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Elionai Cassiana de Lima Gomes Izabella Ercole de Carvalho Silvia Ligório Fialho Jamile Barbosa Maria Irene Yoshida Armando da Silva Cunha Júnior 《Journal of Thermal Analysis and Calorimetry》2018,131(3):2123-2128
Most of the pharmaceutical products are formulated as solid dosage form, which may present drug–excipient interactions that lead to changes in the chemical nature of the drug, such as solubility and bioavailability and may compromise its safety and effectiveness. Differential scanning calorimetry (DSC) is a widely used method for the rapid evaluation of the drug-excipient compatibility and the stability of the mixture formed; however, there is no consensus on the preparation methods of the drug–excipient mixtures. The aim of this study was to investigate the influence of the mixing method on the drug–excipient compatibility studies by means of DSC analysis, using tenofovir disoproxil fumarate as a drug model. Statistical analysis revealed significant differences in the heat of fusion of the drug in the mixtures prepared by several mixing methods. Vortex Mixer with a Pop-Off Cup used for 3 min proved to be very satisfactory for these studies. A polymorphic transition was observed in the mixture prepared with the mortar and pestle. Therefore, this method should be avoided since it may induce errors in the interpretation of DSC results. In this way, the mixing method used to prepare a mixture for studies of interactions between the API and the excipients in a pharmaceutical formulation has a great influence on the results and it must be chosen carefully. 相似文献
113.
We present a simplified correlation for calculating the dissolved gas moles in a pendant drop during the diffusion time, for
several drop shapes. After this correlation is determined, the Yang and Gu (Ind Eng Chem Res 44:4474–4483, 2005) dynamic pendant drop volume analysis (DPDVA) method for calculation of mass diffusivity from the pendant drop volume variation
against time can be used. We solved the differential equation in cylindrical coordinates for the mass transfer model of the
gas diffusion into the liquid inside the pendant drop, using a different characteristic length (LC), instead of the outer radius of the syringe needle (rn) used in Yang and Gu (Ind Eng Chem Res 44:4474–4483, 2005) for defining the dimensionless variables. LC is the relationship between the pendant drop volume and its mass transfer surface area at the initial conditions. The generalized
correlation saves time, simplifies the method application and the deviations in the diffusion coefficient calculation respect
to the complete Yang and Gu model are below 6%. 相似文献
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Antonio J. Ruiz-Ruiz Oscar Canovas Pedro E. Lopez-de-Teruel 《Mobile Networks and Applications》2013,18(3):310-325
This paper introduces a multisensor architecture to fuse data acquired from different sensors available in commodity smartphones in order to build accurate location-based services, and pursuing a good balance between accuracy and performance. Using scale invariant features from the images captured using the smartphone camera, we perform a matching process against previously obtained images to determine the current location of the device. Several refinements are introduced to improve the performance and the scalability of our proposal. Location fingerprinting, based on IEEE 802.11, will be used to determine a cluster of physical points, or zone, where the device seems to be according to the received signal strength. In this way, we will reduce the number of images to analyze to those contained in the tentative zone. Additionally, accelerometers will also be considered in order to improve the system performance, by means of a motion estimator. This set of techniques enables a wide range of location-based applications. 相似文献
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In this paper we present an algorithm, inspired by the cyclic coordinate descent method, which allows the solution of hydrothermal
optimization problems involving pumped-storage plants. The proof of the convergence of the succession generated by the algorithm
was based on the use of an appropriate adaptation of Zangwill’s global theorem of convergence. Finally, the algorithm proposed
is implemented using the Mathematica Package and is applied to an example to illustrate the results obtained. 相似文献
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