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排序方式: 共有144条查询结果,搜索用时 125 毫秒
31.
Pujari Vijay Kumar Vinnakota Srilalitha Kakarla Ramana Kumar Maroju Sreedhar Ganesh Arram Pervaram S. 《Russian Journal of General Chemistry》2018,88(7):1502-1507
Russian Journal of General Chemistry - A novel series of (E)-1-{2/3/4-[(1-aryl-1H-1,2,3-triazol-4-yl)methoxy]phenyl}-3-(2-morpholinoquinolin-3-yl)prop-2-en-1-ones is synthesised from terminal... 相似文献
32.
Polyaniline sulfate‐zeolite composite was prepared by emulsion polymerization. Epoxy resin was cured using polyaniline‐sulfate salt and various amounts of polyaniline sulfate‐zeolite composite. The kinetics of the cure reaction for an epoxy resin based on the diglycidyl ether of bisphenol A (DGEBA) with polyaniline‐sulfate and polyaniline sulfate‐zeolite composite have been studied using differential scanning calorimetry (DSC) under isothermal and dynamic conditions. Isothermal kinetics analysis was performed using the phenomenological model of Kamal. Dynamic kinetic analysis was performed using Kissinger's method. Copyright © 2002 John Wiley & Sons, Ltd. 相似文献
33.
Polyaniline supported palladium catalysts were prepared from different palladium precursors and all the catalysts are well characterized using ICP-AES, FTIR, TGA-DTA, SEM-EDX and XPS analysis. All the catalysts were tested for Suzuki-Miyaura coupling of bromo- and chloroarenes in water and the catalyst prepared from PdCl2 precursor was found to be the most effective catalyst. The catalyst can easily be recovered by simple filtration and reused for several cycles with almost consistent activity. 相似文献
34.
Methylthiolation of structurally diverse aryl halides was accomplished under fluoride free conditions using catalytic amounts of CuI, and DMSO as the methylthiolation source. Optimization studies unveiled several varieties of promoters among which Zn(OAc)2 was found ideal. The analogous reaction with DMSO-d6 afforded corresponding deuterated aryl methyl thioether with 99% purity. Mechanistic studies revealed CuSMe as the active methylthiolation agent. 相似文献
35.
36.
P. Srihari Dinesh C. Bhunia P. Sreedhar S.S. Mandal J. Shyam Sunder Reddy J.S. Yadav 《Tetrahedron letters》2007,48(46):8120-8124
Aryl propargylic methanols undergo C- and O-nucleophilic substitution reactions in the presence of a catalytic amount of iodine in short reaction times with good yields. 相似文献
37.
Pala Rajasekharreddy Pathipati Usha Rani Bojja Sreedhar 《Journal of nanoparticle research》2010,12(5):1711-1721
The development of rapid and ecofriendly processes for the synthesis of silver (Ag) and gold (Au) nanoparticles is of great
importance in the field of nanotechnology. In this study, the extracellular production of Ag and Au nanoparticles was carried
out from the leaves of the plants, Tridax procumbens L. (Coat buttons), Jatropa curcas L. (Barbados nut), Calotropis gigantea L. (Calotropis), Solanum melongena L. (Eggplant), Datura metel L. (Datura), Carica papaya L. (Papaya) and Citrus aurantium L. (Bitter orange) by the sunlight exposure method. Qualitative comparisons of the synthesized nanoparticles between the
plants were measured. Among these T. procumbens, J. curcas and C. gigantea plants synthesized <20 nm sized and spherical-shaped Ag particles, whereas C. papaya, D. metel and S. melongena produced <20 nm sized monodispersed Au particles. The amount of nanoparticles synthesized and its qualitative characterization
was done by UV–vis spectroscopy and transmission electron microscopy (TEM), respectively. X-ray diffraction (XRD) and X-ray
photoelectron spectroscopy (XPS) were used for structural confirmation. Further analysis carried out by fourier transform
infrared spectroscopy (FTIR), provided evidence for the presence of amino groups, which increased the stability of the synthesized
nanoparticles. 相似文献
38.
Selvam Kaliyamoorthy Sreedhar Bojja Swaminathan Meenakshisundaram 《Research on Chemical Intermediates》2022,48(3):1309-1309
Research on Chemical Intermediates - This article has been retracted. Please see the Retraction Notice for more detail: https://doi.org/10.1007/s11164-020-04374-7 相似文献
39.
N. Y. Sreedhar P. Reddy Prasad M. Sankara Nayak D. Rekha C. Nageswara Reddy 《中国化学会会志》2009,56(6):1139-1146
In the present paper novel column solid phase extraction procedure was developed for the determination of Cd(II) and Pb(II) in cows', goats', ewes', buffalos' and humans' milk samples using newly synthesized reagent 2,2′‐DPED3P (2,2′‐{[1,2‐diphenylethane‐1,2‐diylidene]dinitrilo}diphenol) for preconcentration and separation prior to differential pulse polarography using amberlite XAD‐2 in the ranges of pH 4.0–5.0. The sorbed elements were subsequently eluted with 10 mL of 2 M HCl elutes were analysed by differential pulse polarography (DPP). The interference of foreign ions has also been studied. Effects of various instrumental parameters are investigated and received conditions are optimized. The total metal concentration of the milk samples in the study area were in the following ranges 0.030–0.090 μg L?1 of Cd(II), 0.009–0.026 μg L?1 of Pb(II) respectively. The limits of detections were found to be 0.020 and 0.024 μg L?1 for Cd(II) and Pb(II) respectively by applying a preconcentration factor ~40. The proposed enrichment method was applied successfully for the determination of metal ions in cows', goats', ewes', buffalos' and humans' milk samples. 相似文献
40.
The ethyl acetate extract of Excoecaria agallocha L. furnished three more new isopimarane diterpenoids, 11alpha,14alpha-dihydroxy-7,15-isopimaradien-3-one, agallochin J (1), 3alpha, 1alpha,14alpha-trihydroxyisopimara-7,15-diene, agallochin K (2) and 6alpha,14alpha,17-trihydroxy-7,15-isopimaradien-3-one, agallochin L. 相似文献