创建"能力超市"实训基地培养高技能人才

“能力超市”是模仿商业超市的功能而建设的一种校内实践教学基地，主要培养高技能人才，具有开放性、仿真性、高效性等特点，在高职院校实践教学体系中具有一定的发展优势。     

Poisson方程的一种Mortar型广义差分法

给出了Poisson方程的一种Mortar型广义差分法,试探函数空间取为一次有限元空间,检验函数空间取为与对偶单元相对应的分片常数空间,并给出了一个相应的误差分析结果.     

慢性铅中毒一例

详细问诊，为诊断慢性铅中毒提供了重要依据。     

海水中三丁基氟化锡(TBTF)的比色测定

三丁基氟化锡是国内外船底防污漆中广泛使用的毒料之一。对防污漆的深入研制,要求掌握防污漆中的毒料在海水中的渗出情况。然而,快速、简便的测定海水渗出液中微量TBTF的方法目前报导极少。二苯基卡巴腙已成功地被用于卤代二丁基锡的测定。本文以二苯基卡巴腙为显色剂测定了防污漆海水渗出液中的TBTF,取得了较为满意的结果。     

PrCl3催化漆酚干燥成膜的研究

Pr原子特殊的电子层结构使其具有多方面的催化特性．实验发现质量分数为0．7％的PrCl3就可使漆酚(U)于110℃固化成膜的时间从5h降低到1h．用可见分光光度法、电子能谱、紫外和红外光谱等方法研究U在PrCl3作用下的固化成膜历程．结果表明，在Pr(Ⅲ)催化U聚合的过程中首先是U与PrCl3发生配位作用，生成U镨配合物(UPr)，然后该配合物分子中的Pr(Ⅲ)催化U聚合成体形结构的高分子化合物．     

STUDY ON THE CARDANOL-ALDEHYDE CONDENSATION POLYMER CONTAINING BORON-NITROGEN COORDINATE BOND

Cardanol-aldehyde condensation polymer containing boron-nitrogen co-ordinate bond (CFBN) has been synthesized and characterized by IR, XPS, HPLC andDTA-TG. Its properties were also investigated. The results show that the coating filmof CFBN has excellent physico-mechanical properties, good anticorrosive properties andstable at high temperature.     

Comparison of(η~6-Fluoroarene)tricarbonylchromium Complexes with Their Chloro-analogs in Radical Aromatic Substitutions

Reactions of fluoroarene-Cr(CO)_3 complexes with SmI_2 andcarbonyl compounds in THF/HMPA at-40— -60℃ affordedthe corresponding radical aromatic substitution products in highyield. Compared to the corresponding chloroarene-Cr.(CO)_3complexes, fluoroarene-Cr(CO)_3 complexes showed a higher ef-ficiency and slightly lower regioselectivity.     

GEOENVIRONMENTAL CHARACTERS OF YELLOW (HUANGHE) RIVER SUSPENDED LOAD

Three important characters of the suspended load of the Yellow (Huanghe) River are discussed, i.e. its temporal fluctuation as a function of solar activity, its uneven spatial distribution along the main course and the inevitability of these phenomena as a natural earth process rather than a result of disturbed ecological system caused by human activity. Implications of this understanding with regard to the control of the Yellow River are also discussed.     

二氧化钛光催化体系中的羟基自由基的测定

通过ESR光谱测定表明TiO2悬浮液在紫外光照射下产生羟基自由基氧化物种.羟基自由基氧化酸性桃红(sulforhodamine B,SRB)使其褪色,在565 nm处用分光光度法测定其吸光度值的变化,可间接测定羟基自由基的生成量.确定了体系的最佳实验条件pH为2.5;SRB浓度为2.0×10-5mol/L;TiO2浓度为0.1 g/L;光照时间为12 min.采用抗坏血酸为羟基自由基清除剂,测定了其自由基清除率,表明拟定该体系可作为筛选抗氧化剂的方法之一.