稀土元素ICP—AES法摄谱数据的简便处理

本文用PC－1500微机以三次多项式拟合的方法处理稀土元素ICP－AES法摄谱数据，讨论了实验方面的有关问题，提出了一套较为简便的实验方法。通过人工合成样分析及磷矿基体中的加料回收实验，证明本法符合实用要求。     

JY70P等离子体光量计通讯功能的开发

最近我们从法国引进了一台等离子体光量计。本文介绍了在该仪器上开发通讯功能的一种方法，在仪器内部手稿接口板，接上数据传输线，编制通讯软件并使其纳入到原系统软件模块中去，从而完成了异型机之间的PASCAL操作系统下的通讯功能的开发任务。     

等离子体发射光谱法同时测定铬铁矿中铬、铁、镁和铝

铬铁矿属难熔矿种之一，经典分析方法在铂金坩埚内过氧化钠半熔，容量法测定铬、铁离子交换分离富集后，再用容量法或比色法测定其它元素，分离手续繁杂，耗费试剂多，周期长。等离子光谱（ICP）技术具有稳定性好、灵敏度高、线性范围宽、化学干扰少、多元素同时测定等优点，但由于仪器进样量和雾化效率受测定溶液含盐量的限制，试样前处理通常用酸分解，或碱熔后经沉淀分离除去大量可溶性盐类，用酸溶液沉淀，定容，待测。本文利用ICP上述优点对碱熔试样不经分离直接酸化，对高倍稀释试液测定铬铁矿中的主量元素进行了探讨。试验表明，此设想是可行的。本文还就试样的分解条件、酸度、元素间的光谱干扰作了研究，拟出了同时测定铬铁矿中铬、铁、镁、铝的分析方法。本法 质矿产部标准试样的结果与推荐值对照，符合要求。本法称取试样量少，试剂用量少，用银坩埚代替昂贵的铂坩埚，不经分离直接酸化后同时测定4种主量元素，大大简化了操作手续，为分析铬铁矿中主量元素的含量寻找了一条准、快、省的途径。     

Studies of Several Systems with Air Electrode Electro-Synthesizing H2O2 on the Spot for Degrading Aniline in Aqueous

A gas diffusion electrode (air electrode) with a high current efficiency of electro-synthesizing H2O2 using O2 in air was prepared. The several systems with air electrode as cathode of electro-synthesizing H2O2 on the reaction spot for degrading aniline in aqueous--electro-Fenton system, photo-excitation electro-H2O2 system and photo-electro-Fenton system, were developed. The rates of decomposition of H2O2 and mineralization of aniline were experimentally measured respectively under different conditions, and the results indicated there has an excellent parallel relation between decomposition rate of H2O2 and mineralization rate of aniline. Especially, photo-electro-Fenton system, where H2O2 is decomposed the fastest, is the best system of oxidizing and degrading organic toxicants. Compared photo-electro-Fenton system with photo-Fenton system, important role is revealed in the interface of air electrode. In this paper, the mineralization mechanism of aniline in the photo-electro-Fenton system was also discussed.     

浅谈油田开发钕铁硼永磁体温度和环境对其性能的影响

本文简述了工作温度和环境对油田开发用钕铁硼永磁体磁性能的影响，并探讨了改善钕铁硼永磁体耐热、耐蚀性的方法。     

Experimental Evidence of the Rapidly Increasing Neutron Yields in Proton—Induced Reaction on Heavy Target Across 0.6—1 GeV

The independent yield distribution of the Hg isotopes,measured for the reaction of 600MeV ^18O projectile with a ^nat.Pb target,is converted to 18O 208Phb system and is compared with an Hg-isotope distribution from the spallation reaction of 1A GeV^208Pb on proton.The comparison shows the differences between the two distributions on the production cross sections,isotope-distribution widths as well as their shapes.A great increase of the neutron-deficient Hg isotope yield with increase of bombarding energies of protons from 600MeV to 1GeV is derived.This fact results in an experimental evidence for rapid increasing neutron yields with rising proton bombarding energy from 0.6GeV to 1 GeV.     

CCD狭缝摄象

在过去的几十年中,各靶场已广泛应用狭缝摄影对种种飞行弹丸的多项重要技术参数进行测试,它在许多测试项目中应用的有效性、广泛性和经济性已被人们所肯定。据报道,在国外的一些靶场所进行的发射试验中,狭缝摄影机曾占全部测试设备中所使用的摄影仪器的百分之九十,这是因为狭缝摄影有其独特的、其它方法不可比拟的优点。