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Chemical Synthesis and Characterization of Flaky h-BCN at High Pressure and High Temperature
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Hexagonal boron carbonitrogen (h-BCN) compound is synthesized from a mixture of boron powder and CNH compound prepared by pyrolysis of melamine (CaH6N6) under high temperature (1400-1500℃) and high pressure (5.0-5.5 GPa). X-ray photoelectron spectroscopy, Fourier transform infrared spectroscopy and Raman spec- troscopy are used to determine the chemical composition and bonds of the product. The results show that the product has composition of B0.18C0.64N0.16 (near BC4N) and atomic-level hybrid. X-ray diffraction analysis indicates that the powder has a hexagonal network structure. Scanning and transmission electron microscopy results suggest that h-BCN compound morphology is mainly flaky in width about 1 μm and thickness 200nm. 相似文献
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