Chemical Characteristic of Bioactive Polysaccharides Isolated from Ornithogalum caudatum Ait.

A water-soluble crude extract prepared from Ornithogalum caudatum Ait. (()CA) showing a high immunomodulating activitiy was isolated and characterized by virtue of gel filtration and column chromatography. The presence of the monosaccharides has been established by the chemical analysis. The quantitative analysis of the alditol acetate derivatives of them showed the ratios of the monosaccharides analyzed by means of GC respectively. The concentrations of protein(280 nm) and carbohydrate(496 nm) were detected respectively. The information of the molecular weight from the pure polysaccharide was obtained by several standard Dextrans from the Sephadex chromatography.     

双杂环α-氨基膦酸酯的合成及生物活性研究

以2-氨基-5-巯基-1,3,4-噻二唑为原料,经氯代频呐酮取代,溴代、硫脲环合得到中间体,再与一系列芳香醛和亚膦酸酯反应合成了7种目标化合物,并用元素分析、质谱和核磁共振氢谱对化合物进行了表征,生物活性实验证明,该类化合物10mg/L表现出较好的生长素活性和细胞分裂素活性.     

银元素的循环实验

设计并完成了由5步构成的银元素的循环实验,从银粉出发,经过银在硝酸中溶解,银离子与氯离子反应生成氯化银沉淀,氯化银溶解于氨水,银氨络离子与乙炔反应生成乙炔银,水合肼将乙炔银还原为单质银等化学反应,完成了银的循环实验。     

Extraction and Identification of Ginsenoside Re and Its Effects and Mechanism of Protecting Acute Renal Ischemia-reperfusion Injury in Rats

This paper studies the extraction and identification of ginsenoside Re from ginseng fruits and investigates the effect and mechanism of ginsenoside Re of protecting acute renal ischemia-reperfusion injury in rats.Having been smashed,the ginseng fruits were ultrasonically extracted twice with 95% ethanol for 30min each.Having been concentrated,the solution was dissolved with distilled water and separated by two-column chromatography,of which one was packed with macroporous resin D4020,and the other was packe...     

Matrix Solid-phase Dispersion Extraction of Alkaloids from the Roots of Aconitum kusnezoffii Reichb

Matrix solid-phase dispersion(MSPD) was developed for the extraction of four alkaloids, including aconitine, mesaconitine, hypaconitine and deoxyaconitine, from the roots of Aconitum kusnezoffii Reichb. The determination of the analyte was carried out by high performance liquid chromatography with UV detection. The alkaline alumina was used as sorbent. The mixture of acetonitrile and water was used as elution solvent. Several extraction parameters, such as type of sorbent, the ratio of sample to solid suppo...     

氮化铝薄膜的低温沉积

介绍了一种 ECR微波放电和脉冲激光沉积相结合低温沉积 Al N薄膜的新方法 .在 ECR氮等离子体环境中用脉冲激光烧蚀 Al靶 ,以低于 80℃的衬底温度在 Si衬底上沉积了 Al N薄膜 .结合样品表征和等离子体光谱分析 ,探讨了膜层沉积的机理 ,等离子体中活性氮物质的存在是 Al- N化合的重要因素 ,等离子体对衬底的辐照促进膜层的形成     

基于P-V双因素的网络激光标刻性能研究

传统激光标刻技术已在实际工业生产中普遍应用,但其系统最优标刻性能控制参数存在寻找及设置较为困难、繁琐等问题。针对该问题,本文设计了一种基于嵌入式网络激光标刻模式的新型激光标刻控制模型,并在该模型下通过相关数据预处理算法分析单一标刻影响因素对激光标刻性能的影响;再通过对实验数据的数理统计分析得出二值图像的标刻性能变化规律,最终得出在该材质及类似组成工件下的激光标刻的最优参数快速选择模型和性能最优值域。研究结果表明,该模型为最优激光标刻性能控制参数的快速选择提供了可靠的方法,为进一步研究激光标刻性能影响参数提供了重要参考。     

基于支持向量机数据分析红外手势识别方法研究

该文提出了利用支持向量机结合仿生六点手势模型优化红外体感控制设备手势识别的方法。采集空间手势信息,仿生六点手势模型提取手势特征向量,利用支持向量机分类及校对数据,引用核函数将低维空间不可分信息映射至高维空间实现线性可分。结果表明,运用基于支持向量机的红外体感设备手势方法能有效识别手势,减轻计算机通信的传输负荷。     

Effects of High Pressure on the Surface Plasmon Resonance of Copper and Silver Nanocrystals

We used a diamond anvil cell(DAC) to control the deformation of synthesized copper nanorods and silver nanoparticles. And we measured the surface plasmon resonance of copper nanorods and silver nanoparticles, which exhibit redshifts or blueshifts. The surface plasmon resonance shows an abnormal blue shift for both copper nanorods and silver nanoparticles. The solvents of copper nanorods and silver nanoparticles are n-hexane and water, where the pressure loads include quasi-hydrostatic and non-hydrostatic.     

Pd@SiO2/Al2O3的制备及其催化氧化CO性能评价

从Pd纳米粒子出发制备具有核壳结构的Pd@SiO₂纳米粒子,并将其负载于不同形貌Al₂O₃载体上,制备出具有良好CO催化氧化活性的催化剂。以纳米球形Al₂O₃为载体时,Pd@SiO₂/Al₂O₃催化剂活性优于无核壳结构的Pd/Al₂O₃催化剂。将纳米Pd@SiO₂负载到球形和菱形Al₂O₃上,制备出Pd@SiO₂/Al₂O₃催化剂。结果表明:具有较大比表面积的Al₂O₃载体(球形)有利于Pd@SiO₂的分散,且SiO₂层可以抑制Pd粒子的团聚,能在一定程度上改善催化活性。而较小比表面积的载体(菱形)上出现了Pd@SiO₂的团聚,表现出较低的CO氧化活性,但在降低负载量后,CO氧化活性明显提高。该结果为推动新型热稳定、高效纳米三效催化剂的研发具有一定的启示意义。