmed that the model is applicable to the prediction of uncertainty that depends on the pipetting error of the viscous antiserum solution. The model was demonstrated to be useful for estimating the LOD and ROQ of competitive ELISA.     

PET-云母复合体系的双重Tg转变

本文用粘弹谱仪、x射线衍射、DSC研究了PET—云母复合物的Tg区域的多重转变等松驰转变行为,探讨了加工、云母填充对PET—云母材料性能影响的分子运动机理。不同热历史(如不同成型条件、热处理等)使聚合物分子形成不同链段运动;处于高温位的Tg(u)其运动单元是受结晶、内应力、填料作用影响的非晶区链段。     

高低杠“屈体腾越转体180°再握”动作的运动学分析

本文采用固定高速摄影及影片数字化研究方法，对山西体操运动员郭佳在１９９０年新创的屈体腾越转体１８０°再握动作进行运动学分析，得出各技术环节的运动学数据，找到其动作的运动学特征，为我国体操教练员和运动员提供参考。     

曲棍球赛场技战术的计算机分析系统

介绍在ＩＢＭ－ＰＣ／ＸＴ计算机上实现的曲棍球赛场统计系统的研制过程、设计思想、采用的方法、软件设计与功能、技术指标操作步骤以及使用效果。     

档案行政执法要采取监督与业务指导相结合

依法治档，很大程度是通过档案行政执法来实现的。档案行政执法是档案法制建设不可缺少的重要环节。也是依法治档的关键因素和重大举措。要使档案法律、法规落到实处。关键在于从严监督。文章探讨了如何把监督和业务指导有机结合起来，更好地为档案事业服务。     

砂质泥岩工程地质特性及其灾害防治对策

文章阐述了砂质泥岩的工程地质特性及其风化规律，在不同状态下形成的灾害，提出了防治对策。