用GC/MS联用技术测定西藏酥油中的风味物质

采用水蒸汽蒸馏法提取出酥油中的风味物质,利用气相色谱-质谱联用技术对西藏酥油中的风味物质进行了分离、鉴定,共确定了34种化合物及其它们的相对含量.其中羧酸9种,酯11种,酮6种,醇2种,烯类化合物4种,苯胺类化合物和苯酚类化合物各1种.其中主要成分为己酸和辛酸,其相对含量分别为30.35%和33.22%.     

利用动态反射法对手性液晶Bragg反射的分析

利用动态反射法对手性液晶材料的选择性反射特性进行了分析。根据理论分析结果，利用MATLAB程序计算了手性液晶膜层的反射光谱，得到了反射光谱随手性液晶的螺距和折射率变化的关系；利用动态反射法可以较为方便、快速地对手性液晶膜的Bragg反射特性进行数值求解分析，分析和计算结果可以为反射式液晶显示的设计和计算提供理论参考。由于在数值求解中引入了简化条件，因此该计算方法只能应用于△n值较小的情况，当Δn值较大时，应该用其他求解方法来完成计算分析工作。     

SCAN90CP02型LVDS交叉点开关的功能及应用

SCAN90CP02是美国国家半导体公司最新推出的LVDS超高速交叉点开关，具有的预增强功能使其可应用于高损耗的背板及电缆连接中以增强驱动能力。文中详细介绍该电路的功能、结构和配置方式，同时给出它的应用方法。     

Ultrasonic backscatter from bovine tissues: variation with pathology

This is the second in a series of two papers reporting results collected on ultrasonic propagation properties, namely, velocity, attenuation, and backscatter of various mammalian tissues. In the first paper [J. Acoust. Soc. Am 78, 871 (1985)], the experimental results of five different types of normal bovine tissues were given. In this paper, results obtained for the most common bovine disease in the liver, liver abscess, and in the heart, lymphosarcoma, will be presented. These data show that the ultrasonic properties of tissues with these two types of pathologies are significantly deviated from those of normal tissues, thus providing further evidence that ultrasonic properties may be used as quantitative indicators of a certain disease for diagnostic purposes.     

A New CMOS Active Transformer QPSK Modulator With Optimal Bandwidth Control

This brief presents a new quadrature phase-shift keying (QPSK) modulator for Bluetooth applications with an optimal transaction bandwidth control. The modulator reduces the bandwidth of the modulated carrier by minimizing their transition sharpness. CMOS active transformers are developed and utilized in quadrature oscillator and multiplexer of the modulator to provide comparable phase noise performance without using spiral inductors and transformers. The performance of the modulator is assessed using a 1.6-GHz QPSK base-band modulator implemented in TSMC 0.18-mum 1.8-V CMOS technology and analyzed using SpectreRF from Cadence Design Systems with BSIM3v3 device models. The total transistor area and power consumption of the modulator are 2840 mum² and 30 mW, respectively. The phase noise of the quadrature oscillator is 110 dBc/Hz at 500-kHz frequency offset.     

Viscoelastic properties of nanosilica‐filled epoxy composites investigated by dynamic nanoindentation

The viscoelastic properties of the epoxy filled with silica nanoparicles have been investigated by dynamic nanoindentation and characterized by the storage modulus and loss tangent. The materials studied are neat epoxy and silica/epoxy composites with silica volume fraction of 1, 3, 6, 10, and 14 vol %, respectively. The silica nanoparticles with an average diameter of 25 nm are found to disperse homogeneously in the epoxy matrix. The effect of the particle content, force frequency, and penetration load on the viscoelastic behavior is studied and discussed. The comparison with traditional testing methods such as tension, bending, and DMTA is made. Besides, theoretical results by using micromechanics models are also obtained and compared with the experimental results. © 2009 Wiley Periodicals, Inc. J Polym Sci Part B: Polym Phys 47: 1030–1038, 2009     

A wide band gap polymer derived from 3,6‐carbazole and tetraphenylsilane as host for green and blue phosphorescent complexes

We have synthesized a novel wide band gap polymer P36HCTPSi derived from 3,6‐carbazole and tetraphenylsilane by palladium‐catalyzed Suzuki coupling reaction. The resultant polymer shows a high glass transition temperature (217 °C) and good thermal stability. The conjugation length of P36HCTPSi is effectively confined because of the δ‐Si interrupted polymer backbone. The polymer exhibits a violet emission with a peak at 392 nm in solution, and the band gap estimated from the onset of its absorption is 3.26 eV. The high energy emission and wide band gap of P36HCTPSi make it appropriate host for green and blue emission phosphorescent materials. Efficient energy transfers from P36HCTPSi to both fac‐tris[2‐(2‐pyridyl‐kN)‐5‐methylphenyl]iridium(III) (green emission) and bis[(4,6‐difluorophenyl)pyridinato‐N,C²]‐(picolinato)iridium(III) (blue emission) were observed in photoluminescence (PL) spectra. Highly efficient phosphorescent polymer light‐emitting devices were realized by using P36HCTPSi as the host for iridium complexes, the maximum luminous efficiencies for green and blue devices were 27.6 and 3.4 cd/A, respectively. © 2009 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 47: 4784–4792, 2009     

Synthesis,photopolymerization, and adhesive properties of new bisphosphonic acid monomers for dental application

Four new monomers, 3‐(N‐methylacrylamido)propylidenebisphosphonic acid, 3‐(N‐propyl‐acrylamido)propylidenebisphosphonic acid, 3‐(N‐hexylacrylamido)propylidenebisphosphonic acid, and 3‐(N‐octylacrylamido)propylidenebisphosphonic acid, have been synthesized in good yields and fully characterized by ¹H, ¹³C, ³¹P NMR, and HRMS. The copolymerization of these monomers with N,N′‐diethyl‐1,3‐bis(acrylamido)propane (DEBAAP) has been investigated with differential scanning calorimetry. These mixtures show a higher reactivity than DEBAAP. New self‐etch dental primers, based on these acrylamide monomers, have been formulated. Dentin shear bond strength measurements have shown that primers based on these bisphosphonic acids assure a strong bond between the tooth substance and a dental composite. © 2009 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 47: 5258–5271, 2009