巯基乙酸锑配合物的合成与X射线粉末衍射数据指标化

一些锑和铋的配合物可以应用于医药研究[1,2 ] ,已合成了许多锑的有机配体配合物[3～ 7] ,但其中大多数没有生物活性。因此 ,研究锑或铋离子的配合物不仅对主族元素化学、生物无机化学而且对医药都有着非常重要的意义。我们用三氯化锑与巯基乙酸液相反应法合成的二巯基乙酸锑 (Ⅲ)配合物 ,其组成为ＨＳｂ(ＳＣＨ2 ＣＯＯ) 2 ,用Ｘ射线粉末多晶衍射数据指标化来研究配合物晶体结构[8] 。1　实验部分1 1　仪器与试剂ＥＡ - 1 1 0 6型元素分析仪 (意大利卡拉欧巴公司制造 ) ,Ｄ Ｍａｘ -ＹＢ型多晶Ｘ射线粉末衍射仪(日本理学 ,ＣｕＫα射线 ,…     

一种结合知识挖掘的进化规划算法

进化规划是一种进化计算方法。进化规划主要使用随机化技术来实现优化过程。与其它进化算法相比,进化规划只有变异操作,而没有交叉操作,因此变异操作的有效性对进化规划算法的成功至关重要。在传统进化规划算法中,进化规划的变异操作具有完全的随机性,这虽然有利于避免局部极值,但却导致较大的计算量。在本文算法中,将知识挖掘技术引入进化规划之中。知识挖掘技术主要用于发现规则,然后利用发现的规则指导变异操作过程,提高变异操作的效率。最终加快了进化规划算法的速度,而计算效果没有明显下降。通过知识挖掘技术的引入,进化规划算法有了初步的智能特性。将本文所介绍的新算法应用于视频编码的运动估计实验中,结果表明新算法有良好的计算速度和计算精确性。     

On real-time databases: concurrency control and scheduling

In addition to maintaining database consistency as in conventional databases, real-time database systems must also handle transactions with timing constraints. While transaction response time and throughput are usually used to measure a conventional database system, the percentage of transactions satisfying the deadlines or a time-critical value function is often used to evaluate a real-time database system. Scheduling real-time transactions is far more complex than traditional real-time scheduling in the sense that (1) worst case execution times are typically hard to estimate, since not only CPU but also I/O requirement is involved; and (2) certain aspects of concurrency control may not integrate well with real-time scheduling. In this paper, we first develop a taxonomy of the underlying design space of concurrency control including the various techniques for achieving serializability and improving performance. This taxonomy provides us with a foundation for addressing the real-time issues. We then consider the integration of concurrency control with real-time requirements. The implications of using run policies to better utilize real-time scheduling in a database environment are examined. Finally, as timing constraints may be more important than data consistency in certain hard realtime database applications, we also discuss several approaches that explore the nonserializable semantics of real-time transactions to meet the hard deadlines     

IC卡在电信领域的应用模式

本文列举了ＩＣ卡在电信领域及一些国家和地区的应用之后，给出了国际ＩＣ卡的应用发展模式，以供有关部门参考。     

新型可调剪切差平行分束偏光器设计

本文给出了一种新型可调的切差平行分束偏光器设计。它调节方便,可获得较大平行分束剪切差,并可一镜多用     

基于矩的异分辨率图象边界检测

（１）本文引入仿射变换，提出了一种用矩算子以民分辨率图象直接进行边界检测的方法，利用同分辨率图象正方形窗口的模板行矩的计算，推导出了相应用的边界参数公式。（２）本文提出一种隐线笥插值矩计算方法，得到一组与正方形窗口对应的正方形模板，避免了费时的预插值过程，（３）对本文提出的方法进行了实验验证，并给出了实验结果。     

奇点理论浅引

本文是奇点理论的非正式的介绍。主要内容包括奇点分类与奇点拓扑的基本问题与结果。特别突出了简单奇点的券的性质及其与Ｌｉｅ代数的关系。本文的目的在于引起读者对一分支的兴趣。     

Patterned uniformly orientated silicon nanocrystallite films and efficient field emission characteristics

Patterned uniformly (100)-orientated silicon nanocrystallite (SiNC) films were fabricated based on hydrogen ion implantation technique and typical electrochemical anodic etching method. The surface morphology and microstructure characteristics of the films were characterized by scanning electron microscopy, transmission electron microscopy, X-ray diffraction, and atomic force microscopy. The efficient field emission with low turn-on field of about 3.2 V/μm at current density of 0.1 μA/cm² was obtained. The emission current density from the SiNC films reached 1 mA/cm² under a bias field of about 11 V/μm. The experimental results demonstrate that the SiNC films have great potential applications for flat panel displays.