Crystallographic report: Bis(norfloxacin)dilead(II) tetranitrate, [Pb2(H‐Norf)2(ONO2)4]

The centrosymmetric binuclear structure of [Pb₂(H‐Norf)₂(ONO₂)₄]shows the geometry around each lead(II) atom to be distorted trigonal bipyramidal with Pb–O distances ranging from 2.357(3) to 2.769(4) Å. Copyright © 2003 John Wiley & Sons, Ltd.     

多功能滚齿机的数字控制系统

本文叙述了以ＳＴＤＰＣ／ＸＴ（或ＰＣ／ＡＴ）机为主要核心构成的滚齿机数字控制系统的结构，软件设计和特点，系统采用混合语言编程，极大地提高了软件设计的灵活性与快速性，也分析了ＣＮＣ系统的加工过程，提出了加工中的软件预处理控制方法，并给出了轴伺服控制的并行算法分析与实现。     

2‐Cyanoprop‐2‐yl dithiobenzoate mediated reversible addition–fragmentation chain transfer polymerization of acrylonitrile targeting a polymer with a higher molecular weight

The reversible addition–fragmentation chain transfer (RAFT) polymerization of acrylonitrile (AN) mediated by 2‐cyanoprop‐2‐yl dithiobenzoate was first applied to synthesize polyacrylonitrile (PAN) with a high molecular weight up to 32,800 and a polydispersity index as low as 1.29. The key to success was ascribed to the optimization of the experimental conditions to increase the fragmentation reaction efficiency of the intermediate radical. In accordance with the atom transfer radical polymerization of AN, ethylene carbonate was also a better solvent candidate for providing higher controlled/living RAFT polymerization behaviors than dimethylformamide and dimethyl sulfoxide. The various experimental parameters, including the temperature, the molar ratio of dithiobenzoate to the initiator, the molar ratio of the monomer to dithiobenzoate, the monomer concentration, and the addition of the comonomer, were varied to improve the control of the molecular weight and polydispersity index. The molecular weights of PANs were validated by gel permeation chromatography along with a universal calibration procedure and intrinsic viscosity measurements. ¹H NMR analysis confirmed the high chain‐end functionality of the resultant polymers. © 2007 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 45: 1272–1281, 2007     

The compound binomial risk model with time-correlated claims

In this paper, we consider the compound binomial risk model with the time-correlated claims. It is assumed that every main claim will produce a by-claim but the occurrence of the by-claim may be delayed. We obtain the recursive formula of the joint distribution of the surplus immediately prior to ruin and deficit at ruin. Furthermore, the ruin probability is given by means of ruin probability and the deficit at ruin of the classical compound binomial risk model. Finally, we derive an upper bound for the ruin probability.     

SiO2-羟基表面上金属原子的第一性原理研究

采用第一性原理方法研究了SiO2-羟基表面上几种金属原子的吸附性质,发现In和Ga在SiO2-羟基表面上的结合很弱,而Fe,Co,Ni在该表面上与Si,O形成强的化学键.等势能面和扩散势垒计算表明In(Ga)的扩散激活能只有0.1-0.3 eV,表明这两种原子容易在表面上扩散.这些结果可以定性地解释纳米合成中的一些实验现象.     

基于Intel 87c196kc的某机载设备随动系统数字控制器的实现

介绍了某机载光电设备随动系统控制器的设计与实现。该控制器是基于Intel公司87c196kc的数字控制器，设计中充分利用了87c196kc较强的运算能力及其它片内功能，使得控制器设计简捷、调整灵活、体积小，提高了系统的可靠性。     

碳掺杂β-FeSi2薄膜的电子显微学研究

本文利用透射电子显微镜对离子注入合成的β-FeSi2和β-Fe(C,Si)2薄膜进行了对比研究.电镜观察结果表明,选择C作为掺杂元素,能够得到界面平直、厚度均一的高质量β相薄膜,晶粒得到细化,β-FeSi2层稳定性提高.尤其在60kV、4×1017ions/cm2条件下注入直接形成非晶,在退火后会晶化为界面平滑、厚度均匀的β-FeSi2薄膜.因此从微结构角度考虑,引入C离子有益于提高β-FeSi2薄膜的质量.     

偏振模色散统计特性的研究

利用动态方程研究了偏振模色散矢量的统计特性 ,分别用统计系综和频率系综两种方法进行数值模拟。数值结果表明 ,统计系综和频率系综两种方法的结果一致。在大归一化距离条件下 ,均方根时延的平方随归一化距离线性变化 ;偏振模色散矢量的各个分量服从高斯分布 ,差分群时延服从麦克斯韦分布 ;偏振模色散矢量弥散于整个邦加球     

心脏黏液瘤的超微结构研究

对8例心脏黏液瘤进行了临床病理总结，着重进行了超微结构的研究，结果表明黏液瘤细胞有4种超微结构表现：（1）原始间叶细胞；（2）纤维母细胞样；（3）肌纤维母细胞样；（4）上皮样。提出心脏黏液瘤细胞起源于原始间叶细胞，有纤维母细胞、肌及上皮样分化。并且提出瘤细胞参与黏液瘤基质的形成。     

约束装箱问题的混合遗传算法求解

本将最佳适应法和遗传算法相结合，提出了一种新的启发式混合遗传算法对具有时间约束的装箱问题进行求解，给出了具体的算法步骤，试算结果表明基于启发式算法的混合遗传算法适合于求解各种约束条件下的大规模装箱问题。