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141.
Guido Momerency Karel Van Cauwenberghe Ernst A. De Bruijn Allan T. Van Oosterom Martin S. Highley Peter G. Harper 《Journal of separation science》1994,17(9):655-661
A method is described for the determination of the antitumor agent iphosphamide and seven of its metabolites in the plasma of cancer patients by multiple ion monitoring (MIM) GC-MS, mainly using the electron capture chemical ionization mode, of stable methyl and/or trifluoroacetyl derivatives. The metabolites determined were 2- and 3-dechloroethyliphosphamide, 4-ketoiphosphamide, carboxyiphosphamide, iphosphamide mustard, and two previously undetected metabolites, chloroethylamine and 1,3-oxazolidine-2-one. The isolation of the acidic and neutral metabolites was performed by solid phase extraction on to C18 adsorbent at pH 4. The weakly acidic iphosphamide mustard, isolated under these conditions with a yield of ca 50%, was measured as a stable methyltrifluoroacetyl derivative, in contrast to the corresponding phosphoramide mustard of the isomer cyclophosphamide which decomposes during derivatization. Chloroethylamine and 1,3-oxazolidine-2-one were isolated with high yield by liquid extraction with ethyl acetate at pH 10. Selective measurement of several metabolite derivatives with similar retention times was performed by multiple ion monitoring MS of specific ion masses, using a methyl phenyl siloxane capillary column previously employed in the study of cyclophosphamide metabolites. Quantitation of metabolites in patient plasma samples could be performed in the concentration range 3 ng to 20 μg per ml of original plasma. 相似文献
142.
143.
关于RNP和SCS的若干等价条件 总被引:1,自引:0,他引:1
使用切片方法,讨论了Banach空间中有界闭凸子集的RNP和SCS的若干等价条件. 相似文献
144.
145.
Arun Chandrasekhar Steven Brebels Serguei Stoukatch Eric Beyne Walter De Raedt Bart Nauwelaers 《Microelectronics Reliability》2003,43(3):351-357
At frequencies beyond 1 GHz, every component of the IC package contributes to the RF performance, whether required or not. In this work, we study the effects of packaging materials namely, the substrate and the globtop/underfill material on RF performance. We have measured interconnects on two area-array CSPs, the ball grid array and the polymer stud grid array using IMEC’s MCM-D technology. The measurements on the package interconnect show that the losses in the package substrate material account for about 50% of the total losses at 1.8 GHz and this drops to less than 20% at 5.2 GHz. The losses due to impedance mismatch dominate the losses especially below 10 GHz and considerable improvement in performance cannot be obtained by using an improved/expensive substrate. The other study is about the influence of globtop/underfill materials on wirebonds (through 3D EM simulations) as well as on standard 50 Ω MCM-D transmission lines (through experiments). While a higher value of dielectric constant of the globtop/underfill material is better on wirebonds, the influence of loss tangent is felt only above values of 0.1. The influence of seven different globtop/undefill materials on 50 Ω transmission lines has been used to extract their dielectric constant and loss tangent values at 30 GHz. These results are very valuable since one can hardly find the properties of globtop/underfill materials beyond 1 GHz. 相似文献
146.
Crupi F. Kaczer B. Groeseneken G. De Keersgieter A. 《Electron Device Letters, IEEE》2003,24(4):278-280
In this letter, we report new findings in the relation between channel hot-carrier (CHC) degradation and gate-oxide breakdown (BD) in short-channel nMOSFETS biased at V/sub G/>V/sub D/. We observe that the time-to-BD is strongly reduced in the hot carrier regime and that although the channel hot-electron injection into the oxide occurs mainly at the drain side, stress-induced leakage current (SILC) generation and oxide BD always occur at the source side. The results of these measurements indicate that not solely the energy of the injected electrons but also the oxide electric field is determinant in the oxide BD process. 相似文献
147.
Anne Boutet De Monvel-Berthier Louis Boutet De Monvel Gilles Lebeau 《Journal d'Analyse Mathématique》1992,58(1):39-60
Sans résumé
Dedicated to Professor Shmuel Agmon 相似文献
148.
New concepts for the study of incompressible plane or axisymmetric flows are analysed by the stream tube method. Flows without eddies and pure vortex flows are considered in a transformed domain where the mapped streamlines are rectilinear or circular. The transformation between the physical domain and the computational domain is an unknown of the problem. In order to solve the non-linear set of relevant equations, we present a new algorithm based on a trust region technique which is effective for non-convex optimization problems. Experimental results show that the new algorithm is more robust compared to the Newton-Raphson method. 相似文献
149.
Dattoli G. De Angelis A. Gallerano G.P. Mari C. Torre A. 《Quantum Electronics, IEEE Journal of》1991,27(4):903-907
The authors use a simple model of saturation in free-electron lasers operating with pulsed beams to study the intensity growth as a function of the cavity mismatch and of the coupling parameter. In spite of the simplicity of the model, the dependence of the intracavity power, as a function of the cavity detuning, is reproduced remarkably well. It is also pointed out that an enhancement of the optical power is obtained by adjusting the cavity length while the optical signal grows. The problem is analyzed qualitatively and realization schemes are proposed 相似文献
150.
De Jun Mu Guan-Zhong Dai Liu K.J.R. Yao K. 《Signal Processing, IEEE Transactions on》1995,43(2):555-556
Comments that the paper by Liu and Yao (see ibid., vol.40, no.1, p.190, 1992) presented an efficient algorithm for spectral decomposition, but the parallel algorithm and architecture for the Hessenberg reduction has a problem. The matrix obtained from the unitary similarity transformation is not necessarily a Hessenberg matrix. The authors reply that the Hessenberg reduction described is not in the Hessenberg form. Only the first column is in its proper form. There are many ways to overcome such a problem. One simple way is to use the multiphase rectangular systolic array 相似文献