溶胶-凝胶生物玻璃多孔材料显微结构和生物活性的扫描电镜及红外光谱分析

本文利用溶胶．凝胶法制备了CaO-P2O5-SiO，系统生物活性玻璃，并以其为原料制备了用于骨修复及骨组织工程支架的块状生物活性材料。利用体外实验方法(invitro)结合x射线衍射(XRD)、扫描电子显微镜(SEM)和傅立叶变换红外光谱分析(FTIR)技术对不同烧结工艺制备的材料结构、晶相和生物活性的影响进行了分析研究。研究表明，经800℃和1100℃烧结5min的两种材料均有硅磷酸钙Ca5(PO4)2SjO4微晶相析出。烧结温度越高，析出微晶相的体积比例越大，材料的生物活性则越低。在模拟生理溶液中碳酸羟基磷灰石(HCA)只在烧结体中的玻璃颗粒表面形成，而在其硅磷酸钙Ca5(PO4)2SiO4微晶相表面未发现HCA形成。     

支持下一代无线宽带应用自适应QoS模型的研究

作为真正完整的下一代网络 ( NGN,Next Generation Network)解决方案 ,NGN需要在固定通信领域和移动通信领域都能够支持综合多媒体特性。NGN中的新一代移动通信网承载在开放式、层次化结构的分组交换网络之上 ,能够为用户提供端到端的 Qo S解决方案。本文分析了下一代移动通信系统中多媒体宽带应用的 Qo S问题 ,从无线通信系统的多层次结构出发 ,建立了业务流的 Qo S指标评判体系 ,为下一代网络中的无线宽带应用提供了一种自适应Qo S控制模型     

开发有线电视收费管理系统需注意的问题

分析有线电视业务及用户管理中出现的问题与解决办法，为系统的开发建立数据模型，以确保有线电视网络公司和用户的利益。     

PVR机顶盒文件存储系统的设计与实现

简要介绍了具有PVR功能的机顶盒，具体描述了PVR存储系统硬件与软件的设计与实现，重点讨论了PVR的关键部分——文件存储系统的设计和实现。     

Resource management in the next-generation DS-CDMA cellular networks

Direct sequence code-division multiple access has been shown as the predominant access technology to provide high-speed multimedia services in next-generation wireless cellular networks. The DS-CDMA cellular network significantly differentiates itself from the traditional narrowband TDMA/FDMA system, in which great capacity gain can be explored by taking advantage of its unique characteristics. This article addresses resource management in DS-CDMA cellular networks. We first provide an overview of the DS-CDMA network and discuss the main challenges in the design of resource management schemes. We then examine several critical issues within the scope of resource management, including congestion control, rate and power control, and cell planning, with the emphasis on call admission control. Finally, we offer some insights and discussions on the performance aspects, strengths, and weaknesses of existing proposals.     

无线光接入技术

无线光通信系统以其高带宽、低成本和安装迅捷等优势成为非常有竞争力的光接入新技术。对无线光通信系统的关键技术、主要优势和存在的问题及国内外相关产品的发展状况和主要特点进行了论述和介绍。     

Positively Thermo‐Sensitive Monodisperse Core–Shell Microspheres

In this paper, we report on a novel family of monodisperse thermo‐sensitive core–shell hydrogel microspheres that is featured with high monodispersity and positively thermo‐responsive volume phase transition characteristics with tunable swelling kinetics, i.e., the particle swelling is induced by an increase rather than a decrease in temperature. The microspheres were fabricated in a three‐step process. In the first step, monodisperse poly(acrylamide‐co‐styrene) seeds were prepared by emulsifier‐free emulsion polymerization. In the second step, poly(acrylamide) or poly[acrylamide‐co‐(butyl methacrylate)] shells were fabricated on the microsphere seeds by free radical polymerization. In the third step, the core–shell microspheres with poly‐ (acrylamide)/poly(acrylic acid) based interpenetrating polymer network (IPN) shells were finished by a method of sequential IPN synthesis. The proposed monodisperse core–shell microspheres provide a new mode of the phase transition behavior for thermo‐sensitive “smart” or “intelligent” monodisperse micro‐actuators that is highly attractive for targeting drug delivery systems, chemical separations, sensors, and so on.     

Crystallographic report: Bis(norfloxacin)dilead(II) tetranitrate, [Pb2(H‐Norf)2(ONO2)4]

The centrosymmetric binuclear structure of [Pb₂(H‐Norf)₂(ONO₂)₄]shows the geometry around each lead(II) atom to be distorted trigonal bipyramidal with Pb–O distances ranging from 2.357(3) to 2.769(4) Å. Copyright © 2003 John Wiley & Sons, Ltd.     

纳米β-Ni(OH)2与球型Ni(OH)2的热性能比较研究

用配位沉淀法合成出纳米级Ni（OH）2，并对其进行XRD，TEM，DSC分析，分析结果表明，所得纳米β-Ni（OH）2为可用作电极材料的β-Ni（OH）2，粒径为30－40nm，且热分解温度比普通球镍低10℃左右，摩尔分解热比普通球镍低4－7kJ，从理论上分析了产生此现象的原因。