山梨酸的制备

本文讨论的是巴豆醛与乙烯酮在辛酸锌的催化下反应生成聚酯,然后水解生成山梨酸,产率为78％。产品经红外光谱、纸色谱、薄层色谱及中和滴定测定,纯度为99.45％。     

我国现阶段垄断现象的分析

分析了我国现阶段垄断现象产生的特殊原因、形式特点以及对经济发展产生的积极作用等问题。     

1,4—脱水—D,L—木糖醇的制备

戊糖醇酸催化脱水可得到脱水戊糖醇,但产物往往是一系列脱水及取代产物的混合物。本文采用工业木糖醇为原料,经提纯后以浓盐酸或对甲基苯磺酸为脱水剂在氮气中脱水主要得到呋喃型1,4—脱水—D.L—木糖醇。产物易于分离提纯。     

单光镊光阱力分析

在几何光学近似下，利用光线追踪法分析了激光微束作用于微粒的作用力，数值计算中考虑了激光微束的具体结构对光阱力的影响。分析表明：相对折射率和激光束腰对光阱力有重要影响，另外激光波长和微粒大小对光阱力也有一定影响。     

重庆市战略性新兴产业空间集聚测度及时空演变分析

【目的】战略性新兴产业能够带动未来区域经济的发展,深入研究这些产业的空间特征对区域内产业空间结构优化调整有重大意义。【方法】运用Ripley’s K函数、核密度分析等方法研究了战略性新兴产业的地理集聚特征及空间演变特征,并引入空间化的GDP数据分析了产业分布与GDP的关系。【结果】重庆市战略性新兴产业集聚化特征明显,各类产业集聚程度均呈增加趋势,但不同产业类型的集聚特征存在显著差异;4个时期的最高核密度值依次为:0.47,3.30,16.33,29.06,核密度最高值均出现在主城区;战略性新兴产业的平均中心移动轨迹整体表现为由东北逐渐向西南方向偏移;战略性新兴产业的时空演变规律与空间化的GDP数据高度吻合。【结论】研究探明了重庆市战略性新兴产业空间格局演变的特征,并印证了战略性新兴产业与区域GDP之间存在必然的联系,为相关部门在宏观上对战略性新兴产业的调控和布局提供了有效的依据。     

Performance of the low pressure MWPCs for f ission fragments under a high background

Two couples of low pressure multi-wire proportional chambers (MWPC) were located in the target chamber to detect fission fragments in a hypernuclei producing experiment at Thomas Jefferson National Laboratory (Jlab). In the experiment, a continuous wave (CW) electron beam was applied to form hypernuclei by electromagnetic interaction. In the target chamber, the high energy (1.853 GeV) and high intensity (500 nA) primary electron beam caused a high particle background, which influenced the detection of the fission fragments. This report described the design of the MWPCs and studied the fission-fragment detecting performance of them under such a high background. The efficiency of the MWPCs was given with the help of a high resolution kaon spectrometer. At the same time, the background particles were discussed with a Monte Carlo code based on GEANT4.     

在离子液体中合成多取代苯基异丙基醚

以1-甲基3-丁基咪唑四氟硼酸盐离子液体为反应介质,由多取代苯酚与2-溴丙烷反应合成了12个多取代苯基异丙基醚,其结构经1H NMR和IR确证.     

Generalized Principal-State-of-Polarization Analysis and Matrix Model for Piezoelectric Polarization Controllers

We introduce a generalized concept of principal state of polarization （PSP） to analyse the piezoelectric polarization controller （PPC） and find each PPC unit can be described by a rotation matrix determined by the PSP. Our PPC has three components, each made of a jaw and a piezoelectric actuator with the squeezing direction tilted 0°, 45° and 0°, which are driven by a tunable power supply. We demonstrate that all the polarization rotation angles are linear to driving voltages and the PSP of unit 2 is nearly orthogonal to others which are almost equal. Taking some approximate treatments we obtain the matrix model of our PPC with respect to three driving voltages. The average error of our theoretical model is 1.51°, and the polarization response time is 〈50 μs, which is promising to realize an open-loop control of polarization.     

天然气和“报警员”

对于豁达者而言,任何日子都是美满幸福的。硫化氢是一种有臭鸡蛋气味的气体,很难闻。平时,其他气体都不愿接近它。这一天,它来到天然气管道中,里面的乙烷看到后问:"你来干什么?"里面的甲烷也不客气地说:"你赶快走,讨厌的家伙!"