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971.
流动系统中鲁米诺电生化学发光(ECL)系统研究初探 总被引:1,自引:0,他引:1
本文描述了一个新的鲁米诺电生化学发光流动系统.通过微铂电极流动池,H2O2被还原为OH-以维持鲁米诺化学发光所要求的pH条件.本文对鲁米诺化学发光机理进行了初步探讨,并详细研究了ECL的最佳条件,该系统明显降低了反应噪声,优于混合反应系统,可作为液相色谱间接测定检测器. 相似文献
972.
HL-1装置中LHCD和等离子体参数的关系 总被引:1,自引:1,他引:0
本文研究了在HL-1托卡马克的不同放电阶段的低混杂波驱动特性。给出了驱动电流及驱动效率和等离子体参数,如电子平均密度ne、等离子体电流Ip及纵向磁场的关系。也给出和分析了波驱动和入射波功率的关系。在放电平段,对正反向驱动效率进行了研究和比较。 相似文献
973.
An experimental study for the pathologic changes of the canine tracheal mucosa under YAG:Nd laser ablation was performed in order to master the appropriate parameters for the clinical treatment of YAG:Nd laser. 6 male and female Mongolia dogs weighing 13-18 kg were received 20W YAG:Nd laser treatment and their pathologic changes were examined instantly and 3, 7, 14 and 28 days after ablation. 相似文献
974.
57Fe Mössbauer effect study has been performed on intercalated compound 2H?Fe0.5TaSe2 over a temperature range between 14K and 500K. The highly concentrated intercalation samples 2H?FexTaSe2 with Fe atoms (x up to 2) are prepared by the electrochemical method for the first time. The Mössbauer measurement shows that iron is in Fe3+ high spin state and with the same probability occupies both octahedral and tetrahedral interstices of the Van der Waals gap. The fact that effective masses of iron ions in both sites are close to 57 amu and characteristic temperatures (ΘM =130K, 107K respectively) are found to be relatively small is attributed to the weak forces on Fe3+. 相似文献
975.
采用ππ偏振激光,通过两步激发和光电离方法,在0-154V/cm电场范围内,测定了Yb原子n-18附近m=0的斯塔克光谱,首次把包含斯塔克效应的能量矩阵对角化方法推广到Yb原子,所获得的理论斯塔克图与实验结果基本符合,观察到低场中斯塔克簇随电场增加呈现线性结构以及^1P1态与斯塔克簇在抗交叉过程中振子强度发生转移的现象,讨论了结构与量子亏损的关系。 相似文献
976.
随着内窥镜检查及胸部手术的广泛开展、气管切开后金属插管的较长期使用,气管支气管肉芽肿以及良恶性肿瘤等已为常见疾病。激光治疗气管、支气管疾病在临床上已证明有效,但激光对气道粘膜的作用究竟如何尚鲜见报道。本实验应用机械刺激原理,置异物于大道某一部位,造成持续性刺激而促使该部位生长出炎性肉芽肿,然后以YAG:Nd激光照射汽化之,观察治疗后局部大体及镜下病理变化,旨在为临床激光治疗气道内阻塞性病变提供理论参考。 相似文献
977.
The reduction of chromate by glutathione, its mono- and diethyl esters,
-cysteine, 2-mercapto-propionic acid and mercapto-succinic acid has been studied. The empirical rate law kobs = ab[Thiol]2/(1 + b[Thiol]) is obeyed by all of these thiols, at neutral pH. No evidence could be obtained for a first-order pathway in glutathione under these conditions. These observations are used to comment on the stability of intermediates potentially important in explaining chromate toxicity. 相似文献
978.
Main chain liquid crystal polymers are modelled as either worms or jointed rods. In reality they are composed of mesogenic units (rods) linked by spacers with varying degrees of flexibility. We present a molecular model to describe non-homogeneous nematic polymers. The model takes account of molecular parameters, such as the lengths of the mesogenic group and the spacer units, and the interactions between them. The spacers are found to have an order differing from the mesogenic units. If the spacer is not very long and thus in effect is inflexible, one end of the spacer can retain to some extent the orientation of the other end, allowing orientational correlation between spacers mediated by the intermediate mesogenic unit. This is important in giving the chain a global rod-like behaviour as the nematic field becomes strong or the temperature low. The nematic order of the two components (mesogens and spacers), the nematic-isotropic transition as well as the latent entropy are examined. Furthermore, the anisotropic conformations of the polymers are investigated, which show either rod-like or random walk behaviour. Comparison of our results with experiment is found to be satisfactory. 相似文献
979.
980.
The unity gain buffer will be good to design high frequency SCF if its resistiveeffects can be eliminated,and therefore the whole parasitic sensitivities will greatly be reduced.On the basis of this concept,a novel parasitic tolerant SC DTE(differential transconductanceelement)is proposed.SC floating inductor and integrator fit for high frequency applications areformed by the DTE.The computer simulation and experiment on a third order elliptic LP filterverify its validity. 相似文献