Synthesis and Crystal Structure of (Z)-N-(2-(diethylamino)ethyl)-7-(5-fluoro-2-oxoindolin-3-ylidene)-2-methyl-4,5,6,7-tetrahydro-1H-indole-3-carboxamide Methanol Solvate

The crystal structure of a new compound (Z)-N-(2-(diethylamino)ethyl)-7-(5- fluoro-2-oxoindolin-3-ylidene)-2-methyl-4,5,6,7-tetrahydro-1H-indole-3-carboxamidemethanol solvate (C24H29FN4O2CH4O, Mr = 456.55) has been prepared and determined by single-crystal X-ray diffraction. The crystal is of monoclinic, space group P21/c with a = 14.560(3), b = 7.3200(2), c = 22.233(4) , β = 101.78(3)°, V = 2319.7(8) 3 , Z = 4, Dc = 1.307 g/cm 3 , F(000) = 976, μ = 0.092 mm -1 , MoKa radiation (λ = 0.71073), R = 0.0604 and wR = 0.1644 for 4262 observed reflections with I > 2 (I). X-ray diffraction analysis reveals that the indole and pyrrole are almost coplanar. Intramolecular C-H···O and N-H···O hydrogen bonds together with π-π interactions are found in the structure.     

超声辅助酶法提取-原子荧光光谱法测定富硒黑木耳中硒形态

建立了富硒黑木耳中硒代胱氨酸、硒代半胱氨酸、亚硒酸、硒蛋氨酸、硒酸5种硒形态的液相色谱-原子荧光光谱分析方法。通过链酶蛋白酶E酶解,结合超声提取后,选取Hamilton PRP-X100离子交换色谱柱(250 mm×4.1 mm,10μm),40 mmol/L的磷酸氢二铵为流动相,在16 min内,5种硒形态完全达到基线分离。5种硒形态在线性范围内相关系数R为0.9990~0.9999;加标回收率为76.1%~108%;检出限分别为硒代胱氨酸0.35μg/L、甲基-硒代半胱氨酸0.46μg/L、亚硒酸0.26μg/L、硒代蛋氨酸0.64μg/L、硒酸3.06μg/L;方法应用于富硒黑木耳中硒形态的分析,精密度高、重现性好、方法稳定、准确可靠,是测定富硒黑木耳中硒形态含量的有效方法。     

胡萝卜施用“禾肥宝”牌酵素菌有机肥的肥效试验

在乌兰县胡萝卜的种植中,进行了“禾肥宝”牌酵素菌有机肥肥效试验。结果表明：“禾肥宝”牌酵素菌有机肥能够促进胡萝卜肉质根长、肉质根横径、单根重的增长,提高产量,对胡萝卜肉质根的裂根率,分叉率影响不大;“禾肥宝”酵素菌有机肥2 600 kg/hm^2是乌兰地区胡萝卜施用酵素菌有机肥的最佳施用量。     

孟塞尔标号向CIE色座标的转化

本文提出了一种从孟塞尔标号(H、V、C)向CIE色座标(x、y、Y)转化的新方法,该方法利用了牛顿插值公式及二元函数插值法。为了准确迅速地在计算机上实现这种转换,给出了转换程序。     

公平和效率兼顾的教师远程继续教育模式

公平与效率的和谐是教育发展的永恒追求。现代远程教育彻底打破了时空的限制,实现资源共享,提供给每个受教育者相同的受教育机会;同时减少教育成本投入,提高学习效率,成为符合时代发展需求的新型教师继续教育模式。     

Algorithms for semi on-line multiprocessor scheduling problems

In the classical multiprocessor scheduling problems, it is assumed that the problems are considered in off-line or on-line enviromnent. But in practice, problems are often not really off-line or on-line but somehow in between. This means that, with respect to the on-line problem, some further information about the tasks is available, which allows the improvement of the performance of the best possible algorithms. Problems of this class are called semi on-line ones. The authors studied two semi on-line multiprocessor scheduling problems, in which, the total processing time of all tasks is known in advance, or all processing times lie in a given interval. They proposed approximation algorithms for minimizing the makespan and analyzed their performance guarantee. The algorithms improve the known results for 3 or more processor cases in the literature.     

基于“数字城市”的昆明市规划和管理信息系统初步研究

分析阐述了“数字城市”的概念，目前国内外的研究情况，以及其主要技术和应用领域，然后以昆明市为例提出构建昆明市规划和管理信系统的设想。     

迄今发现最早的郑和下西洋船队图像资料--<天妃经>卷首插图

郑和下西洋是航海史上的壮举,但是关于下西洋所使用的大型船舶--宝船的船型及样式,却一直缺乏历史的图像资料.文章仅就新发现的一幅<天妃经>的卷首插图郑和航海图进行介绍.文中指出,该图关于郑和船队的形象,可以作为宝船是福船型的有力证据.     

扭矩对三维空间圆截面曲杆弹性屈曲的影响

采用自然坐标系,由Green应变张量的定义,给出了自然坐标形式的三维细长空间曲杆的Green应变计算公式,建立了同时考虑轴向压力和扭矩影响的能量变分方程.采用2节点12个自由度的自然坐标形式的三维空间曲梁单元,采用线性特征值分析方法,研究分析了同时受轴向压力和扭矩作用的具有初始曲率和挠率的三维空间杆柱的屈曲问题.数值结果与存在的理论解极为吻合,验证了公式的正确性.更为引人注意的是:不论直杆还是曲杆,扭矩对它们的弹性屈曲影响不可不计.