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991.
Several extraction procedures are described allowing arsenic speciation in sediments. The extraction of organometallic compounds
such as dimethylarsinic acid or monomethylarsonic acid is quite simple since these compounds are stable in the different extraction
media (HCl/ HNO3, H3PO4, ammonium oxalate) and are easily released independent of the extraction mode (magnetic stirring or microwave solubilization).
Extraction yields are higher than 96% for these two arsenic forms. An HCl/HNO3 microwave solubilization procedure allows the quantitative solubilization of mineral arsenic, but the differentiation between
the two oxidation states is not possible owing to the oxidation of As(III) to As(V). Extractions with orthophosphoric acid
or ammonium oxalate allow the solubilization of mineral arsenic with extraction yields ranging from 90 to 95% and the differentiation
between As(III) and As(V). Nevertheless, the amount of As(III) is underestimated owing to its partial oxidation. The usefulness
and advantages of microwave solubilization compared with conventional extraction procedures are discussed.
Received: 17 May 1996 / Revised: 19 September 1996 / Accepted: 25 September 1996 相似文献
992.
本文描述了用膜吸收法测量激光等离子体辐射温度空间分布的原理和方法给出了柱形缝靶轴向辐射温度随空间位置变化的特征,对测量结果进行了分析讨论。 相似文献
993.
A broad range echelle spectrograph with a CCD matrix detector is developed for different applications in atomic spectroscopy. The compact optical design in combination with a dispersive entrance slit illumination offers a low stray light level and high throughput in the UV spectral region comparable only with spectrographs of higher focal length. Ray tracing calculations for typical wavelengths and the multi-line spectrum of an iron arc show the excellent overall spectrum quality. The subtraction of two partial spectra of different steel alloys demonstrates the spectra evaluation possibilities of the CCD spectrograph. 相似文献
994.
I.IlltroductionWhenanactiveunderwateracousticalpositioningsystemissearchingforanunderwatertarget,itisnecessaryforittocompleteatransmittingandreceivingcycIewithineachworkingperiodinordertofindoutthelocationofthetargetcorrectly.Forexample,whenanunder-wateracoustica1synchronouspositioningsystemistrackinganunderwatertargetwithagivensynchr0nizingperiod,thepropagati0ntimeofthepositioningsignaltravellingfr0mthetaJrgettothearrayofthesystemshouldbelessthanthesynchronizingperiod0therwisetargetdis-tance… 相似文献
995.
K''Andrea C. Bickerstaff Michael J. Schulte Earl E. Swartzlander 《The Journal of VLSI Signal Processing》1995,9(3):181-191
As developed by Wallace and Dadda, a method for high-speed, parallel multiplication is to generate a matrix of partial products
and then reduce the partial products to two numbers whose sum is equal to the final product. The resulting two numbers are
then summed using a fast carry-propagate adder. This paper presents Reduced Area multipliers, which employ a modified reduction
scheme that results in fewer components and less interconnect overhead than either Wallace or Dadda multipliers. This reduction
scheme is especially useful for pipelined multipliers, because it minimizes the number of latches required in the reduction
of the partial products. The reduction scheme can be applied to either unsigned (sign-magnitude) or two's complement numbers.
Equations are given for determining the number of components and a method is presented for estimating the interconnect overhead
for Wallace, Dadda, and Reduced Area multipliers. Area estimates indicate that for non-pipelined multipliers, the reduction
in area achieved with Reduced Area multipliers ranges from 3.7 to 6.6 percent relative to Dadda multipliers, and from 3.8
to 8.4 percent relative to Wallace multipliers. For fully pipelined multipliers, the reduction in area ranges from 15.1 to
33.6 percent relative to Dadda multipliers, and from 2.9 to 9.0 percent relative to Wallace multipliers. 相似文献
996.
997.
本文主要研究了滤束扫描合成孔径雷达的杨像处理方法,分析了SCANSAR的工作原理、信号格式、信号结构和信号参数限制,成像处理算法包括块数据成像算法和块图像拼接算法两部分,频谱分析法和时域频域混合相关法被用于数据成像,块图像的拼接是利用时间有系剪裁块图像再顺次拼接,计算机仿真验证了本文提出的SCANSAR信号格式和成像算法的可行性。 相似文献
998.
OntheRealizationofCurrent-ModeContinuousTimeOperationalTransconductanceCapacitanceFilter¥GuoJingboandHanQingquan(ChangchunPos... 相似文献
999.
1000.
1μm宽硅深槽刻蚀技术 总被引:1,自引:1,他引:0
介绍了硅深槽刻蚀的基本原理和影响刻蚀效果的几个主要工艺因素。提出了一种实现1μm宽的硅深槽刻蚀工艺途径;并给出了1μm宽、8μm深、侧壁及底部光洁的硅深槽刻蚀工艺条件。 相似文献