A Novel Polymethyl Methacrylate （PMMA）TiO2 Nanocomposite and Its Thermal and Photic Stability

A new kind of polymethyl methacrylate （PMMA）-TiO2 nanocomposite was synthesized through polymerization. The thermal and photic stability of this PMMA TiO2 nanocomposites were investigated. The as prepared samples were characterized by scanning electron microscopy （SEM）, UV-Vis spectroscopy, differential thermal analysis （DTA） and the photo-induced weight loss, The results show that the photostability of the PMMA-TiO2 nanocomposite is higher than that of the pure PMMA under UV-light irradiation, The weight loss of the pure PMMA reaches 30 % after 300 h UVirradiation, while the composite only 0.3% under the identical experimental condition. The glass transition temperature （TR） of pure PMMA is only 80℃, while the Tg of the composite reaches 258℃. Compared with pure PMMA, the thermal stability of the composite is greatly enhanced.     

The influence of hard‐segments on two‐phase structure and shape memory properties of PCL‐based segmented polyurethanes

Poly(ε‐caprolactone)‐based segmented polyurethanes (PCLUs) were prepared from poly(ε‐caprolactone) diol, diisocyanates (DI), and 1,4‐butanediol. The DIs used were 4,4′‐diphenylmethane diisocyanate (MDI), 2,4‐toluenediisocyanate (TDI), isophorone diisocyanate (IPDI), and hexamethylene diisocyanate (HDI). Differential scanning calorimetry, small‐angle X‐ray scattering, and dynamic mechanical analysis were employed to characterize the two‐phase structures of all PCLUs. It was found that HDI‐ and MDI‐based PCLUs had higher degree of microphase separation than did IPDI‐ and TDI‐based PCLUs, which was primarily due to the crystallization of HDI‐ and MDI‐based hard‐segments. As a result, the HDI‐based PCLU exhibited the highest recovery force up to 6 MPa and slowest stress relaxation with increasing temperature. Besides, it was found that the partial damage in hard‐segment domains during the sample deformation was responsible for the incomplete shape‐recovery of PCLUs after the first deformation, but the damage did not develop during the subsequent deformation. © 2007 Wiley Periodicals, Inc. J Polym Sci Part B: Polym Phys 45: 557–570, 2007     

关于W_2~1[a,b]能否扩大的一些问题

讨论了W12[a,b]能否扩大为含有有间断点函数的再生核空间的问题.结论是:若再生核空间W W12[a,b]含有有间断点的函数,则间断点必固定、间断点个数必有限且非端点a,b.进一步,我们构造了函数含有n个间断点的再生核空间并给出其再生核表达式.     

非球面最适球面的确定方法——三点法

根据非球面生产的实际情况．指出非球面最适球面的确定方法．详细分析最适球面的计算方法．并对一抛物面进行了实例计算，通过与最小二乘法的计算结果比较．指出该方法具有计算简单、与加工工艺过程相符合等特点。     

CreditRisk+模型下商业银行经济资本配置研究

对金融资产风险的度量与经济资本的分配应该体现分散化效应,传统的V aR方式不能保证分散化效应的次可加性.本文讨论了基于T a ilV aR这一新的风险度量与经济资本分配标准,并在违约率均值不变情况下,对C red itR isk+模型下的商业银行经济资本分配进行了实证分析.     

南宋新喻籍高僧德光禅师生平

德光不仅是一位佛教思想家和实践家,同时又是一位教育家。他是历代新喻籍僧人中最出色的一位。他天姿聪颖,少壮出家,参悟佛法,观机逗教,为临济宗的发展做出了自己的贡献。他法嗣遍布海内,甚至远播东瀛。他名满当时,广结善缘,与皇帝文臣有着广泛的交往,并留下了一些佳话。     

浅谈幼儿基本体操对幼儿发育的促进作用

幼儿基本体操是以幼儿为对象,以增强体质为目的的大众健身体操。从幼儿基本体操的概念上、幼儿生理上、心理上、智力发展方面介绍和论述幼儿基本体操对幼儿发育的促进作用。     

学年学分制模式下的高校学生工作探索

我国目前大多数高校采用学年学分制,与学年制和完全学分制不同,它以学分为计量单位,按学年或学期作为结算时段确定学生的降级和退学标准,有相对固定的修业年限。文章对该模式下的学生工作进行初步探讨,提出了进一步完善辅导员制度、加强班集体建设等系列措施。     

Robust H∞ control for linear Markovian jump systems with unknown nonlinearities

This paper studies the problem of stochastic stability and disturbance attenuation for a class of linear continuous-time uncertain systems with Markovian jumping parameters. The uncertainties are assumed to be nonlinear and state, control and external disturbance dependent. A sufficient condition is provided to solve the above problem. An H_∞ controller is designed such that the resulting closed-loop system is stochastically stable and has a disturbance attenuation γ for all admissible uncertainties. It is shown that the control law is in terms of the solutions of a set of coupled Riccati inequalities. A numerical example is included to demonstrate the potential of the proposed technique.     

等截面垂直管道中气粉流的临界管长

考虑重力和摩擦力的影响，建立了描述垂直管道中气粉流行为的数学模型，采用马赫数检验法，确定了产生摩擦壅塞时的临界管长，计算表明，当气粉流以不同方式喷入相同的冶金熔池时，底吹垂直管道比顶吹垂直管道需要更大的临界管长。