排序方式: 共有29条查询结果,搜索用时 796 毫秒
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建立了同时测定污水中7种糖皮质激素的固相萃取-超高效液相色谱串联质谱的分析方法.利用单因素实验优化固相萃取影响因素:洗脱液、洗脱体积、水样pH值及淋洗液.在此基础上,进行L9(34)正交实验.通过直观分析和方差分析区分主次因素,确定了最佳固相萃取条件:洗脱剂为乙酸乙酯,洗脱剂用量为10 mL,pH=5.0,清洗剂为20%甲醇.7种糖皮质激素的检出限为1.56~10.59 ng/L;在20~100 ng/L的3个添加水平范围内的平均回收率为72.5%~101.4%,相对标准偏差(RSD)小于10.9%. 相似文献
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This paper uses a nonperturbative scattering theory to
study photoelectron angular distributions of homonuclear diatomic
molecules irradiated by circularly polarized laser fields. This
study shows that the nonisotropic feature of photoelectron angular
distributions is not due to the polarization of the laser field but
the internuclear vector of the molecules. It suggests a method to
measure the molecular orientation and the internuclear distance of
molecules through the measurement of photoelectron angular
distributions. 相似文献
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温度荷载下薄板的弹性理论分析 总被引:1,自引:0,他引:1
把三边简支一边固支矩形薄板受沿厚度方向均匀变化的温差荷载作用的问题视为一边作用等效温差力矩的四边简支板与在温差荷载作用下的四边简支板的叠加。根据固定边界的位移协调条件导出温差荷载引起的板内力的表达式和挠度方程。 相似文献
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以双酚A型环氧树脂为基体、甲基纳迪克酸酐为固化剂、聚磷酸铵为膨胀阻燃剂、水热法制备的二氧化钛纳米管(TNTs)为阻燃协效剂,共混后交联固化制得了膨胀阻燃型环氧树脂复合材料。采用极限氧指数测试、垂直燃烧实验、扫描电镜和拉曼光谱分析了添加TNTs对环氧树脂膨胀阻燃材料的阻燃成炭协效作用。结果表明:TNTs的引入提高了环氧树脂膨胀阻燃材料的极限氧指数以及垂直燃烧UL-94测试评级。当TNTs质量分数为2%时,膨胀阻燃体系的极限氧指数达到28.4%,UL-94达到V-1级。同时,TNTs延缓了环氧树脂膨胀阻燃材料在高温下的热降解,提升了体系高温热稳定性和成炭性能。TNTs可以作为成炭的网络骨架,并促进高温下生成更多连续致密的炭层结构,且高温煅烧后残留的炭层具有更低的ID/IG(拉曼光谱在1 360cm-1及1 600cm-1处的吸收峰强度比)值,石墨化程度更高,炭层结构更加致密规整。 相似文献
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考虑到投资者通常采取安全第一的准则,采用跟踪偏差的下半概率作为跟踪风险的度量;而为在恰当描述证券收益分布的厚尾特性的同时克服机会约束对模型求解所造成的困难,假设风险资产的收益服从多元t分布,由此建立了新型金融指数跟踪模型.在分析所建立模型结构特性的基础上,文中还导出了该模型的解析最优解.实证结果表明了新模型的有效性和实用价值. 相似文献
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The photoelectron angular distributions (PADs) of hydrogen
atoms in an intense laser field of linear polarization are studied
using the S-matrix theory in the length gauge. The PADs show main
lobes along the laser polarization and jet-like structures sticking
from the waist of main lobes. Our previous prediction, based on a
nonperturbative scattering theory of photoionization developed by
Guo et al, showing that the number of jets on one side of PADs
may increase by one, three, or other odd numbers and may decrease by one
when one more photon is absorbed, is confirmed by this treatment.
Within the strong-field approximation, good agreement is obtained
between these two quite different treatments. We further study the
influence of the Coulomb attraction to PADs, by taking a
Coulomb--Volkov state as the continuum state of photoelectrons. We
find that under the influence of the Coulomb attraction, the PADs
change greatly but the predicted phenomena still appear. This study
verifies that the jet-like structures have no relation with the
angular momentum of photoelectrons. 相似文献