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991.
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Baoliang Lv Zhenyu Liu Hong Tian Yao Xu Dong Wu Yuhan Sun 《Advanced functional materials》2010,20(22):3987-3996
Despite significant advances in iron oxide nanoparticles, it is still a challenge to synthesize regular polyhedral single‐crystalline α‐Fe2O3 particles because the surface energies of several low‐index planes are fairly similar. In the work presented here, well‐dispersed and single‐crystalline dodecahedral and octodecahedral α‐Fe2O3 particles are synthesized by a facile hydrothermal method with the aid of F? anions. The crystalline structure of the polyhedral particles is disclosed by various characterization techniques. The dodecahedral particles are of hexagonal bipyramidal shape and enclosed by twelve equivalent (101) planes. The octodecahedral particles are formed by adding six equivalent (111) planes on the two tips of a dodecahedral particle, that is, they are enclosed by twelve (101) planes and six (111) planes. The existence of F? anions plays a crucial role in the control of polyhedral particle shape. The function of F? anions in the shape formation of the polyhedral particles is proposed as follows: 1) A high concentration of exposed Fe3+ cations induces preferential adsorption of F? anions on the (100) plane and leads to the slowest growth along the [100] direction. When the concentration of F? anions is higher than 24 mM , a stable speed ratio of growth along the [001] and [100] directions results in the exposure of (101) planes. 2) With a lower concentration of F? anions, six symmetrical (111) planes with low concentration of exposed Fe3+ cations are present at the tops of a dodecahedral particle to form an octodecahedron. Furthermore, the dodecahedral and octodecahedral α‐Fe2O3 particles show much stronger magnetism than the previously reported α‐Fe2O3 nanostructures, having coercivities of 4986 Oe and 6512 Oe, respectively. Such high coercivities are attributed to a large local magnetic anisotropy, which might be induced by the polyhedron with equivalent crystallographic planes and/or the presence of F? anions. 相似文献
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An improved two-channel Synthetic Aperture Radar Ground Moving Target Indication (SAR-GMTI) method based on eigen-decomposition
of the covariance matrix is investigated. Based on the joint Probability Density Function (PDF) of the Along-Track Interferometric
(ATI) phase and the similarity between the two SAR complex images, a novel ellipse detector is presented and is applied to
the indication of ground moving targets. We derive its statistics and analyze the performance of detection process in detail.
Compared with the approach using the ATI phase, the ellipse detector has a better performance of detection in homogenous clutter.
Numerical experiments on simulated data are presented to validate the improved performance of the ellipse detector with respect
to the ATI phase approach. Finally, the detection capability of the proposed method is demonstrated by measured SAR data. 相似文献
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We consider asynchronous Slepian-Wolf coding where the two encoders may not have completely accurate timing information to synchronize their individual block code boundaries, and propose LDPC code design in this scenario. A new information-theoretic coding scheme based on source splitting is provided, which can achieve the entire asynchronous Slepian-Wolf rate region. Unlike existing methods based on source splitting, the proposed scheme does not require common randomness at the encoder and the decoder, or the construction of super-letter from several individual symbols. We then design LDPC codes based on this new scheme, by applying the recently discovered source-channel code correspondence. Experimental results validate the effectiveness of the proposed method. 相似文献
1000.
Most of the recently reported test point selection algorithms for analog fault dictionary techniques are based on integer-coded
table (ICT) technique. Hence, the accuracy of these algorithms is closely related to the accuracy of the ICT technique. Unfortunately,
this technique is not accurate, especially when the size of fault dictionary is large. This paper proposes an accurate fault-pair
Boolean table technique for the test point selection problem. First, the approach to transform the fault dictionary into a
fault-pair Boolean table is introduced. Then, a test point selection algorithm based on the fault-pair Boolean table is proposed.
Thirdly, several example circuits are used to illustrate the proposed algorithm. Simulated results indicate that the proposed
method is more accurate than the other methods. Therefore, it is a good solution for minimizing the size of the test point
set. 相似文献