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51.
A systematic study on the electrochemical behavior of diosmin in Britton-Robinson buffer (pH 2.0-10.0) at a glassy carbon electrode (GCE) was made. The oxidation process of the drug was found to be quasi-reversible with an adsorption-controlled step. The adsorption stripping response was evaluated with respect to various experimental conditions, such as the pH of the supporting electrolyte, the accumulation potential and the accumulation time. The observed anodic peak current at +0.73 V vs. Ag/AgCl reference electrode increased linearly over two orders of magnitude from 5.0x10(-8) M to 9.0x10(-6) M. A limit of detection down to 3.5x10(-8) M of diosmin at the GCE was achieved with a mean recovery of 97+/-2.1%. Based on the electrochemical data, an open-circuit accumulation step in a stirred sample solution of BR at pH 3.0 was developed. The proposed method was successfully applied to the determination of the drug in pharmaceutical formulations. The results compared favorably with the data obtained via spectrophotometric and HPLC methods. 相似文献
52.
A. Bozkurt 《Journal of Physics and Chemistry of Solids》2002,63(4):685-690
Ionic conductivity of dry quaternary ammonium polymer, polydiallyldimethylammonium with Cl− and H2PO4− counter ions was studied in a wide range of frequencies (10−2-107 Hz) and temperatures (300-470 K). The data were analysed within the formalism of permittivity. WAXS, and thermal properties of this polymer were investigated prior to conductivity measurements. 相似文献
53.
54.
Kuh S.S. Strozier T.A. Ryan C.R. 《Selected Areas in Communications, IEEE Journal on》1989,7(9):1462-1469
A continuous phase quadrature phase shift keyed (CPQPSK) modulation technique is presented. This method utilizes a conventional QPSK modulator and a phase trajectory converter to approximate M =4, h =1/4 continuous phase signal and allows low cost, low complexity, and high rate (>1 Gbit/s) CPM modem implementation for bandwidth efficient transmission through nonlinear satellite channels. Using a communications analysis computer program it has been found that CPQPSK has 99 percent out-of-band power of 0.8R (MSK has 99 percent out-of-band power of 1.2 R where R is defined as bit rate), continuous phase trajectories, and nearly constant envelope amplitude. Simulation of realistic hardware designs indicate that the CPQPSK will require an Eb /No of 14 dB to achieve a bit error rate (BER) of 10-6. Forward error correcting techniques using block codes with an overhead of 10 percent indicate that the Eb /No requirements can be reduced to 11.2 dB for 10-6 BER 相似文献
55.
A general formalism for the study of nonlinear pulse propagation in optical fibres is presented. It is then applied to study the time evolution of a Gaussian laser pulse in a fibre with cubic and fifth-order nonlinearity in the index of refraction. The results are presented and discussed. 相似文献
56.
I. A. Bol'shakov 《Journal of Mathematical Sciences》1991,56(1):2263-2279
Systems for automatic detection and correction of spelling errors in natural language texts are considered. The development of such systems for both English and Russian (and for inflected languages in general, including all Slavic languages) is discussed. An approach associated with morphological analysis of the wordforms in the given text is described. The topics considered in the paper include the main methods of automatic spelling correction, levels of automation of the spelling error correction process, the effect of the type of computer used, the use of spelling error correctors in a stand-alone mode and in combination with word-processing software, and the maintenance of auxiliary dictionaries.Translated from Itogi Nauki i Tekhniki, Seriya Teoriya Veroyatnostei, Matematicheskaya Statistika, Teoreticheskaya Kibernetika, Vol. 28, pp. 111–139, 1988. 相似文献
57.
A. L. Chistov 《Journal of Mathematical Sciences》2006,138(3):5733-5752
Consider a projective algebraic variety W which is an irreducible component of the set of all common zeros of a family of
homogeneous polynomials of degrees less than d in n + 1 variables over a field of zero characteristic. Consider a dominant
rational morphism from W to W′ given by homogeneous polynomials of degree d′. We suggest algorithms for constructing objects
in general position related to this morphism. They generalize some algorithms from the first part of the paper to the case
dim W > dim W′. These algorithms are deterministic and polynomial in (dd′)n and the size of the input. Bibliography: 12 titles.
__________
Translated from Zapiski Nauchnykh Seminarov POMI, Vol. 325, 2005, pp. 181–224. 相似文献
58.
Tipton C.W. Bayne S.B. Griffin T.E. Scozzie C.J. Geil B. Agarwal A.K. Richmond J. 《Electron Device Letters, IEEE》2002,23(4):194-196
This paper reports on the first demonstration of a half-bridge power inverter constructed from silicon carbide gate turn-off thyristors (GTOs) operated in the conventional GTO mode. This circuit was characterized with input bus voltages of up to 600 VDC and 2 A (peak current density of 540 A/cm2) with resistive loads using a pulse-width modulated switching frequency of 2 kHz. We discuss the implications of the thyristor's electrical characteristics and the circuit topology on the overall operation of the half-bridge circuit. This work has determined the conservative critical rate of rise value of the off-state voltage to be 200 V/μs in these devices 相似文献
59.
Krahenbuhl R. Howerton M.M. Dubinger J. Greenblatt A.S. 《Lightwave Technology, Journal of》2002,20(1):92-99
High-performance Y-branch digital optical switches realized in Ti:LiNbO3 are presented. Their switching response functions have been optimized in terms of switch voltage and crosstalk ratio. The optimization is based on analyzing different types of waveguide shaping and switching arrangements using coupled mode theory and computer simulations. Excellent switching characteristics are achieved with devices exploiting a specially shaped waveguide branch in a dilated switch arrangement. Demonstrated performances include switching voltage as low as 9 V with crosstalk suppression better than 45 dB and fiber-to-fiber losses as low as 4 dB. Polarization independence with crosstalk suppression better than 40 dB over a 1520- to 1570-nm wavelength range is achieved for any applied switch voltage greater than 18 V. These optimized digital optical switches have further demonstrated the capability to reshape electrical input signals at switching rates of several hundred megahertz 相似文献
60.
Self-similarity in diffraction by a self-similar fractal screen 总被引:1,自引:0,他引:1
Lakhtakia A. Holter N. Varadan V. 《Antennas and Propagation, IEEE Transactions on》1987,35(2):236-239
Using the Sierpinski gasket as an example, it has been shown here that the paraxial Fraunhoffer-zone diffracted field of a self-similar fractal screen also exhibits self-similarity. This also establishes that fractal structures can be used with great profit in problems involving array syntheses. Recently, it has been shown that the Sierpinski gasket is itself a member of a much wider class of gaskets, and the potential for the use of fractal structures in electromagnetic (EM) problems may be vast indeed. 相似文献