植物营养剂对沙梨品质的影响

采用田间试验和仪器分析方法,研究了植物营养剂对沙梨品质的影响．结果表明：植物营养剂处理的沙梨品质高于常规对照,有益矿物质元素硒的含量比常规对照增加1542．9％,为0．046ug／kg,在人体正常需求范围内,对人体具有保健作用,有害元素铅、镉、汞含量比常规对照分别减少30％、23．9％、6．35％,维生素C的含量没有变化．     

蓝光445nm/绿光532nm双波段激光物证搜索仪

激光物证搜索仪,可以无损直接发现潜在手印、汗液、精斑、血液等体液和其它隐藏,处理或者覆盖过的证据等,而不用对其进行化学预处理,从而保证其原始信息的真实性、完整性和生物活性。各种波长的激光物证搜索仪中,输出波长445nm的蓝激光和532nm的绿激光物证搜索仪最具有应用价值。设计了基于输出波长445nm/532nm的蓝绿光双波段激光物证搜索仪,系统实现三种波段激光(蓝光、绿光、蓝绿光混合)输出,结合了(蓝光/绿光)分别在物证搜索的优势,扩大了应用范围,提高了现场操作性,具有较大的推广应用价值。     

Microwave absorption properties regulation and bandwidth formula of oriented Y2Fe17N3-δ@SiO2/PU composite synthesized by reduction-diffusion method

As concepts closely related to microwave absorption properties, impedance matching and phase matching were rarely combined with material parameters to regulate properties and explore related mechanisms. In this work, reduction-diffusion method was innovatively applied to synthesize rare earth alloy Y$_{2}$Fe$_{17}$. In order to regulate the electromagnetic parameters of absorbers, the Y$_{2}$Fe$_{17}$N$_{3-\delta }$ particles were coated with silica (Y$_{2}$Fe$_{17}$N$_{3-\delta }$@SiO$_{2}$) and absorbers with different volume fractions were prepared. The relationship between impedance matching, matching thickness, and the strongest reflection loss peak (${\rm RL}_{\rm min}$) was presented obviously. Compared to the microwave absorption properties of Y$_{2}$Fe$_{17}$N$_{3-\delta }$/PU absorber, Y$_{2}$Fe$_{17}$N$_{3-\delta }$@SiO$_{2}$/PU absorbers are more conducive to the realization of microwave absorption material standards which are thin thickness, light weight, strong absorbing intensity, and broad bandwidth. Based on microwave frequency bands, the microwave absorption properties of the absorbers were analyzed and the related parameters were listed. As an important parameter related to perfect matching, reflection factor ($\sqrt {ărepsilon_{\rm r}/\mu_{\rm r}}$) was discussed combined with microwave amplitude attenuation. According to the origin and mathematical model of bandwidth, the formula of EAB (${\rm RL}<-10$ dB) was derived and simplified. The calculated bandwidths agreed well with experimental results.     

Microwave reflection properties of planar anisotropy FesoNi50 powder/paraffin composites

The reflection properties of planar anisotropy Fe50Ni50 powder/paraffin composites have been studied in the microwave frequency range.The permeability of Fe50Ni50 powder/paraffin composites is greatly enhanced by introducing the planar anisotropy,and can be further enhanced by using a rotational orientation method.The complex permeability can be considered as the superposition of two types of magnetic resonance.The resonance peak at high frequency is attributed to the natural resonance,while the peak at low frequency is attributed to the domain-wall resonance.The simulated results of the microwave reflectivity show that the matching thickness,peak frequency,permeability,and permittivity are closely related to the quarter wavelength matching condition.The Fe50Ni50 powder/paraffin composites can be attractive candidates for thinner microwave absorbers in the L-band(1-2 GHz).     

离子色谱-电感耦合等离子体质谱联用测定不同形态碘元素

用离子色谱（IC）和电感耦合等离子体质谱（ICP—MS）联用测定了IO3^-和I^-．使用DIONEX IonPacAS14分离柱（4mm×250mm,9．0μm）和IonPacAG14保护柱（4mm×50mm,9．0μm）,通过改变淋洗液种类、浓度、pH值和流速等,确定了碘形态分析的最佳条件,并在此条件下进行了方法的线性范围、最低检出限和重现性的测试．用快速溶剂萃取和超声波两种方法处理海带样品,用浓度30mmol·L^-1的Na2S2O3作为淋洗液检测了海带中的IO3^-和I^-,在同样条件下测试了海水样品．实验证明该方法快速、灵敏度高、干扰小．     

变速恒频双馈风力发电系统的励磁电源

给出了变速恒频双馈风力发电系统中交流励磁电源的控制方案.在基于电网电压定向的基础上,分别对转子侧变换器和网侧变换器进行了研究.分析了双馈电机数学模型,并对空载并网控制策略进行了设计,实现了系统在变风速条件下无冲击电流并网.采用直接电流控制对网侧变换器进行控制,并实现了能量双向流动,功率因数可调,使双馈风力发电系统能运行在次同步和超同步两种状态下.实验结果证实了理论分析的正确性和控制策略的有效性.     

Src激酶抑制剂FB2抗前列腺癌作用研究

探讨Src激酶抑制剂FB2抗前列腺癌的作用及机制.整体动物实验观察FB2对人前列腺癌PC-3细胞在裸鼠异体中生长的影响;MMT、克隆原形成、细胞黏附试验观察FB2对肿瘤细胞增殖、黏附的影响;流式细胞术分析FB2对细胞周期的影响;Western blot观察细胞及组织内Src及p-Src表达.实验结果表明FB2抑制PC-3细胞裸鼠移植瘤的生长;FB2抑制PC-3细胞增殖及对基底膜成分的黏附,并将细胞周期阻滞于G1期;机制研究表明,FB2抑制PC-3细胞及瘤组织中Src激酶Tyr416磷酸化.因此Src激酶抑制剂FB2在体内外均有较强的抗前列腺癌作用,其机制可能与抑制Src激酶Tyr416磷酸化有关.     

γ′-Fe3SnN的制备与穆斯堡尔谱研究

热处理（Ｆｅ０．７５Ｓｎ０．２５）Ｃ２Ｏ４．ｎＨＯ可制得单相氮化物γ′－Ｆｅ３ＳｎＮ,其中氮化前的氧化过程,热处理温度和Ｈ２／ＮＨ３气流比是影响产物的３个关键因素。此氮化物的晶格参数为ａ＝０．３８３７１（５）ｎｍ;室温下＾５７Ｆｅ穆堡尔谱为顺磁双峰,低温下谱中显示出铁磁相。     

First-principles study on magnetism of different dimensional Ru systems

The magnetism, the magnetocrystalline anisotropy and the optical properties of the monolayer and atomic chain of 4d transition-metal Ru are investigated by using the full-potential linearized-augmented-plane-wave method in a generalized gradient approximation. The magnetic moments are 1.039~μ __B/atom and 1.130~μ_B/atom for the monolayer and atomic chain, respectively. Both systems have large magnetocrystalline anisotropy energy (MAE). The magnetic easy axis is normal to the monolayer and perpendicular to the chain axis in the atomic chain. The optical properties of the two low-dimensional Ru systems are investigated by calculating the complex optical conductivity tensor. Both systems exhibit anisotropy in photoconductivity, especially for the atomic chain. The physical origins of MAE and photoconductivity are studied based on electronic structures. It is found that the changes in crystal field caused by different symmetry-breaking mechanisms in the two low-dimensional Ru systems result in MAE through spin--orbit coupling, while the anisotropy in photoconductivity mainly comes from the crystallographic anisotropy.     

一种新型光伏独立发电系统拓扑及控制策略

提出一种采用推挽输出的新型光伏独立发电主电路拓扑结构,系统由光伏电池阵列、充电器、蓄电池和逆变器组成.该逆变器能同时实现升压和逆变,省去了蓄电池之后的DC-DC升压部分.在简化主电路拓扑的同时,能够有效输出稳定的220 V交流电压.此外,该系统采用基于高频链SPWM调制方法及电压有效值外环、瞬时值内环的闭环控制策略.采用该系统不仅可以减小系统体积,降低系统成本,而且具有输出电压动态响应好、稳态精度高等优点.