一对IT恋人的对话

男:就职于一家IT媒体。 女:就职于一家IT公司。 女:亲爱的,最近我发现你情绪低落,反应速度大大降低,是不是头脑里碎片太多,要不要我帮你整理一下? 男:我也说不清楚,我觉得越来越与同事不兼容了。 女:也许这与你和他们配置有关系,你们办公室好像就你一个是从外地毕业分到北京的。 男:这不是主要原因。有时,他们谈得正热闹时,我一插话就死机。     

屑石型高白乳浊釉的试验研究

通过对 1 0 1 0～ 1 0 4 0℃氧化气氛下烧成的高白钛乳浊釉的试验 ,探讨了化学成分、晶粒大小对钛釉的影响 ,遴选出屑石型高白乳浊釉的最佳配方。     

测定诺氟沙星胶囊含量的HPLC法

用高效液相色谱法测定了诺氟沙星胶囊的含量。采用岛津ShimpackODS色谱柱;0.1%(φ)磷酸溶液-甲醇 (体积比55∶25,含1%(φ)三乙胺 ,磷酸调pH2.7)为流动相;检测波长278nm;外标法定量 ,样品测定结果与药典的方法一致。该法快速、准确、可靠 ,结果满意。     

Micromagnetic simulation for high field sensors with perpendicular magnetizations

In this paper, we present a micromagnetic design for high field sensors. The hard layer of the sensors is L1垂直磁化;强磁场传感器;微磁学模拟;高巨磁阻效应micromagnetic simulation, giant magnetoresistive, coercivity, demagnetizing fieldProject supported by the Nature Science Foundation of China (Grant No~10404019) and by the Science and Technology Committee of Shanghai (Grant No~05PJ14090).2006-09-232006-11-28In this paper, we present a micromagnetic design for high field sensors. The hard layer of the sensors is L1垂直磁化;强磁场传感器;微磁学模拟;高巨磁阻效应micromagnetic simulation, giant magnetoresistive, coercivity, demagnetizing fieldProject supported by the Nature Science Foundation of China (Grant No~10404019) and by the Science and Technology Committee of Shanghai (Grant No~05PJ14090).2006-09-232006-11-28In this paper, we present a micromagnetic design for high field sensors. The hard layer of the sensors is L10-FePt which is magnetized perpendicularly to film plane and the sense layer is NiFe which is magnetized in the film plane. The magnetization configurations of the hard and sense layers at different external magnetic fields have been simulated. In micromagnetic simulation, the sense field up to one tesla can be reached by using this sensor. We find that whether the sensor has a symmetric or an asymmetric field-sensing window is determined by the coercive field of the hard layer and the demagnetizing field of the sense layer.Corresponding author. E-mail： yaowen@mail.tongji.edu.cn/qk/85823A/200706/24631993.html7000, 7500, 7570P, 7540Mhttp://cpb.iphy.ac.cn/CN/10.1088/1009-1963/16/6/042https://cpb.iphy.ac.cn/CN/article/downloadArticleFile.do?attachType=PDF&id=1092012006-09-23In this paper, we present a micromagnetic design for high field sensors. The hard layer of the sensors is L10-FePt which is magnetized perpendicularly to film plane and the sense layer is NiFe which is magnetized in the film plane. The magnetization configurations of the hard and sense layers at different external magnetic fields have been simulated. In micromagnetic simulation, the sense field up to one tesla can be reached by using this sensor. We find that whether the sensor has a symmetric or an asymmetric field-sensing window is determined by the coercive field of the hard layer and the demagnetizing field of the sense layer.     

功能化离子液体催化二苯甲酮的合成工艺

二苯甲酮是有机合成的重要中间体和精细化工重要的添加剂,广泛应用于有机涂料、医药、农药、塑料、香料、日用化工、电子化学品及其它特殊化学合成行业和领域.目前,二苯甲酮在工业上的合成工艺路线很多,大体上可以分为以下几种[3-6]:(1)光气法:苯与光气催化反应,收率90%;但光气剧毒,需要投资较大的处理装置.(2)四氯化碳法:苯与四氯化碳缩合水解,原料价格高,有副反应,产率容易下降,且有废液产生.(3)二苯甲烷稀硝酸氧化法:有污染环境的氮氧化合物产生.(4)Friedel-Crafts酰化反应法:以苯和苯甲酰氯为原料,原料易得,操作简单,产率也较高,工业上多采用这种方法.但最古老最成熟的制备过程中需要大量的AlCl3,具有很强的腐蚀性;产物的获得需用酸性溶液水解且产生大量含铝盐的废酸,造成了严重的环境污染和经济浪费.韦长梅[7]用FeCl3替代AlCl3,反应8h,收率82.1%,但需要加压下进行.因此,开发二苯甲酮绿色合成新工艺有着重要的现实意义和工业价值.     

First-Principles Study of Magnetic Properties of TM_(13) and TM_(13)@Au_(32) Clusters(TM = Mn,Co)

The structural and magnetic properties of TM_(13 )and TM_(13)@Au_(32 )clusters(TM=Mn,Co)are studied by firstprinciples calculations.We find that the Au_(32 )cluster can tune not only the magnetic moment but also the magnetic coupling properties between the TM atoms of the TM cluster.The Au_(32 )cluster can increase the net magnetic moment of Mn_(13 )clusters while reducing that of Co_(13 )clusters.The interaction between Au and Mn atoms induces more Mn atoms to form spin parallel coupling,resulting in an increase of the total magnetic moment of Mn_(13 )clusters,while for the Co_(13 )clusters,the interaction between Au and Co atoms does not change the magnetic coupling states between the Co atoms,but reduces the magnetic moment of the Co atoms,leading to a decrease of the total magnetic moment of this system.Our findings indicate that the encapsulation of Au_(32 )clusters can not only raise the chemical stability of TM clusters,but also can tune their magnetic coupling properties and magnetic moment,which enables such systems to be widely applied in fields of spintronics and medical science.     

2010年上海世博会影响力模型及其综合评价

利用时间序列分析了2010年上海世博会的客流总量,类比二维有热源的热传导问题,建立了世博会带动相关产业发展的热力学传导模型．基于灰色关联分析,得到了定量多因素的评价模型,并据此对上海世博会和前几届世博会做了综合比较．     

从国外污水回用情况谈我国城市污水回用

此文描述了国外先进的污水综合利用情况,指明了我国的水资源现状和污水回用的情况,给出了我国进行城市污水资源化应该采取的措花和建议。     

水产食品及酒中微量砷的测定

目前用Ag-DDC(二乙基二硫代氨基甲酸银)测定微量砷,以有毒的吡啶碱作溶剂。也有人用有机碱代替吡啶,用氯仿或二氯乙烷作溶剂,又使灵敏度降低。本文用Ag-DDC及少量吡啶和二氯乙烷作吸收液测定十多种水产品和酒中1—20微克砷。基本上消除了吡啶的毒害,灵     

ZnSe MIS二极管蓝色电致发光的空间分布

本文研究了用ZnS多晶薄膜作绝缘层时制备的ZnSe MIS二极管,在正向电压激发下的蓝色电致发光的空间分布,在光学显微镜下观察到电致发光呈稀疏的点状分布。为了了解发光点的起因,用扫描电镜观测了二极管的二次电子像(SEI),束感生电流像(EBICI)和吸收电流像(AEI)。一个重要的发现是二极管的电致发光点(ELS)和EBICI有相当好的对应关系。文中指出了发光点的存在与绝缘层(Ⅰ)的引入有关。绝缘层一半导体(I-S)界面较大的能带失配和较差的结合,从而产生较多的无辐射复合中心,是产生稀疏发光点可能的原因。文中根据对发光点起因的分析,提出用ZnSe多晶薄膜取代ZnS多晶薄膜作绝缘层来铡备ZnSe MIS二极管。当用显微镜观察时,电致发光点呈密集分布,而用肉眼观察时是均匀的蓝色发光。文中还指出了进一步改进电致发光空间分布的可能途径。