Al-Cu-Fe系初生准晶相凝固过程的电子显微分析

采用包括金相（OM），粉末X射线衍射（XRD），扫描电子显微镜（SEM）观察和透射电子显微（TEM）分析等方法，研究了铸态Al592.Cu36.8Fe3.0Si1.0合金（700℃保温2．5h后水淬）的显微组织及相组成。发现铸锭中存在4种相：准晶I相，τ3相（或φ相），θ－Al2Cu相和η－AlCu相，凝固过程可描述为：初生晶是准晶Ⅰ相；在保温过程中发生包晶或共晶反应（L＋i→τ3(或φ）或L→τ3（或φ）＋i)形成的τ3相（或φ相），呈微畴结构；而剩余液体水淬形成θ－Al2Cu相和η－AlCu 相。     

电视节目包装中的文字设计艺术

文字是电视节目包装中的重要元素之一,除了传达信息的基本功能外,经常起到决定整体效果的关键作用。节目包装文字设计应突出本台文化和本土文化,文字的设计必须与节目相匹配,形成统一整体。     

Pd-Ge contact to n-GaAs with the TiW diffusion barrier

Pd-Ge based ohmic contact to n-GaAs with a TiW diffusion barrier was investigated. Electrical analysis as well as Auger electron spectroscopy and the scanning electron microscopy were used to study the contact after it was subjected to different furnace and rapid thermal annealing and different aging steps. All analyses show that TiW can act as a good barrier metal for the Au/Ge/Pd/n-GaAs contact system. A value of 1.45 × 10⁻⁶ Ω-cm² for the specific contact resistance was obtained for the Au/TiW/Ge/Pd/n-GaAs contact after it was rapid thermally annealed at 425°C for 90 s. It can withstand a thermal aging at 350°C for 40 h with its ρ_c increasing to 2.94 × 10⁻⁶Ω-cm² and for an aging at 410°C for 40 h with its ρ_c increasing to 1.38 × 10⁻⁵ Ω-cm².     

Bayesian bounds for matched-field parameter estimation

Matched-field methods concern estimation of source locations and/or ocean environmental parameters by exploiting full wave modeling of acoustic waveguide propagation. Because of the nonlinear parameter-dependence of the signal field, the estimate is subject to ambiguities and the sidelobe contribution often dominates the estimation error below a threshold signal-to-noise ratio (SNR). To study the matched-field performance, three Bayesian lower bounds on mean-square error are developed: the Bayesian Crame/spl acute/r-Rao bound (BCRB), the Weiss-Weinstein bound (WWB), and the Ziv-Zakai bound (ZZB). Particularly, for a multiple-frequency, multiple-snapshot random signal model, a closed-form minimum probability of error associated with the likelihood ratio test is derived, which facilitates error analysis in a wide scope of applications. Analysis and example simulations demonstrate that 1) unlike the local CRB, the BCRB is not achieved by the maximum likelihood estimate (MLE) even at high SNR if the local performance is not uniform across the prior parameter space; 2) the ZZB gives the closest MLE performance prediction at most SNR levels of practical interest; 3) the ZZB can also be used to determine the necessary number of independent snapshots achieving the asymptotic performance of the MLE at a given SNR; 4) incoherent frequency averaging, which is a popular multitone processing approach, reduces the peak sidelobe error but may not improve the overall performance due to the increased ambiguity baseline; and finally, 5) effects of adding additional parameters (e.g., environmental uncertainty) can be well predicted from the parameter coupling.     

图像边缘检测在关节镜图像处理中的应用

主要论述了采用图像边缘检测和图像跟踪算法对采集的关节镜图像进行图像处理和分析的过程。在图像处理的基础上，系统自动测量出指定目标的形状参数，实现了系统的测量要求。本研究为实现关节镜手术过程图像的保存和手术的准确性提供了可行的方法。     

革新质量观念,打造制造业强国

最近美国内布拉斯加州林肯大学的MARC J.SCHNIEDERJANS等人对中国制造产品和外国制造产品进行了对比调查与分析,根据对500位美国消费者的调查数据分析,中国产品平均质量得分2.77(满分为10分),非中国产品平均质量得分7.22.这一结果显示中国产品在美国消费者心目中的质量形象很差,这对于希望成为世界制造业基地的中国来说应是一个值得警惕的信号.尽管2004年中国国际贸易额将突破万亿美元大关,但我们必须冷静思考:中国产品仅仅依靠低廉价格抢占国际市场的做法是否可以长期持续?外国对我国产品的反倾销制裁日益频繁、当地制造业的激烈抵制给我国企业敲响了警钟:市场竞争不仅仅是价格竞争,更重要的是质量竞争.那么,是什么制约了中国产品质量的提高?     

Preparation,thermal properties,and flame retardance of epoxy–silica hybrid resins

A novel epoxy system was developed through the in situ curing of bisphenol A type epoxy and 4,4′‐diaminodiphenylmethane with the sol–gel reaction of a phosphorus‐containing trimethoxysilane (DOPO–GPTMS), which was prepared from the reaction of 9,10‐dihydro‐9‐oxa‐10‐phosphaphenanthrene‐10‐oxide (DOPO) with 3‐glycidoxypropyltrimethoxysilane (GPTMS). The preparation of DOPO–GPTMS was confirmed with Fourier transform infrared, ¹H and ³¹P NMR, and elemental analysis. The resulting organic–inorganic hybrid epoxy resins exhibited a high glass‐transition temperature (167 °C), good thermal stability over 320 °C, and a high limited oxygen index of 28.5. The synergism of phosphorus and silicon on flame retardance was observed. Moreover, the kinetics of the thermal oxidative degradation of the hybrid epoxy resins were studied. © 2003 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 41: 2354–2367, 2003     

Synthesis and transition temperatures of liquid crystals incorporating a 1,4-tetrafluorophenylene unit

Two homologous series of mesogenic materials which incorporate a 1,4-tetrafluorophenylene moiety and a terminal cyano- or nitro-substituent have been synthesized by using palladiumcatalysed coupling procedures. The compounds exhibit nematic and/or smectic A phases.     

基于IPv6校园网的智能选课系统的J2EE架构的设计与实现

通过分析IPv6校园网自主学习模式下的自主选课问题,提出了利用J2EE技术构建基于IPv6校园网的智能选课系统的总体结构及具体实现.     

Syntheses,crystal structures and blue emission of three zinc(II) coordination polymers with a 4,4′‐dicarboxybiphenyl sulfone ligand

Three novel zinc complexes [Zn(dbsf)(H₂O)₂] ( 1 ), [Zn(dbsf)(2,2′‐bpy)(H₂O)]·(i‐C₃H₇OH) ( 2 ) and [Zn(dbsf)(DMF)] ( 3 ) (H₂dbsf = 4,4′‐dicarboxybiphenyl sulfone, 2,2′‐bpy = 2,2′‐bipyridine, i‐C₃H₇OH = iso‐propanol, DMF = N,N‐dimethylformamide) were first obtained and characterized by single crystal X‐ray crystallography. Although the results show that all the complexes 1–3 have one‐dimensional chains formed via coordination bonds, unique three‐dimensional supramolecular structures are formed due to different coordination modes and configuration of the dbsf^2? ligand, hydrogen bonds and π–π interactions. Iso‐propanol molecules are in open channels of 2 while larger empty channels are formed in 3 . As compared with emission band of the free H₂dbsf ligand, emission peaks of the complexes 1–3 are red‐shifted, and they show blue emission, which originates from enlarging conjugation upon coordination. Copyright © 2006 John Wiley & Sons, Ltd.