温度和流速对齐口裂腹鱼幼鱼呼吸代谢的影响

通过流水式呼吸仪研究了齐口裂腹鱼(Schizothorax prenanti)幼鱼在不同水温(11,15,20,23℃)和流速(0.00,0.10,0.30,0.50m/s)环境下的呼吸代谢.研究发现,齐口裂腹鱼幼鱼呼吸代谢率(MR)和单位体重呼吸代谢率(MR′)都随着温度的升高而增大.在11～23℃之间,代谢率的变幅为0.85～7.21mg/h,单位体重代谢率的变幅为350.81～1858.16mg/(kg·h).回归方程MR=a.mb能够较好的描述4个温度水平的幼鱼代谢率与体重之间的关系(p<0.05),体重指数b随着温度的升高而降低.并且在11～23℃之间,幼鱼的代谢率与温度、体重间的关系可通过模型MR=0.525m0.788.e0.033T(R2=0.907,p<0.05,n=32)较好地表征.在0.00,0.10,0.30,0.50m/s4个流速下裂腹鱼幼鱼呼吸代谢率的波动范围为0.59～2.35mg/h,单位体重代谢率波动范围为469.93～1281.56mg/(kg.h).各流速平均代谢率的大小顺序为0.937mg/h(0.10m/s)<1.089mg/h(0.00m/s)<1.104mg/h(...     

Gold and Carbene Relay Catalytic Enantioselective Cycloisomerization/Cyclization Reactions of Ynamides and Enals

The combined use of gold as transition metal catalyst and N‐heterocyclic carbene (NHC) as organic catalyst in the same solution for relay catalytic reactions was disclosed. The ynamide substrate was activated by gold catalyst to form unsaturated ketimine intermediate that subsequently reacted with the enals (via azolium enolate intermediate generated with NHC) effectively to form bicyclic lactam products with excellent diastereo‐ and enantio‐selectivities. The gold and NHC coordination and dissociation can be dynamic and tunable events, and thus allow the co‐existence of both active metal and carbene organic catalysts in appreciable concentrations, for the dual catalytic reaction to proceed.     

J/psi production versus centrality, transverse momentum, and rapidity in Au+Au collisions at square root sNN=200 GeV

The PHENIX experiment at the BNL Relativistic Heavy Ion Collider (RHIC) has measured J/psi production for rapidities -2.2相似文献   

实现操作人员控制策略的模糊神经网络方法

通过一个仿真实例的研究。阐述了实现操作人员控制策略的模糊糊神经网络方法，并讨论了模糊神经网络控制器的鲁棒性问题，仿真结果证实了该实现了方法的有效性。     

氢化物原子荧光法测定化妆品中的汞

采用微波消解技术对化妆品样品进行消解,用氢化物原子荧光法测定样品中的汞.改变仪器条件及溶液浓度进行试验,确定最佳试验参数.汞浓度在0～20μg/L范围内与原子荧光强度呈良好的线性关系,相关系数为0.9997,方法检出限为0.0005μg/L.对眼影和润肤露样品进行加标回收试验,回收率为95%～100%.与浸提法相比,微波消解法提取出的汞完全且损失少.     

关于混合型多项式Hammerstein积分方程正解迭代求法

本文给出了混合型多项式Ｈａｍｍｅｒｓｔｅｉｎ积分方程正解的迭代求法，并将所得结果应用到二阶非线性常微分方程的边值问题     

掺Yb3+双包层大模场面积光纤锁模激光器

报道了一种结构简单、运转稳定并可以输出高脉冲能量的被动锁模光纤激光器.激光器的增益介质为掺Yb³⁺双包层大模场面积光纤,具有非常低的非线性系数.利用非线性偏振旋转效应和半导体可饱和吸收镜结合实现自启动锁模,获得了平均功率为160mW、重复频率为55.9MHz(对应于3nJ的单脉冲能量)、脉冲宽度为10.6ps的激光脉冲输出. 关键词： 大模场面积光纤 光纤激光器 锁模     

高效液相色谱-电感耦合等离子体质谱联用测定生物样品中无机汞和甲基汞

建立了高效液相色谱(HPLC)和电感耦合等离子体质谱(ICP-MS)联用测定多种生物样品中的无机汞和甲基汞的方法,并对比了提取生物样品中无机汞和甲基汞的不同前处理方法。实验使用5 mol/L的盐酸超声波提取样品中的无机汞和甲基汞。高效液相色谱流动相为含有0.06 mol/L醋酸氨,20μg/L B i,0.1%(V/V)2-巯基乙醇的5%(V/V)甲醇-水溶液,色谱柱为C18反相柱(5μm,3.9 mm×150 mm)。提取液在液相色谱中分离后,进入电感耦合等离子体质谱检测其中无机汞和甲基汞的浓度。测定了人发(GBW 07601),对虾(GBW 08572),鱼肉组织(IAEA MA-B-3/TM)和牛肝(GBW 080193)4种生物标准参考物,结果与标准参考物的标准值相符。无机汞和甲基汞检出限分别为0.3和0.2μg/L。     

Lyotropic liquid crystalline phases formed in an ionic liquid

Lyotropic liquid crystalline phases of an amphiphilic block copolymer are constructed and characterized in an ionic liquid with comparison of component and temperature effects.     

Application of an efficient strategy based on MAE,HPLC‐DAD‐MS/MS and HSCCC for the rapid extraction,identification, separation and purification of flavonoids from Fructus Aurantii Immaturus

This study presents an efficient strategy based on microwave‐assisted extraction (MAE), HPLC‐DAD‐MS/MS and high‐speed counter‐current chromatography (HSCCC) for the rapid extraction, identification, separation and purification of active components from the traditional Chinese medicine Fructus Aurantii Immaturus. An LC‐DAD‐MS/MS method was applied for the screening and structural identification of main components in crude extract, and five components were preliminarily identified as neoeriocitrin, narirutin, naringin, hesperidin and neohesperidin according to their UV and mass spectra. An efficient MAE method for the extraction of the three most abundant components (narirutin, naringin and neohesperidin) was optimized by the combination of univariate and multivariate approaches. The crude extract was then separated and purified by HSCCC and a total of 61.6 mg of narirutin, 207.3 mg of naringin and 159.5 mg of neohesperidin at high purities of 98.1, 97.2 and 99.5%, respectively, were obtained from 1.42 g of crude extract. The recoveries of these compounds were 86, 93 and 89%, respectively. Copyright © 2009 John Wiley & Sons, Ltd.