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141.
Xiaohua He Hailiang Zhang Deyue Yan Xiayu Wang 《Journal of polymer science. Part A, Polymer chemistry》2003,41(18):2854-2864
A series of side‐chain liquid‐crystalline (LC) homopolymers of poly[6‐(4‐methoxy‐4′‐oxy‐azobenzene) hexyl methacrylate] with different degrees of polymerization were synthesized by atom transfer radical polymerization (ATRP), which were prepared with a wide range of number‐average molecular weights from 5.1 × 103 to 20.6 × 103 with narrow polydispersities of around 1.17. Thermal investigation showed that the homopolymers exhibit two mesophases, a smectic phase, and a nematic phase, and the phase‐transition temperatures of the homopolymers increase clearly with increasing molecular weights. A series of novel LC coil triblock copolymers with narrow polydispersities was synthesized by ATRP, and their thermotropic phase behavior was investigated with differential scanning calorimetry and polarized optical microscopy. The LC coil triblocks were designed to have an LC conformation of poly[6‐(4‐methoxy‐4′‐oxy‐azobenzene) hexyl methacrylate] with a wide range of molecular weights from 3.5 × 103 to 1.7 × 104 and the coil conformation of poly(ethylene glycol) (PEG) (number‐average molecular weight: 6000 or 12,000) segment. Their characterization was investigated with 1H NMR, Fourier transform infrared spectra, and gel permeation chromatography. Triblock copolymers exhibited a crystalline phase, a smectic phase, and a nematic phase. The phase‐transition temperatures from the smectic to nematic phase and from the nematic to isotropic phase increased, and the crystallization of PEG depressed with increasing molecular weight of the LC block. © 2003 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 41: 2854–2864, 2003 相似文献
142.
Haihong Fang Binyuan Hu Lingshen Wang Rongli Lu Cui Yang 《Frontiers of Chemistry in China》2008,3(2):193-197
Nanometer MgO was prepared via a sol-gel auto-combustion technique using magnesium nitrate as raw material and citric acid
as chelating agent. IR spectra of the dried gel were used to investigate the structure of the precursors. By studying the
different TG curves of magnesium citrate gel prepared by different methods, we found that a combustion process occurred and
the nitrate ions acted as an oxidant in the combustion process. TEM photographs of synthesized powders from the sol-gel auto-combustion
showed that the crystallites were uniform in size. In addition, the XRD pattern of this sample showed that the particle size
was 8.9 nm. The BET curves, in turn, showed that the specific surface of the sample was 26.34 m2/g. The mechanism of the frothing process in restraining agglomeration is discussed.
__________
Translated from Journal of East China Normal University (Natural Science), 2007, (2): 52–57 [译自: 华东师范大学学报(自然科学版)] 相似文献
143.
Frictionless indentation responses of transversely isotropic piezoelectric film/rigid substrate systems under circular cylindrical indenter (i.e., punch), conical indenter (i.e., cone), and spherical indenter (i.e., sphere) are investigated. Both insulating and conducting indenters are considered. The technique of Hankel transformation is employed to derive the corresponding dual integral equations for the mixed boundary value indentation problems. For the two limiting cases of infinitely thick and infinitely thin piezoelectric films, closed-form solutions are obtained. For piezoelectric films of finite thickness, a numerical method is constructed to solve the dual integral equations and semi-empirical models having only two unknown parameters are proposed for the responses of indentation force, electric charge and electric potential, and contact radius. With the two parameters inferred from the numerical results, the semi-empirical formulae are found to provide good estimates of the indentation responses for the two limiting cases of infinitely thick and thin piezoelectric films, as well as those in between. The inferred parameters in the proposed semi-empirical formulae for normalized indentation force and electric charge are checked against four different piezoelectric materials and are found to be insensitive to the selection of piezoelectric materials. It is believed that the proposed semi-empirical indentation formulae are useful in developing experimental indentation techniques to extract the material properties of piezoelectric films. 相似文献
144.
Tie-Jun Liu Yue-Sheng Wang Chuanzeng Zhang 《Archive of Applied Mechanics (Ingenieur Archiv)》2008,78(4):267-282
The main interest of this study is a new method to solve the axisymmetric frictionless contact problem of functionally graded
materials (FGMs). Based on the fact that an arbitrary curve can be approached by a series of continuous but piecewise linear
curves, the FGM is divided into a series of sub-layers with shear modulus varying linearly in each sub-layer and continuous
at the sub-interfaces. With this model, the axisymmetric frictionless contact problem of a functionally graded coated half-space
is investigated. By using the transfer matrix method and Hankel integral transform technique, the problem is reduced to a
Cauchy singular integral equation. The contact pressure, contact region and indentation are calculated for various indenters
by solving the equations numerically.
An erratum to this article can be found at 相似文献
145.
We demonstrate three-dimensional tomographic imaging using a Fresnel lens with broadband terahertzpulses.Objects at various locations along the beam propagation path are uniquely imaged on the sameimaging plane using a Fresnel lens with different frequencies of the imaging beam.This procedure allowsthe reconstruction of an object's tomographic contrast image by assembling the frequency-dependentimages. 相似文献
146.
147.
The communication infrastructure of a mobile computing environment can be based on the structure of a cellular/microcellular telephone system or a PCS network. In such a system, the occurrence of handoffs cannot be avoided and when handoffs occur, wireless links held by mobile computers crossing cell boundaries may be forced to terminate. The probability that a handoff access request will result in forced termination has a significant effect on the performance of a mobile computing environment, as does the probability that an initial access request will be blocked. Although some research has been done on initial and handoff accesses in cellular/microcellular telephone systems and PCS networks, the analytical models used in this research are not appropriate for mobile computing, since unlike a telephone, a mobile computer may use several channels at once. In this paper, we develop an analytical model to study initial and handoff accesses in a mobile computing environment. The model is based on a multi-dimensional continuous time Markov chain. The accuracy of the model is verified by comparison with simulation results. We then use the model to find a practical approach to balancing the initial access blocking probability and avarage forced termination probability of a connection in a mobile computing network.This research was supported by the National Science Council, ROC, under grant NSC 85-2213-E-009-063. 相似文献
148.
坦克红外特征控制技术评述 总被引:2,自引:1,他引:1
坦克红外特征控制对于提高坦克的战场生存能力具有重要意义。控制的主要方法有遮障、表面处理、外形技术、主动冷却、总体设计等。坦克红外特征的控制必须与其他波段,特别是射频波段的特性控制兼容。遮障和低发射率涂料是现役坦克红外特征控制的主要措施。而对未来的主战坦克,设计应是减少其系统特性的重要途径。 相似文献
149.
Yong Wang 《Journal of Infrared, Millimeter and Terahertz Waves》1996,17(6):1095-1101
G.T.D. Analysis of the radiation from magnetic line source on a conducting circular cylinder with dielectric coating is presented. The G.T.D. solution is computed numerically by the residue series, Taylor series and the method of stationary phased in the shadow, transition and illuminated region, respectively. The numerical results of the G.T.D. solution show good agreement with the eigenfunction results. 相似文献
150.
PFC控制技术的一种改进方案 总被引:1,自引:0,他引:1
文章首先指出了目前PFC所用控制技术的缺陷,然后提出了一各改进方案,并从理论分析和仿真验证的角度证明了改进方案的可行性和先进性。 相似文献