Chlorination of aromatic substrates catalyzed by the phthalocyanine complexes

The chlorination of benzene, toluene, and o-xylene with molecular chlorine in the presence of the phthalocyanine complexes of different structures was studied. The transformations of the catalysts during the reaction were investigated. Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, No. 8, pp. 1644–1647, August, 2008.     

4-Functionally-substituted 3-heterylpyrazoles: XIX. 3-aryl-4-(5-isoxazolyl)pyrazoles

Oximes of 4-(4-pyrazolyl)-3-buten-2-onees obtained by successive reaction of 3-aryl-4-formylpyrazoles with acetone and hydroxylamine at the treatment with iodine suffered an oxidative cyclization yielding 3-aryl-4-(5-isoxazolyl)pyrazoles.     

FIR的FPGA实现及其QuartusⅡ与MATLAB仿真

利用Altera公司的Stratix系列芯片内部的ROM实现了一种基于查找表结构的有限冲击响应(FIR)数字滤波器,从而将卷积运算变换成一种查表后的加法运算,提高了运算速度,节省了逻辑单元;并且利用Altera公司的FPGA开发软件QuartusⅡ与MathWorks公司的MATLAB软件实现电子设计自动化(EDA)应用中的联合仿真,从而提高了现场可编程门阵列(FPGA)设计的效率,使得QuartusⅡ的波形仿真功能更加强大;利用最新版本的QuartusⅡ3.0还可以将波形文件转换成Testbench文件导入到专业仿真软件例如ModelSim中进行仿真.     

关于本地传输网网络优化的探讨

根据长期工作经验,对现有网络存在的问题进行分析,提出对本地传输网网络优化的有关建议。     

Analysis and Simulation of S-shaped Waveguide in Silicon-on-insulator

The simulation and analysis of S-shaped waveguide bend are presented.Bend radius larger than 30 mm assures less than 0.5 dB radiation loss for a 4-μm-wide silicon-on-insulator waveguide bend with 2-μm etch depth.Intersection angle greater than 20° provides negligible crosstalk (<-30 dB) and very low insertion loss.Any reduction in bend radius and intersection angle is at the cost of the degradation of characteristics of bent waveguide and intersecting waveguide, respectively.     

Anisotropic and isotropic phases of polymer melts

The melting mechanism of polymer crystals is proposed. It is assumed that the melting happens due to forming supervacancies. This mechanism leads the appearance of anisotropic phase of a melt. It is shown that two phases—anisotropic and isotropic—can exist in polymer melts.     

Low-frequency internal friction in complex composite strands

Conclusion A method was proposed which makes it possible to study the low-frequency internal friction of complex fibers. This method was used to study the internal friction of complex composite fibers based on PCA and PE. We observed a relaxation process which is typical of the composite and is absent in the pure materials.Translated from Mekhanika Kompozitnykh Materialov, No. 1, pp. 11–15, January–February, 1989.     

激光晶体YAG中Er3+的辐射跃迁

本文讨论和分析了激光晶体YAG中Er3+离子的激光上能级的4S3/2、4I11/2和4I13/2辐射跃迁的有关因素。