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21.
22.
We report a study of a series of heavy rare earth tris‐8‐hydroxyquinolines (REQ3s), using UV‐visible absorption spectroscopy, infrared absorption spectroscopy, and photoluminescence (PL) measurements. We show that the heavy REQ3s are all chemically similar to each other and to aluminium tris‐8‐hydroxyquinoline, at least in terms of the ligand behavior. Characteristic rare earth 4f–4f luminescence is only observed for ErQ3 and YbQ3 due to the relatively low energy of the ligand triplet state. We show that a triplet transfer mechanism cannot be responsible for the observed Yb 4f–4f luminescence observed in YbQ3. Instead, an internal chemiluminescent process is shown to be energetically favorable. The thin film PL spectra of all the heavy REQ3s are dominated by triplet emission, except for that of ErQ3, for which transfer to the Er3+ ion represents an efficient alternative. The PL spectra of powder samples, which would be expected to consist of approximately equal amounts of both isomers, are dominated by singlet emission. This is in contrast to the results from the thin films, and suggests that the isomer which predominates in the thin films has a much higher intersystem crossing rate than the other isomer. 相似文献
23.
Arghavani R. Xia L. M'Saad H. Balseanu M. Karunasiri G. Mascarenhas A. Thompson S.E. 《Electron Device Letters, IEEE》2006,27(2):114-116
This letter discusses a reliable and manufacturable integration technique to induce greater than 1 GPa of stress into a p-channel MOSFET, which will be required to increase the drive current beyond 1 mA//spl mu/m at the sub-90-nm process generation. Uniaxial compressive stress is introduced into the p-channel by both a selective deposition of SiGe in the source/drain and an engineered 2.5-GPa compressively stressed nitride. The highest to date compressively stressed SiN film is obtained by heavy ion bombardment during the deposition of the film. 相似文献
24.
Non-compact generalized variational inequalities for quasi-monotone and hemi-continuous operators with applications 总被引:1,自引:0,他引:1
Some results are obtained for non-compact cases in topological vector spaces for the existence problem of solutions for some
set-valued variational inequalities with quasi-monotone and lower hemi-continuous operators, and with quasi-semi-monotone
and upper hemi-continuous operators. Some applications are given in non-reflexive Banach spaces for these existence problems
of solutions and for perturbation problems for these set-valued variational inequalities with quasi-monotone and quasi-semi-monotone
operators.
This revised version was published online in June 2006 with corrections to the Cover Date. 相似文献
25.
A comparison of a theoretical model for quasi-statically and dynamically induced environmental vibration from trains with measurements 总被引:1,自引:0,他引:1
This paper presents comparisons between a theoretical ground vibration model and measured data at three sites. The model, which is briefly outlined here, encompasses both the quasi-static and dynamic mechanisms of excitation. The vertical dynamics of a number of vehicles travelling at a constant speed on an infinite track are coupled to a semi-analytical model for a three-dimensional layered ground. This model is also used to demonstrate the roles of the two components of vibration at different frequencies and for train speeds below and above the lowest ground wave speed. It is found that, in most practical cases, the dynamic component gives rise to the higher level of vibration. 相似文献
26.
27.
We have prepared glucose and cellobiose conjugates at the phenolic 3- and hydroxylic 17-positions of the pure anti-estrogenic compound fulvestrant (ICI 182,780), which has recently been approved in the USA for the treatment of advanced postmenopausal breast cancer. Glycosylation at the 17-position was achieved most effectively using pivaloyl protection of the sugar imidates employed, which we found suppressed the competing transacylation reaction and led to improved yields of the product glycosides. 相似文献
28.
Colin J. Thompson Keith M. Briggs Peter Farrell Anthony Fleming Bruce Hocking Kenneth Joyner Vitas Anderson Andrew W. Wood 《Physica A》1995,220(3-4):471-484
A nonlinear Lorenz model describing interactions between charged particles and combined ac-dc electromagnetic fields is studied for various combinations of frequencies, field strengths and relative angle (θ) between the ac and dc magnetic fields. Strong directional effects on the magnitude and location of resonant particle motion are observed when θ is varied and the regular resonance windows in the aligned field (θ = 0) and linear version of the model studied previously by Durney etaal., break up to form irregular and less well pronounced regions of large and small particle displacements when nonlinearities are taken into account. The length of time takne to achieve resonant behaviour also becomes larger and more variable when nonlinearities are present. The possible relevance of these effects to interactions between electromagnetic fields and biological media is briefly discussed. 相似文献
29.
Ge segregation during the growth of Si1 − xGex alloys (x = 5, 10, 20, and 40%) was studied using X-ray photoelectron spectroscopy. The alloys were grown in thicknesses up to 20.0 nm at 500°C to measure quantitatively the amount of segregated surface Ge. The length of alloy needed to reach steady-state growth edge was found to decrease with increasing alloy concentration (4.8, 2.8, 2.4, and 2.0 nm, respectively). It was found that each alloy had a complete monolayer of Ge on the surface and an increasing amount of segregated Ge in the second layer (20, 55, 80, and 95%, respectively) during steady-state growth. An increase in the temperature of alloy growth (400–750°C) resulted in an increase in the leading edge of alloy growth but did not change the amount of segregated Ge during steady-state growth. We propose that film stress is responsible for the amount of Ge segregation. 相似文献
30.
A real-time interactive graphics simulation of the mechanics of the human thumb has been developed. The simulation utilizes a realistic data structure for the bones of the thumb which may be expanded to include the hand and forearm. This is coupled to a model of the kinematics of the joints in a concurrent processing arrangement in which the dynamic graphical transformations for scaling, translation, rotation, perspective, and clipping are all performed on a special-purpose display processor. The model and the control functions are distributed between this processor and a separate general-purpose superminicomputer. The resulting system presents the user with a realistic simulation of the movements of the thumb in normal and impaired states. The user may choose from a menu of options, including an interactive tendon transfer simulation for the current hand being simulated. He may control (interactively and in real time) the view, observation position, skeletal motion, and parameters for use in the model of joint mechanics. This type of computer modeling, utilizing a realistic three-dimensional data structure, models of musculoskeletal kinematics, and interactive programming, shows great potential for bringing mathematical modeling into useful clinical, research, and educational applications. 相似文献