十六烷基三甲基溴化铵柱撑膨润土的制备及其吸附刚果红特性研究

制备了十六烷基三甲基溴化铵柱撑膨润土,考察了p H、吸附剂用量、震荡时间、刚果红初始浓度和温度等条件对其吸附刚果红行为的影响,研究了热力学、动力学、等温线等。研究结果表明,十六烷基三甲基溴化铵柱撑膨润土较原土吸附能力强;吸附率随p H值增加而减小;吸附过程符合准二级动力学模型,化学吸附控制吸附速率;Langmuir等温模型与吸附过程相关系数较大,理论最大吸附量达819.83 mg/g;热力学参数表明熵增是吸附的推动力。本研究证实十六烷基三甲基溴化铵柱撑膨润土是具有前景的分离水环境中阴离子染料的吸附材料。     

前置反射器比色高温计的研究

研究了一种改进的比色高温计测量表面温度,测量范围为600~1200℃.将半球型镀金反射器置于比色高温计上,利用多次反射效应,可缩小两个接收波长的有效发射率之间的差异,从而减小比色高温计误差.研究了反射器对焦情况下的辐射特性,推导出有效发射率的表达式.为避免反射器对被测面温度场的破坏,设计了一套快速测量装置,每次测量需时0.7s.为验证其准确性,制作了平片热电偶,直接测量平片热电偶的表面温度.结果显示,与平片热电偶相比,测量误差小于1.1℃.     

带浇水功能的花盆

正材料剪刀、塑料瓶、棉线、美工刀、水、营养土、花苗。步骤1.用美工刀将塑料瓶从中间割开,分成甲、乙两部分。2.如图,用剪刀在甲上剪出许多长条,长条宽度约为1厘米。33.拿起一根长条,将它横折放在右边第一根长条的上面根长条的上面,再将多余的部分放到右边第二根长条的下面根长条的下面。用同样的方法编织其余长条。     

基于强化研磨轴承套圈表面化学成分分析

强化研磨是一种金属表面处理的新型精密加工工艺,文章采用对轴承套圈表面进行强化研磨加工工艺,通过X射线能谱仪对强化研磨加工前后试样表面化学元素组成成分及含量进行对比分析,得出经过表面强化研磨处理过的试样表面发生摩擦化学反应,元素种类增加,原子百分比含量发生相应变化,如B、N元素含量增加,这为研究强化研磨加工工艺能否在套圈表面形成含B、N化学物理膜层(B2O3、BN、硼酸酯铁、含氮有机物等)提供了相关实验依据.     

Image charge effect on the light emission of rutile TiO_2(110) induced by a scanning tunneling microscope

The plasmon-enhanced light emission of rutile TiO_2(110) surface has been investigated by a low-temperature scanning tunneling microscope(STM). We found that the photon emission arises from the inelastic electron tunneling between the STM tip and the conduction band or defect states of TiO_2(110). In contrast to the Au(111) surface, the maximum photon energy as a function of the bias voltage clearly deviates from the linear scaling behavior, suggesting the non-negligible effect of the STM tip on the band structure of TiO_2. By performing differential conductance( dI/dV) measurements, it was revealed that such a deviation is not related to the tip-induced band bending, but is attributed to the image charge effect of the metal tip, which significantly shifts the band edges of the TiO_2(110) towards the Femi level(E_F) during the tunneling process. This work not only sheds new lights onto the understanding of plasmon-enhanced light emission of semiconductor surfaces, but also opens up a new avenue for engineering the plasmon-mediated interfacial charge transfer in molecular and semiconducting materials.     

Quantum oscillation measurements in high magnetic field and ultra-low temperature

The physical properties of a solid are determined by the electrons near the Fermi energy and their low-lying excitations. Thus, it is crucially important to obtain the band structure near the Fermi energy of a material to understand many novel phenomena that occur, such as high-T_c superconductivity, density waves, and Dirac-type excitations. One important way to determine the Fermi surface topology of a material is from its quantum oscillations in an external magnetic field. In this article, we provide a brief introduction to the substation at the Synergetic Extreme Condition User Facility(SECUF),with a focus on quantum oscillation measurements, including our motivation, the structure of and the challenges in building the substation, and perspectives.     

有效因子综合偏好强度与CVaR整合优化模型

本文从股票多维特征因子中选择有效因子,融合形成最大化有效因子综合偏好强度(IPS)的附加理性,构建并验证IPS-均值-CVaR投资组合优化模型。基于沪深300股2006~2015年数据分析显示:(1)有效因子IPS投资组合优越于单因子投资组合;(2)IPS方法相较于因子打分法,具有更优的多维数据整合功效;(3)IPS-均值-CVaR投资组合优化模型相对于均值-CVaR模型具有更优越的资产选择能力,也拓展了投资组合模型的多维数据处理能力和适用性。     

紫外光电芬顿降解四环素性能研究

以钌铱钛电极为阳极，碳刷为阴极，长波紫外线LED灯为光源构建光电芬顿体系降解四环素.研究了四环素初始浓度、电流密度、pH值和通气条件对四环素降解的影响及不同类型的活性氧簇所发挥的作用.结果表明，·OH是降解四环素的主要活性物种，适宜的pH条件(pH=3)、通气增氧可显著提高四环素的降解率.当电流从60 mA增加至100 mA,四环素的降解率可提高至95.51%,最佳条件下四环素降解率达97.00%,矿化率达57.85%.     

基于XSLT和XML的智能电子表单的研究

随着网络技术与信息处理技术的发展,基于传统纸质表单和针对每个表单编写固定程序代码的表单模式,已不能满足现在信息处理的需要。本文简要介绍了智能电子表单的工作原理、XSLT的构成和处理模型以及基于XSLT和XML的智能电子表单功能设计。