The effect of micro-morphology of Bi2O3 on catalytic properties of Co/Bi catalyst for wet air oxidation of acetic acid

The novel phase transfer catalysts S-8 [4-(dimethyloctylammonium) propansultan] and DB-X [1,4-bis(triethylmethylammonium)benzene dibromide] were synthesized and employed for high conversion synthesis of dichlorocyclopropane from various olefins.This revised version was published online in December 2005 with corrections to the Cover Date.     

基于DMF捕获系统频率选择性信道下捕获性能的分析

对基于数字匹配滤波器(DMF)捕获系统在频率选择性信道下的捕获性能进行了深入讨论，利用状态转移图推导出单次驻留判决方式时平均捕获时间的表达式，对平均捕获时间与多径分量的关系进行了数字分析。得出的主要结论是：对于多径分量为非衰落信号时，多径分量之间的能量差别越大，系统捕获性能越好，多径分量的能量相等时，系统捕获性能最差，且随着可以分离的多径路数的增加下降；对于多径分量为慢衰落信号时，多径信道的捕获性能好于单径信道(非频率选择性衰落信道)，且多径分量之间的能量差别越大，系统捕获性能越差，当多径分量的能量相等时，捕获性能最好，这与非衰落信道的情形相反。因此在频率选择性衰落信道中，采用分集接收可以改善系统的捕获性能。     

一种前馈型全摆幅恒跨导准恒增益CMOS运放设计

设计了一种适合在低电源电压下工作的前馈型输入级放大结构，在全摆幅的动态工作范围内，输入级跨导保持不变，采用负载电流补偿以保证增益近似恒定，输出采用前馈型AB类输结构，实现全摆幅输出。     

以寻呼区分析为基础的PHS网络优化方法

通过分析PHS网络中各寻呼区的统计指标,剖析指标劣化的根本原因,采取修改相应的参数配置、移站、调整天线等措施进行网络优化,优化实施后再次收集统计指标做对比分析,总结经验。     

半导体带电粒子探测器的研制及其在空间物理中的应用

阐述了空间辐射环境监测的意义,描述了半导体带电粒子探测器的研制及由其组成的望远镜系统在空间物理中的应用,并给出了用此探测器在卫星上进行地球辐射环境监测、太阳质子事件和地磁暴探测的部分结果.     

An Additive Problem with Primes in Arithmetic Progressions

In this paper, we extend a classical result of Hua to arithmetic progressions with large moduli. The result implies the Linnik Theorem on the least prime in an arithmetic progression.     

Study on the Reaction of Benzimidazolium Salt with Amine Compounds

The addition-hydrolysis reaction of benzimidazolium salt with some mono- and bifunctional amine nucleophiles is reported,and a novel method of biomimetic synthesis for formamides and heterocycle compounds is provided.     

PURIFICATION OF L-METHIONINE AND N-ACETYL-D-METHIONINE FROM THE MIXTURE OF ENZYMATICALLY DEACYLATED N-ACETYL-DL-METHIONINE

1. INTRODUCTION Methionine, namely 2-amido-4-thiomethyl butyric acid with a structure of CH3SCH2CH2CHCOOH, is one of the essential amino acids and has two natural enantionmers, D and L-methionine. The mixture of L- and D-isomers can be used as analeptics or nutritive additives to maintain the equilibrium of amino acids of feed [1,2]. L-methionine can release active methyl and accelerate the synthesis of choline, which further speeds up the conversion of the lipid accumulated in liv…     

Microwave Synthesis, Characterization and DNA-binding Properties of a New Cobalt（ Ⅱ ） Complex with 2,6-Bis（benzimidazol-2-yl）pyridine

A new cobalt(Ⅱ) complex with tridentate ligand 2, 6-bis (benzimidazol-2-yl)pyridine has been synthesized by microwave irradiation method and characterized by elemental analysis,electrochemical and spectral methods. The binding of the complex with calf thymus DNA has also been investigated by absorption and fluorescence spectra.     

Synthesis of New 13-O-Acylavermectin Bl Aglycones

Six new 13-O-acylavermectin Bl aglycones(3-8) were synthesized from avermectin B1 aglycone and their bioactivities were evaluated against Spodoptera exigua, Spodoptera eridania, Tetranychus urticae and Aphis fabae.