纳米技术的研究现状与将来

纳米科学技术将成为２１世纪最重要的高技术之一。纳米技术的最终目标是直接操纵单个原子和分子，制造量子功能器件，从而开拓人类崭新的生产生活模式。文章评述利用电子束、离子束的精细技术和ＳＴＭ原子操纵技术的研究现状，介绍原子层蚀刻，单层抗蚀剂自形成蚀刻，纳米自然蚀刻和电子束全息纳米蚀刻等高技术前沿动态，展望纳米技术的发展前景。     

Al—Si—Mn—Fe合金中相组成的电子衍射鉴定

本文利用选区电子衍射,并结合X射线衍射对六种不同成份的急冷合金及其退火后的相组成进行了鉴定,得到了它们的相组成。     

双线性系统的无反馈解耦线性化

用现代微分几何方法研究了双线性控制系统的解耦线性化问题，给出了一般双线性系统解耦线性化的充分条件及严格双线性系统解耦线性化的充要条件，并举例说明了本文的结论。     

Validation of fuzzy logic method for automated mass spectral classification for mineral imaging

Imaging mass spectrometry requires the acquisition and interpretation of hundreds to thousands of individual spectra in order to map the mineral phases within heterogeneous geomatrices. A fuzzy logic inference engine (FLIE) was developed to automate data interpretation. To evaluate the strengths and limitations of FLIE, the chemical images obtained using FLIE were compared with those developed using two chemometric methods: principle component analysis (PCA) and cluster analysis (K-Means). Two heterogeneous geomatrices, a low-grade chalcopyrite ore and basalt, were imaged using a laser-desorption Fourier transform mass spectrometer. Similar mineral distribution patterns in the chalcopyrite ore sample were obtained by the three data analysis methods with most of the differences occurring at the interfaces between mineral phases. PCA missed one minor mineral phase in the chalcopyrite ore sample and did not clearly differentiate among the mineral classes of the basalt. K-Means cluster analysis differentiated among the various mineral phases in both samples, but improperly grouped some spectra in the chalcopyrite sample that only contained unanticipated high mass peaks. Unlike the chemometric methods, FLIE was able to classify spectra as unknowns for those spectra that fell below the confidence level threshold. A nearest neighbor approach, included in FLIE, was used to classify the unknowns to form a visually complete image; however, the unknowns identified by FLIE can be informative because they highlight potential problems or overlooked results. In conclusion, this study validated the fuzzy logic-based approach used in our laboratory and reveald some limitations in the three techniques that were evaluated.     

四（对-羟基苯基）卟啉氧合配合物的室温固相合成，表征及氧合能力

采用固相反应合成了四羟基苯基卟啉与与Fe^2＋,Co^2＋金属离子的配合物,在室温下,将其与分子O2作用,提纯后得到两种固态氧合配合物．通过元素分析、红外光谱（IR）、核磁共振氢谱（^1HNMR）、电导、热分析（TG／DTA）、紫外光谱（UV）等测试手段确定了氧合配合物的组成为[Co·THPP·O2]（NO3）2·2H2O、[Fe·THPP·O2]Cl2·2H2O]，可知1mol配合物吸收了1molO2,采用失重法测定了氧合配合物中的配位氧,确定1mol金属配合物吸收1molO2形成超氧配合物．     

中压变频器在宣钢炼钢厂除尘风机中的应用

本文介绍了SIMOVERT MV中压变频器在宣钢炼钢厂一次除尘风机中的应用情况。变频器现场运行表明，采用中压变频器对转炉除尘风机进行调速节能获得了成功，节能效果明显。     

球栅阵列倒装焊封装中的热应变值的测试

利用高温云纹实验方法测试球栅阵列(BGA)封装焊点的热应变,采用硅橡胶试件光栅复制技术,使测试环境温度提高到200℃.通过实时热应变测量,得到各焊点的热应变关系以及封装材料、电路板各部分的热应变分布状况,为研究集成电路封装组件焊点的建模和热疲劳破坏机理提供了可靠的实验依据.     

存储媒体的媒体内同步反馈控制算法

本文提出了一种存储媒体的媒体内同步反馈控制算法，该方案是建立在缓冲区占用率控制基础上，通过周期性地检查缓冲区的占用情况来检测失步，并将其反馈给发送方，由发送方对发送帧速率进行调整。文章给出了接收方所需缓冲区的设计准则及发送帧速率的调整方法，并分析了算法中各参数对同步性能的影响。实验表明该方案能够处理由于网络传输时延特性变化引起的失步，与其它反馈控制方案相比具有更低的数据丢弃率，从而使接收端播放平滑连续，具有良好的视频播放质量。     

毛细管电色谱中进样时间对柱效的影响

毛细管电色谱是近年发展起来的一种新型微分离技术，它结合了高效液相色谱和毛细管电泳的物点，具有高效、快速，高选择性，其有关理论研究和应用越来越深入，本文从色谱动力学角度讨论了毛细管电色谱中进样时间对柱的影响。