Determination of gold in ore by flame atomic absorption spectrometry with flow-injection on-line sorbent extraction preconcentration

Gold in ores was determined by flame atomic absorption spectrometry following on-line preconcentration by sorbent extraction in a flow-injection system. The medium polarity adsorption resin Amberlite XAD-8 packed in a 220-μl micro-column was used to collect gold(III) from hydrochloric acid sample solutions for 40 s at 7.6 ml/min. Ethanol was used to elute the adsorbed analytes into the nebulizer. Optimization studies were made on sample loading rate, elution rate and sample acidity. Some possible interferences on the determination are discussed. A 35-fold enrichment was achieved at a sampling frequency of 60 h^?1 and with an RSD of 1.4%. The detection limit (3σ) and 2 μg l^?1. Results for gold in ore samples showed good agreement with those obtained using activated carbon adsorption preconcentration. The recoveries were 97–108%.     

电控发动机喷油脉宽的分析

本文介绍了利用喷油脉宽大小的变化来分析电控发动机电控系统、燃油供给等系统故障的一种方法,在汽车故障检测与诊断中有着广泛的应用。     

Features of the total disintegration events of heavyemulsion targets caused by 4.5A GeV/c16O

Total disintegration events produced by 4.5\,A GeV/c $^{16}$O--AgBr interactions are analysed to investigate the characteristics of secondary charged particles produced in such collisions. The multiplicity distributions of grey, black, and relativistic charged particles can be well represented by Gaussian distribution. The average multiplicity of grey particles is found to increase with the mass of projectile increasing, while that of black particles is found to decrease with the mass of projectile increasing. This result is in good agreement with the prediction of fireball model. Finally, the linear dependence between grey and black particles is observed, but there is no distinct dependence between the production of relativistic charged particles and the target excitation.     

含有五边形—七边形缺陷的单壁纳米碳管的输运性质研究

运用第一性原理的密度泛函理论结合非平衡格林函数研究了含有五边形—七边形拓扑缺陷的纳米碳管异质结的输运性质.结果发现：拓扑缺陷对碳管的输运性质有很大影响；另外，不同类型的碳管形成的异质结的输运性质也有明显的差异. 关键词： 纳米碳管 输运性质 异质结 透射系数     

火工品可靠性试验数据的综合分析方法

升降法试验数据和固定刺激量下的成败型试验数据,是两种最常见的火工品可靠性试验数据．我们应用Markov链,研究了升降法试验数据下,感度分布参数的极大似然估计的特性．在此基础上,应用Bootstrap方法和Bayes方法,给出了综合分析两种试验数据的方法．最后,将该方法应用于520底火的可靠性鉴定,得出了有益的结论．     

绝缘层上半导体多晶膜激光再结晶临界条件

从理论的角度分析了绝缘衬底对其上面半导体多晶膜激光熔化再结晶过程的影响, 发现低导热的绝缘层使产生固一液相变的临界激光功率有明显的降低.用喇曼光谱测量了激光再结晶SOI层中的应力. 应力的出现是多晶膜内曾经发生过固一液相的佐证.从这一思想出发, 对LPCVD方法制备的大量SOI 样品进行激光再结晶临界条件的研究, 证明了忽略绝缘层低热导影响的模型不能解释实验结果, 而经过修正的公式则可以较好地拟合实验结果, 关键词：     

线性规划问题的一种新的摄动法

在用单纯形方法解线性规划的问题时，不可避免会出现退化情况，而某些退化情况会导致循环。目前采用的避免循环的方法一共有两类：传统的摄动法（字典序）和Bland方法。本分析了传统摄动法的一些不足，给出了一种新的摄动法。     

APDT-00三极放电管全自动打印机的研制

介绍了新近研制的APTD - 0 0三极放电管全自动打印机的结构特点及整机设计的关键技术 ,阐述了自动上料机构、打印机构和控制电路的设计     

光子晶体中四能级系统的量子相干效应

研究了处于光子带隙材料中的四能级原子系统的电磁感应透明、自发辐射和光子开关效应，分析了其稳态与瞬态特性, 发现特殊的模密度能够导致反常的吸收、色散、自发辐射及瞬态无反转增益, 并可以通过外加调制场进行控制.详细讨论了特殊频率处模密度的变化对透明窗口和光子开关效应的影响. 关键词： 光子带隙材料 电磁感应透明 模密度 光子开关     

有Edgeworth展式的分布的随机加权逼近的重对数律

本文研究了未知分布的逼近问题，利用随机加权法，给出了有Edgeworth展式的一类（未知）分布的模拟分布，证明了在一定条件下，模拟分布与未知分布的逼近精度达到O(n^-1√lnlnn），称之为随机加权逼近的重对数律。