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Chin‐Ping Yang Ruei‐Shin Chen Kuei‐Hung Chen 《Journal of polymer science. Part A, Polymer chemistry》2003,41(7):922-938
To investigate the position and amount of the CF3 group affecting the coloration of polyimides (PIs), we prepared 2,2‐bis[4‐(4‐amino‐2‐trifluoromethylphenoxy)phenyl]hexafluoropropane ( 2 ) with four CF3 groups with 2‐chloro‐5‐nitrobenzotrifluoride and 2,2‐bis(4‐hydroxyphenol)hexafluoropropane. A series of soluble and light‐colored fluorinated PIs ( 5 ) were synthesized from 2 and various aromatic dianhydrides ( 3a – 3f ). 5a – 5f had inherent viscosities ranging from 0.80 to 1.19 dL/g and were soluble in amide polar solvents and even in less polar solvents. The glass‐transition temperatures of 5 were 221–265 °C, and the 10% weight‐loss temperatures were above 493 °C. Their films had cutoff wavelengths between 343 and 390 nm, b* values (a yellowness index) ranging from 5 to 41, dielectric constants of 2.68–3.01 (1 MHz), and moisture absorptions of 0.03–0.29 wt %. In a comparison of the PI series 6 – 8 based on 2,2‐bis[4‐(4‐aminophenoxy)phenyl]hexafluoropropane, 2,2‐bis[4‐(4‐amino‐2‐trifluoromethylphenoxy)phenyl]propane, and 2,2‐bis[4‐(4‐aminophenoxy)phenyl]propane, we found that the CF3 group close to the imide group was more effective in lowering the color; this means that CF3 of 5 , 7 , and 8f was more effective than that of 6c . The color intensity of the four PI series was lowered in the following order: 5 > 7 > 6 > 8 . The PI 5f , synthesized from diamine 2 and 4,4′‐hexafluoroisopropylidenediphthalic anhydride, had six CF3 groups in a repeated segment, so it exhibited the lightest color among the four series. © 2003 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 41: 922–938, 2003 相似文献
185.
双金属催化剂是一类重要的多相催化剂。其中d电子在催化活性方面起着重要的作用.本文在Co_3[Fe(CN)_6]_2的工作基础上,进一步研究了该配合物在硅胶、氧化铝、以及氧化镁上的热性质,同时考察了CN~-在Co-Fe体系双端基配位的活化加氢,探讨了载体的影响. 相似文献
186.
Z.J. Yang T.H. Johansen H. Bratsberg G. Helgesen A.T. Skjeltorp 《Physica C: Superconductivity and its Applications》1989,160(5-6):461-465
Based on a dipole-dipole interaction model, we discuss the levitation force and related vibration problems to understand the effects of flux pinning in type-II superconductors, and the applications of levitation in superconducting systems. 相似文献
187.
This paper concerns CDMA cellular networks equipped with conventional matched filter receivers. For this type of cellular networks, two problems exist. One is the inverse relationship between the coverage and capacity, and the other one is the near-far unfair access problem. To resolve these two problems, a bandwidth-space partitioning technique is adopted. Several admission control schemes based on the bandwidth-space partitioning technique are proposed, and their performances are evaluated based on the simulation.Shih-Tsung Yang received his B.S. (1989) and M.S. (1991) degrees in electrical engineering from the National Taiwan University, and Ph.D. (1999) degree in electrical and computer engineering from University of Maryland, College Park.From 1999 to 2000, he was with SBC Technology Resourtces, Inc. where he was involved in the network architecture design for the ATM based networks. From November 2000 to May 2003, he was with Transilica/Microtune where he was involved in the design of Baseband and RF for the wireless communications. Since May 2003, Dr. Yang is now with Genesys Logic, Inc. where he is responsible for the baseband design of the WLAN and Ethernet.Dr. Yang’s research interests are in the area of Digital Communications, Communication networks and signal processing. E-mail: thomas.yang@genesyslogic.com.twAnthony Ephremides received his B.S. degree from the National Technical University of Athens (1967), and M.S. (1969) and Ph.D. (1971) degrees from Princeton University, all in Electrical Engineering. He has been at the University of Maryland since 1971, and currently holds a joint appointment as Professor in the Electrical Engineering Department and in the Institute of Systems Research (ISR) of which he is a founding member. He is co-founder of the NASA Center for Commercial Development of Space on Hybrid and Satellite Communications Networks established in 1991 at Maryland as an off-shoot of the ISR. He served as Co-Director of that Center from 1991 to 1994.He was a Visiting Professor in 1978 at the National Technical University in Athenas, Greece, and in 1979 at the EECS Department of the University of California, Berkeley, and at INRIA, France. During 1985-1986 he was on leave at MIT and ETH in Zurich, Switzerland. He was the General Chairman of the 1986 IEEE Conference on Decision and Control in Athens, Greece and of the 1991 IEEE International Symposium on Information Theory in Budapest, Hungary. He also organized two workshops on Information theory in 1984 (Hot Springs, VA) and in 1999 (Metsovo, Greece). He was the Technical Program Co-Chair of the IEEE INFOCOM in New York City in 1999 and of the IEEE International Symposium on Information theory in Sorrento, Italy in 2000. He has also been the Director of the Fairchild Scholars and Doctoral Fellows Program, an academic and research partnership program in Satellite Communications between Fairchild Industries and the University of Maryland. He won the IEEE Donald E. Fink Prize Paper Award (1992) and he was the first recipient of the Sigmobile Award of the ACM (Association of Computer Machinery) for contributions to wireless communications in 1997. He has been the President of the Information Theory Society of the IEEE (1987) and has served on its Board of Governors almost continuously from 1981 until the present. He was elected to the Board of Directors of the IEEE in 1989 and 1990. Dr. Ephremides has authored or co-authored over 100 technical journal papers and 300 technical conference presentations. He has also contributed chapters to several books and edited numerous special issues of scientific journals. He has also won awards from the Maryland Office of Technology Liaison for the commercialization of products and ideas stemming from his research. He has served on the Editorial Boards of the IEEE Transactions on Automatic Control, IEEE Transactions on Information theory, the Journal of Wireless Networks, and the International Journal of Satellite Communications.He has been the Dissertation Supervisor of over twenty Ph.D. students who now hold prominent positions in academia, industry, and research labs. He is the founder and President of Pontos, Inc., a Maryland company that provides technical consulting services, since 1980.Dr. Ephremides’ interests are in the areas of communication theory, communication systems and networks, queueing systems, signal processing, and satellite communications. His research has been continuously supported since 1971 by NSF, NASA, ONR, ARL, NRL, NSA, and Industry. E-mail: tony@eng.umd.edu 相似文献
188.
J.J. Pan Xiangdong Qiu Kejian Guan Liang Dong FengQing Zhou Wei Wang Mingjie Zhang James Guo Jun Yang Chunmeng Wu 《光学学报》2003,23(Z1)
A low cost, coolerless 980nm diode pumped, gain flattened L band EDFA with fast transient control, high pump efficiency and gain clamping effect was realized by using FBGs as C band seed generators. 相似文献
189.
Previous studies of the initial stage of oxidation on clean single crystal of Cu(1 0 0) have been extended to the case of the Cu(1 1 0) surface. The dynamic observation of the nucleation and growth of Cu oxide by means of in situ ultra high vacuum transmission electron microscopy (UHV-TEM) shows a highly enhanced oxidation rate on Cu(1 1 0) surface as compared to Cu(1 0 0). The kinetic data on the nucleation and growth of the three-dimensional oxide islands agree well with our heteroepitaxial model of surface diffusion of oxygen. 相似文献
190.