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991.
A series of shape memory polyurethanes were synthesized from poly(tetramethylene glycol), 4,4‐methylene diphenyl diisocyanate, and 1,3‐butanediol. The prepolymers with different molecular weights (Mc) were capped with 2‐hydroxyl ethylacrylate or 3‐aminopropyltriethoxysilane (APTES) and crosslinked by UV curing or a sol–gel reaction. Variations of the crosslinker functionality (f), subchain density (N), and hard segment content (HSC) produced systematic variations of the glass transition temperature (6–45 °C), accompanied by changes in the mechanical, dynamic mechanical and shape memory properties. More than 95% of shape fixity and 98% of shape recovery up to the fourth cycles were obtained with APTES crosslinked 3000Mc with 30% of HSC. © 2013 Wiley Periodicals, Inc. J. Polym. Sci., Part B: Polym. Phys. 2013 , 51, 1473–1479 相似文献
992.
A sensitively electrochemical aptasensor was developed to detect zearalenone, utilizing DNA assembly based on hybridization chain reaction to amplify the signal current and exonuclease III to reduce the background current. The linear range 5.0×10−5 ng/mL-50 ng/mL, and the limit of detection is 0.013 pg/mL. The fabricated aptasensor showed the high specificity toward aflatoxin B1 (AFB1), fumonisin B1 (FB1) and ochratoxin A (OTA), good repeatability and reproducibility. In addition, the average recoveries of spiked corn and beer samples were in the range of 89 % to 102 %. The established method is of great significance in the field of food safety detection. 相似文献
993.
994.
n n n设 a1,a2,…,an为正数,若∏i=1 ai =1或∑i=1 ai =1,借助数学归纳法可相应地证明∑ai ≥ n或i=1 n nn∏ai ≤1.这两个不等式可用于证明平均值不等式,并由此得出三者相互等价.实例说明平均值不等式在求数列极限方面的应用. i=1 相似文献
995.
近年乡镇的有线电视网络得到了长足的发展,为了给网络运营提供有效保障,其施工和验收环节必须严格把关。系统地阐述有线数字电视网络的施工工艺要求和工程质量验收规范,供乡镇网络施工时参考。 相似文献
996.
997.
HAN Tao LU XiaoChun WANG Xue RAO YongNan ZOU DeCai YANG JianFei & WU YangYang National Time Service Center Xi'an China Key Laboratory of Precision Navigation Timing Technology Chinese Academy of Sciences Graduate University of the Chinese Academy of Sciences Beijing 《中国科学:物理学 力学 天文学(英文版)》2011,(6)
With the development of Global Navigation Satellite System (GNSS),the idea of GNSS interoperability is born and has become the focus of study in the field of satellite navigation.The popularity for GNSS to augment the interoperability with the existing ones necessitates the study of the assessment algorithm of this idea.In this paper,an assessment algorithm for interoperability comprehensive benefits based on the differential equation dynamical system is discussed.There are two important aspects in GNSS tha... 相似文献
998.
In this work, a projection algorithm is considered for treating strongly continuous semigroups of demicontinuous pseudocontractions. Theorems of strong convergence of fixed points are established in the framework of real Hilbert spaces. 相似文献
999.
Fengfeng Chi Yanguang Qin Shaoshuai Zhou Xiantao Wei Yonghu Chen Changkui Duan Min Yin 《Current Applied Physics》2017,17(1):24-30
In order to clarify the site occupancy of rare-earth ions in rare-earth doped perovskite materials, the un-doped pure CaTiO3 and Eu3+-doped CaTiO3 samples with a series of Ca/Ti ratio were synthesized via high-temperature solid-state reaction method. X-ray diffraction (XRD) powder patterns confirm that the crystal structure keeps invariant at various Ca/Ti ratios. Measurement results of unit-cell parameters and X-ray photoelectron spectroscopy (XPS) indicate that Eu3+ ions enter into the Ca2+ site. The high-resolution photoluminescence spectra of Eu3+ ions at 20 K in all samples did not witness a significant change under the excitation at different wavelength, implying that Eu3+ ions occupy only one type of site. Considering the small spectral splitting range of 5D0 → 7F2 transition and the large intensity ratio of 5D0 → 7F2/5D0 → 7F1, it can be concluded that Eu3+ occupies Ca2+ site with larger coordinate numbers rather than Ti4+ site. 相似文献
1000.