2,9-disubstituted 1,10-phenanthroline nickel complexes: Syntheses,characterization, and their ethylene oligomerization

Nickel complexes 1–4 ligated with 2,9-disubstituted-1,10-phenanthroline were synthesized and characterized by FT-IR spectra and elemental analysis. The molecular structure of complex 2 was confirmed by X-ray crystal diffraction analysis. Activated with methylaluminoxane (MAO), those complexes showed moderate activities for ethylene oligomerization. Published in Kinetika i Kataliz, 2007, Vol. 48, No. 5, pp. 710–714. This article was submitted by the authors in English.     

A method to collect an infrared spectrum in solution.

Herein we report a new method to collect a qualified infrared spectrum of a solute in solution by two solvent cells with different thickness during background single-beam spectrum scanning. By collecting the background spectrum with two cells (two stages), we successfully achieved accurate solvent compensation between a sample and a reference, namely, the solvent amounts in the sample and background measurements could become congruent. Therefore, the solvent bands were thoroughly suppressed in the infrared spectrum and a qualified spectrum of the solute was obtained.     

Buckling of a stiff thin film on a compliant substrate in large deformation

A finite-deformation theory is developed to study the mechanics of thin buckled films on compliant substrates. Perturbation analysis is performed for this highly nonlinear system to obtain the analytical solution. The results agree well with experiments and finite element analysis in wavelength and amplitude. In particular, it is found that the wavelength depends on the strain. Based on the accurate wavelength and amplitude, the membrane and peak strains in thin films, and stretchability and compressibility of the system are also obtained analytically.     

模拟电路故障诊断系统的设计

介绍了板级模拟电路故障诊断系统,论述了系统的硬件组成和软件功能,该系统结合了测试技术、故障诊断理论,将专家经验融合到计算机软件系统中,能自动完成电路板的性能测试,并根据性能测试结果生成故障隔离引导树,引导操作人员对被测电路板进行故障的检测和维修.系统符合开放的、模块化、通用化的构建思想及在硬件资源的可互换方面的考虑,大大提高了系统的扩展能力和测试程序集(TPS)的重用性,节约了软件开发的成本,对于开发集数字电路与模拟电路为一体的通用故障诊断平台具有一定的借鉴作用.     

CDMA发射分集系统的多用户检测常模算法分析

空时分集技术的最大优点在于在不增加带宽的情况下可以提高系统的可靠性,是目前移动通信的研究热点.常模算法是一种性能优良的码分多址(CDMA)盲多用户检测技术,能确保判决信号与实际传送信号之间的差错较小,误码率性能良好.文中提出将标准线性受限常模算法(LCCMA)与空时分组码(STBC)相结合,设计出一种收敛快、能够改善系统性能的基于2-空时分组码的多用户接收机.     

基于DTW算法的语音识别系统实现

动态时间归整(DTW)算法的实现简单有效,在孤立词语音识别系统中得到了广泛的应用.介绍了将DTW算法移植到TMS320VC5402上实现孤立词语音识别的原理、系统硬件组成和软件设计.研究结果表明,系统能满足实时性能要求,识别效果良好.     

朗讯cdma 1x基站分组管宽度的配置

简单介绍朗讯系统cdma 1x基站分组管(PP)宽度的配置，并对朗讯cdma 1x基站分组管宽度不合理的配置及信道板扩容后的PP宽度配置进行了案例分析。     

An improved On-Surface Radiation Condition for acoustic scattering problems in the high-frequency spectrum

This Note addresses the derivation of an improved On-Surface Radiation Condition for the numerical solution of the exterior Helmholtz equation at high-frequencies. This condition is built as an approximation of the Neumann-to-Dirichlet map by using a local regularization of its principal classical symbol in the gliding zone for modelling the creeping waves. The numerical simulation of this pseudodifferential operator is efficiently realized with a linear cost according to the dimension of the boundary element approximation space using suitable complex Padé approximants. A numerical example is provided. To cite this article: X. Antoine et al., C. R. Acad. Sci. Paris, Ser. I 340 (2005).     

负载型CO3[Fe（CN）6]2及CN^—加氢反应的研究

双金属催化剂是一类重要的多相催化剂。其中d电子在催化活性方面起着重要的作用.本文在Co_3[Fe(CN)_6]_2的工作基础上,进一步研究了该配合物在硅胶、氧化铝、以及氧化镁上的热性质,同时考察了CN~-在Co-Fe体系双端基配位的活化加氢,探讨了载体的影响.     

Conflict detection and resolution in two-dimensional prefix router tables

We show that determining the minimum number of resolve filters that need to be added to a set of two-dimensional (2-D) prefix filters so that the filter set can implement a given policy using the first-matching-rule-in-table tie breaker is NP-hard. Additionally, we develop a fast O(nlogn+s) time, where n is the number of filters and s is the number of conflicts, plane-sweep algorithm to detect and report all pairs of conflicting 2-D prefix filters. The space complexity of our algorithm is O(n). On our test set of 15 2-D filter sets, our algorithm runs between 4 and 17 times as fast as the 2-D trie algorithm of A. Hari et al. (2000) and uses between 1/4th and 1/8th the memory used by the algorithm of Hari et al. On the same test set, our algorithm is between 4 and 27 times as fast as the bit-vector algorithm of Baboescu and Varghese (2002) and uses between 1/205 and 1/6 as much memory. We introduce the notion of an essential resolve filter and develop an efficient algorithm to determine the essential resolve filters of a prefix filter set.