ZLRJ－I型智能流量热量积算仪

论述了ＺＬＲＪ－Ｉ型智能流量热量积算仪的设计与现行的流量热量仪表之间的差异。介绍了该仪器原理、特点,及其利用微机技术、弯管流量计技术、ＡＤ５９０温度测量装置,解决了供热管网系统中流量节流装置测量准确度低、阻力损失大、大管径一次元件加工精度难以保证、安装不方便等四大难题。     

企业应用程序的Web层与EJB层接口的实现

介绍了在利用J2EE开发企业管理系统时Web层与EJB层接口的实现技术.提出了多种合理的解决方案,使得调用EJB的程序更加简捷.     

非线性Schrdinger方程的Compacton解和孤立波解

研究了非线性Schro..dinger方程:iut+αuxx+β|u|2pu=0(p为任意实数),得到丰富的孤立波解:当p>0时得到孤立波解,p<0时得到移动Compacton解,p=0时得到Compacton解;研究了(2+1)维非线性Schro..dinger方程的解,并推广到(n+1)维非线性Schro..dinger方程 还比较了任意维非线性Schro..dinger方程解的情况以及不同解与系数的关系     

关于两个角平分线不等式的探讨

对文献[1]和文献[2]中提出的两个不等式作了新的探索,运用数学软件Mathematica4.0在计算机上进行了数值推导,并进行了一部分的严格理论证明。给出了关于这两个几何不等式的一些数值结果。     

Duffing 系统的非线性反馈同步控制

对Duffing混沌系统进行非线性反馈控制，设计出一种含参控制器，使得受控Duffing系统的某一状态变量与任意给定的参考信号同步．利用Lyapunov函数方法证明在此控制器作用下该系统的此状态变量按指数速率收敛到参考信号．在此基础上，研究了该受控混沌系统的自同步和异结构同步问题．数值仿真结果说明了此控制器设计方法的有效性．     

in-situ ESR AND RAMAN SPECTROSCOPIC STUDIES ON ELECTROPOLYMERIZATION OF PYRROLE

The in-situ transient ESR measurements reveal that the oxidized structure (PP++) of polypyrrole (PP) films has an electrocatalytic activity to the oxidation of pyrrole during the electropolymerization process. Surface-enhanced resonance Raman scattering (SERRS) effect was used to probe the structure of PP films in very early stages of the polymerization on gold electrodes. It is of special interest that the electropolymerization can take place at much less positive potentials (about 300 mV) under the irradiation of light. This photocatalytic effect may be applied to the pattern deposition of polymers.     

表面等离子体共振生物传感器研究人参皂甙与血清白蛋白的相互作用

To use a newly developed wavelength modulation surface plasmon resonance （SPR） biosensor, an experimental protocol was developed to investigate the interaction of ginsenosides with serum albumin. With a known concentration of the ginsenosides, bound percentages of the ginsenosides with human serum albumin （HSA） or bovine serum albumin （BSA） were obtained. SPR technique could require no labeling and this method provided the detailed information on association and disassociation of molecules in real time. The results indicate that the sensitivity of wavelength modulation SPR biosensor is sufficient for detection and characterization of binding events involving low-molecular weight compounds and their immobilized protein targets.     

Nd2O3掺杂(BaSr)TiO3对陶瓷结构和性能的影响

采用常规固相反应法,以Ba0.6Sr0.4TiO3 10%MgO(BSTO)体系为基体成分,研究了Nd2O3掺杂对其显微组织结构和介电性能的影响规律,结果表明掺杂Nd2O3后,抑制了BSTO晶粒的生长;随着Nd2O3掺杂量的增加,陶瓷的晶粒尺寸变小,密度增大,材料的居里温度向负温度方向移动,并且展宽了介电峰,使材料的温度稳定性提高,此外,随着Nd2O3掺杂量的增加,材料的可调性减小,介电常数减小。     

自旋标记鬼桕类化合物圆二色谱的研究

给已知抗癌药物分子中引入稳定氮氧自由基,合成较母体药物高效低毒的抗癌药物已引起国内外学者的重视.我们在具有抗癌活性的鬼桕毒分子中引入稳定氮氧自由基,药理试验表明其活性保持或增加,而毒性却显著地降低.     

Purification of 2,6-Diisopropylnaphthalene by Static Melt Crystallization from a Mixture Containing Diisopropylnaphthalene Isomers

2,6-Diisopropylnaphthalene （2,6-DIPN）, as the precursor of important monomer 2,6-naphthalene dicarboxylic acid, could be produced by the shape-selective isopropylation of naphthalene with propene resulting in an isomeric mixture having different alkylation levels. Since the boiling points of DIPNs were very close and the differences of melting points in-between isomers were quite distinctive, the static melt crystallization was applied to separate and purify 2,6-DIPN from its isomers. 2,6-DIPN with purity ≥99% was produced through a process of three stages： crystallization→sweating→melting. The phase diagram of 2,6-DIPN-2,7-DIPN binary system was plotted to opti- mize the temperature control of crystallization. By repeated crystallization of melts with different concentration levels, the yield of pure 2,6-DIPN could be enhanced to 87%. No solvent was necessary. Keywords 2,6-diisopropylnaphthalene, static melt crystallization, crystallization rate, sweating rate, eutectic temperature