含1,2,4-三唑-5-硫酮席夫碱的新型1,2,4-三唑并[1,5-a]嘧啶衍生物的合成及生物活性研究

以2-苄硫基-5-甲基-7-羟基-1,2,4-三唑并[1,5-a]嘧啶为原料,经醚化、肼解、成盐、关环和席夫碱反应合成了20个新型的含1,2,4-三唑-5-硫酮席夫碱的1,2,4-三唑并[1,5-a]嘧啶类化合物,通过IR,1H NMR,MS和元素分析对所合成的化合物进行了结构表征.初步生物活性测试结果表明,部分化合物表现出一定的抑菌或较好的抗烟草花叶病毒(TMV)活性.在500μg/mL浓度下,化合物6b,6f和6p对TMV的抑制率分别为41%,43%和40%.     

Applications of the molecular orbital graph theory (XI)

The tree graph method of evaluating the local molecular moment is proposed. By applying this method and the molecular moment formula of π-electron energy in the molecular orbital graph theory, a topological method of using the molecular moment to judge the relatively reactive point of even AH is achieved.     

Electrochemiluminescence Behavior of Ru(bpy)32+/Carbofuran System on an Electrically Heated Microelectrode Chip

An electrically heated microelectrode chip (HMEC) was designed and the Ru(bpy)₃²⁺/carbofuran electrochemiluminescence (ECL) systems were applied to characterize the performance of the HMEC. The ECL intensities increase at elevated electrode temperature, and the detection limit at 60°C (electrode surface temperature) was about 10 times lower than that at 30°C. The results indicate that new heated electrode can be handled easily and can be mass produced, the difference between the electrodes was little. The stability of the HMEC was good since the electrode surface can hardly be destroyed during detection and storage.     

Representations of centrally-extended Lie algebras over differential operators and vertex algebras

We construct irreducible modules of centrally-extended classical Lie algebras over left ideals of the algebra of differential operators on the circle, through certain irreducible modules of centrally-extended classical Lie algebras of infinite matrices with finite number of nonzero entries. The structures of vertex algebras associated with the vacuum representations of these algebras are determined. Moreover, we prove that under certain conditions, the highest-weight irreducible modules of centrally-extended classical Lie algebras of infinite matrices with finite number of nonzero entries naturally give rise to the irreducible modules of the simple quotients of these vertex algebras. From vertex algebra and its representation point of view, our results with positive integral central charge are high-order differential operator analogues of the well-known WZW models in conformal field theory associated with affine Kac-Moody algebras. Indeed, when the left ideals are the algebra of differential operators, our Lie algebras do contain affine Kac-Moody algebras as subalgebras and our results restricted on them are exactly the representation contents in WZW models. Similar results with negative central charge are also obtained.     

动态冷原子吸收法快速测定地球化学样品中微量汞

本文介绍了动态冷原子吸收法快速测定地球化学样品中微量汞的方法。本文研究采用了新型的汞蒸气发生器，并对气泡的干扰进行了研究。线性范围为0.2-12ng/mL，标准回收率为97％－106％，相对标准偏差为3.6%，相关系数为0.9997，试验结果表明此方法简便、快速、准确。     

埋入电镀电阻在高速线路中的应用

埋入电阻是实现高频电路的重要方法之一。现已开发出在内层要求精确电镀上电阻元件的工艺,这意味着PCB制造厂可采用各种类型层压板材料,根据不同电镀时间得到从25 Ω到100 Ω范围内的方块电阻值(电阻率),而不是采用各种不同电阻值金属箔的基材来制备不同阻值的埋入电阻。采用常规PWB的活化和化学镀等制造步骤便可制作这种电阻,这种埋入电阻工艺是易于激光检修并层压到多层板内部是很稳定的。这种埋入电阻经过多层层压,温度变化或者显露于潮湿环境下表明电阻值是很小改变的,经过模拟电路运作具有好的稳定性。     

CO_2激光“提切法”治疗寻常疣和足庶疣

采用“提切”方式,用CO_2激光对寻常疣和蹠疣进行治疗,比传统方式出血少,复发率低。     

超高速炸药加速器炮口弹丸速度的测量

炸药驱动器超高速(>3000m/s)弹丸速度的测量是超高速发生器及超高速碰撞现象研究等领域内一个必不可少的环节,本文在传统电测法及X光闪先照相技术的基础上,提出了改进的测量技术,使测量中尽量避免各种因素对测试的干扰,成功地获得了弹丸的炮口速度。实验表明,该技术为超高速驱动器及超高速撞击现象研究提供了一种可靠而方便的测试手段。     

各向异性内包层对双包层光纤特性影响的分析

提出了单轴各向异性材料为内包层，且其主轴沿光纤轴线（z轴）方向的双包层光纤模型，推出了矢量模特征方程，重点研究了主轴折射率比kcl对波导色散的影响，针对从矢量模特征方程求解波导色散因表达式极为复杂而无法直接求解的困难，提出了一种求解波导色散的有效方法，研究结果发现可以在不改变光波导结构参量的条件下，通过改变kcl可有效地改变光纤的波导色散，也分析了kcl、几何参量S、光学参量R对低次模的传输和截止特性的影响。研究结果为获得更为理想的色散补偿、色散平坦光纤及设计新型无源光器件提供了重要的依据。     

卷积交织器和解交织器的VHDL设计和FPGA实现

介绍了信道编码中所采用的前向纠错编码(FEC)方案中的重要技术——卷积交织器和解交织器的原理，并在此基础上提出了一种VHDL设计和FPGA实现方案，给出了具体的实现方法，该方法具有实现简单和占用资源少的优点。