Spectrofluorimetric analysis of cefoxitin in pharmaceutical dosage

A fluorescence method involving sample pre-treatment is investigated concerning the determination of cefoxitin. A fluorescent product is formed when samples containing cefoxitin are subjected to alkaline hydrolysis with 1.0M sodium hydroxide and heated for 60 min at 90 degrees . The fluorescence is measured in ethanol/water medium (50% v/v) at approximately pH 2.0 provided by adding of 0.1M hydrochloric acid. The fluorescence excitation and emission maxima were 317 and 400 nm, respectively. The quantitative range is between 0.020 and 1.40 mug/ml. A detection limit of 2 x 10(-3) mug/ml was found. The proposed method has been applied to the determination of cefoxitin in commercial injections, saline and glucosed physiological serum.     

Comparative voltammetric study of 2,4-dinitrophenol (DNP), albumin and DNP-albumin as an analytical approach to the use of DNP as a universal label in immunoelectrochemical assays

A comparative electrochemical study of 2,4-dinitrophenol (DNP), albumin and DNP-albumin has been carried out at a hanging mercury drop electrode, in order to use DNP as a universal label in immunoelectrical assays. Several electrochemical techniques have been used. Differential pulse voltammetry has proved to be the most suitable. Wide dynamic linear ranges (more than three orders of magnitude for DNP-albumin) and low detection limits have been achieved (5 x 10(-10)M, 2 x 10(-10)M, 3 x 10(-12)M for DNP, albumin and DNP-albumin, respectively). Good reproducibility has been obtained in all cases (R.S.D. < 2.2%).     

知识经济与科技发展若干问题研究

随着现代科学技术的迅猛发展,特别是信息科学和信息传播手段的日益发展,知识量在短时间内发生猛增,这种“知识爆炸”现象及知识在经济生活中的广泛应用,导致人类社会出现一种新型的经济。这种经济就称为知识经济。它将使人类步入一个以智力资源的占有配置,知识的产生、分配、使用(消费)为重要因素的经济时代。当前“知     

福建省农业现代化过程中的科学技术政策研究

改革开放以来,福建省的农业和农村经济得到了飞速发展,为我省国民经济提前翻两番作出了贡献。并进一步提出了要在坚持“增粮增收保供给,脱贫致富奔小康”的基础上,加快发展现代农业,全面推进小康建设。农业现代化是农业良种化、水利化、化学化、机械化、电气化、生态化、持续化、工业化和农民知识化、农村小城镇化的综合体现。世界上发达国家科技对现代农业的贡献率高达80％左右,说明农业的根本出路在于科技进步。农业现代化的关键     

软磁Fe基纳米微晶的穆斯堡尔谱研究

对纳米软磁合金Ｆｅ７３Ｃｕ１Ｎｂ１．５Ｍｏ２ｓＩ１２．５Ｂ１０的制备态和各退火态的室温Ｍｏｓｓｂａｕｅｒ谱研究,发现非晶相的超精细内场存在高场和低场两部分,