用于中子发生器加速极电源的高频变压器设计

根据中子发生器加速极电源功率要求,通过AP(Area Product)法对加速极电源中的关键部件高频变压器进行设计.在推挽前级逆变电路中,增加去磁回路抑制变压器偏磁问题,采用分段分组绕制法减小分布电容.同时,测量和比较了不同频率下,变压器原、副边电压实验波形.结果表明:高频变压器的转换效率随频率升高而增大,当工作频率为20 kHz时,输出效率达到84％,满足了中子发生器加速极电源的要求.     

烟气中Hg的氧化机理的研究

本文对Ｈｇ与Ｃｌ２在烟气中的氧化反应进行了热力平衡计算和动力学计算。平衡计算的结果表明有ＣＩ元索存在时Ｈｇ的氧化率为１００％，而在相同的条件下动力学计算纺果为Ｈｇ的氧化率在２０％～８０％之间变化，与实验结果吻合。实际的氧化反应是一种超平衡状态，不能达到理想的平衡状态。因此应采用动力学与热力平衡分析相结合的方法研究Ｈｇ在烟气中的反应机理。同时，计算结果显示Ｃｌ含量对Ｈｇ的氧化率的影响很大．     

Clifford分析中无界域上正则函数的边值问题

在引入修正Cauchy核的基础上,讨论了无界域上正则函数的带共轭值的边值问题：a(t)Φ (t) b(t)Φ (t) c(t)Φ-(t) d(t)Φ=g(t)．首先给出了无界域上正则函数的Plemelj公式,然后利用积分方程方法和压缩不动点原理证明了问题解的存在唯一性．     

D. Liu and X. Zhu,Erratum to: “Fractional chromatic number and circular chromatic number for distance graphs with large clique size”. Journal of Graph Theory47(2) 2004, 129–146

The original article to which this Erratum refers was published in Journal of Graph Theory 47:129–146,2004 .     

Direct Observation of Non-covalent Complexes for Phosphorylated Flavonoid-protein Interaction by ESI

Diethyl flavon-7-yl phosphate was synthesized by modified Atheron-Todd reaction. The result of ESI shows that the phosphated flavonoids possess stronger binding affinities toward proteins such as myoglobin, insulin and lysozyme and are easier to form the non-covalent complexes with them.     

防紫外线伞ATR-OMNI采样器的FTIR分析

本实验使用OMNI采样器，直接对伞面内外进行单反射ATR的分析，快速、简便、不破坏样品，得到分辨率很好的红外图谱，再配合红外谱库的谱图检索，可以分别得到匹配率95％以上的尼龙－6和聚酯型聚氨酯的分析结果。     

Conformational characteristics of polycaproamide in dimethylacetamide containing lithium chloride

The viscosity behavior, index of refraction, and density of dilute polycaproamide solutions in DMAc containing lithium chloride have been studied. On the basis of temperature dependences of the index of refraction and the density of solutions, the θ-condition of polycaproamide solutions in DMAc containing 2.5% lithium chloride is estimated as 21.3°C. From intrinsic viscosity [η] measurements, the coefficients of swelling of a polymer coil, the mean-square distance between chain ends, and other parameters of macromolecules in solution are calculated.     

改革实验课教学方式提高实验课水平

通过对以教师为中心及以学生为中心的两种实验课教学方式的对比，探讨其对学生的科学文化素质、实践能力素质、身心素质培养的作用。     

Photoluminescence characteristics of ZnTiO3: Bi nanocrystals

The photoluminescence properties of the Bi³⁺ in sol-gel derived ZnTiO₃ nanocrystals have been investigated. An ultra-violet emission at 360 nm and a visible emission band at 506 nm have been observed, originating from two kinds of emission centers. The former is ascribed to the ³P₁-¹S₀ transition of Bi³⁺ and the latter to the recombination of the electrons with the photo-generated holes trapped in the zinc vacancies. In all cases the latter contribution is predominant.     

An Improved Synthesis of Retinoic Acid from β-Ionone

A convenient and large-scale preparation of retinoic acid 1 from β-ionone in five steps with 38% overall yield is described.The key steps are the epoxidization of 2 with a new methylated agent and the condensation 4 with tetraethyl methylenediphophonate in one-pot procedure to prepare 6.