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41.
Yu‐Hsiang Hu Chuh‐Yung Chen Chen‐Chien Wang Yao‐Hui Huang Shao‐Ping Wang 《Journal of polymer science. Part A, Polymer chemistry》2004,42(19):4976-4993
The bulk polymerization of styrene initiated by ?‐caprolactam (CL) and n‐dodecyl mercaptan (RSH) has been explored. This novel polymerization system shows living characteristics. For example, the molecular weight of the resulting polymers increases with conversion, and the system has the ability to form diblock copolymers and so forth. The polymer chain end contains thiol and lactam structures, which we have investigated with Fourier transform infrared, 1H NMR, and 13C NMR techniques. Electron spin resonance spectra and theoretical calculations by the Hartree–Fock methods have been used to examine the mechanism. The results reveal that the initial polymerization starts from thiol via a chain‐transfer reaction, and the propagation proceeds by the insertion of a monomer between the terminal group and the intermediate structure of lactam. Finally, the polymerization kinetics have been examined. The polymerization rate varies linearly with the concentration of CL and RSH, and this confirms the mechanism. © 2004 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 42: 4976–4993, 2004 相似文献
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Yao Ping HOU 《数学学报(英文版)》2005,21(4):955-960
A signed graph is a graph with a sign attached to each edge. This paper extends some fundamental concepts of the Laplacian matrices from graphs to signed graphs. In particular, the relationships between the least Laplacian eigenvalue and the unbalancedness of a signed graph are investigated. 相似文献
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本文提出了孙子定理的微分方程求解法,讨论了系数为求余算子的非线性微分方程的稳定平衡点和最佳解的误差。本文构造的非线性微分方程可以唯一地收敛于孙子定理的解,其误差可任意小。该微分方程可用人工神经网络实时计算,实现余/十转换。计算机模拟结果证实了本文理论的正确性。 相似文献
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钛酸铅系薄膜的热释电性能及其应用 总被引:10,自引:1,他引:9
叙述了钛酸铅系薄膜的热释电原理,介绍了国际上近几年钛酸铅系薄膜材料、制备工艺及热释电性能,并与块状陶瓷材料进行了比较,分析表明钛酸铅系薄膜具有优良的热释电性能及可观的应用前景。 相似文献
49.
J.S. Tsay H.W. Chang Y.L. Chiou K.T. Huang W.Y. Chan Y.D. Yao 《Journal of magnetism and magnetic materials》2006
Influences of oxygen exposure on the magnetic properties of Co/Ge(1 1 1) ultrathin films have been investigated by surface magneto-optic Kerr effect technique. As the oxygen exposure increases on Co/Ge(1 1 1) films, their magnetic properties could be modified. As an example for 15 ML Co/Ge(1 1 1) films, the coercivity increases from 730 to 920 Oe and the remanence Kerr intensity is reduced for 500 Langmuir (L) of oxygen exposure. Corresponding compositions analyzed by Auger electron spectroscopy measurement shows that the amount of oxygen on the surface layers increases with increasing the oxygen exposure time. Oxygen distributes on the topmost layers of the film. The adsorbed oxygen influences the electronic density of states of Co and results in the changes of the magnetic properties. Besides, the appearance of O/Co/Ge interface could modify the stress anisotropy, and as a result the coercivity of ultrathin Co/Ge(1 1 1) film is enhanced. 相似文献
50.
For vertical-cavity surface-emitting lasers (VCSELs) with polarization-rotated feedback, there exist several synchronization
types such as synchronizations between total powers and synchronizations between separate polarization modes. Based on the
two-mode rate equations, we study and compare numerically the performances of different synchronization types. Our results
show that three synchronization types exhibit good performances when their synchronization conditions are satisfied. They
are the complete synchronization between total powers, complete synchronization between x-polarized modes, and generalized synchronization between x-polarized and y-polarized modes. The former two types are sensitive to the injection rate and spontaneous emission, while the third type
is contrary. Synchronization type with the best performance may switch from one to another, with changing of injection rate
and spontaneous emission factor. 相似文献