An easy and fast way to determine the enantiomeric purity of substituted cyclanones

The determination of the enantiomeric purity of 2 or 3-substituted cyclanones, particularly cyclohexanones, is conveniently achieved by derivatisation into cyclic aminals with commercially available (R, R)-1,2-diphenylethylenediamine. The derivatisation procedure is directly done into the NMR tube, instantaneously, and ¹³C NMR allows an accurate measure of the ee.     

Measurement of intense microwave field patterns using a neon glow indicator lamp

A novel method using small neon glow lamps with electrodes is developed for measuring intense microwave field patterns. When the lamp axis coincide with the electric field direction, the lamp discharge starts at the feeblest microwave electric field strength. Therefore, the lamp axis shows the field direction and the discharge starting indicates the field strength. The field strength for starting the microwave discharge is less than the strength for AC discharge, because of its low loss discharge mechanism. In the experiments using a microwave oven, it has been demonstrated again comparing with the simulated results that the method is able to use for measuring the intense electric field strength and direction.     

To the problem of energy recuperation in gyrotrons

A relatively high level of the minimal electron energy at the gyrotron output even at very large spread in pitch factor is explained. An estimation of the recuperation efficiency, which can be obtained due to this effect, is given.     

火焰原子吸收光谱法测定磁化杯中铅、镉和铁

本文研究了火焰原子吸收光谱法测定磁化杯陶瓷内胆中Ｐｈ、Ｃｄ和Ｆｅ含量的方法。样品经粉碎，用硝酸－高氯酸混合液进行消解后测定。本法灵敏度高，干扰少，简单，快速，具有良好的精密度和准确度，其相对标准偏差分别为Ｐｂ３．９９％，Ｃｄ１０．７％，Ｆｅ０．９％。回收率Ｐｂ１００．６１％，Ｃｄ１０１．１８％，Ｆｅ１０２．４％。     

Electron tuning of frequency in gyrotrons

Formulas for shifts of gyrotron autooscillation frequency due to change of electron beam parameters are presented. The frequency shifts can be commensurable with the frequency band of the beam-unloaded cavity. The autooscillation frequency is most sensitive to the change of the magnetic field, less to the change of the anode voltage and least to the the change of the beam voltage. Experiments presented are in satisfactory agreement with the theory.The authors wish to thank M.I. Petelin for his interest to the present work.     

超稳Y沸石制备技术对沸石铝分布的影响 Ⅱ.均匀铝分布的超稳Y沸石的制备

对水热处理后得到的USY沸石作进一步的酸处理以及采用改进的氟硅酸盐溶液骨架富硅工艺,分别得到了经XPS剖面分析证实为铝分布均匀的超稳Y沸石HAY-Ⅰ和HAY-Ⅱ。IR分析表明,在酸处理过程中从USY沸石中去掉的那部分非骨架铝类与3690cm~(-1)处羟基有关,仍残留在HAY-Ⅰ沸石中的那部分非骨架铝类与3670cm~(-1)和3600cm~(-1)处羟基有关。XRD和化学分析表明HAY-Ⅰ沸石仍含有约50％的非骨架铝类,而HAY-Ⅱ沸石则基本上不含非骨架铝类,HAY-Ⅱ沸石还显示更高的结晶保留度。DTA分析表明,HAY-Ⅰ和HAY-Ⅱ两种沸石的热稳定性均高于USY沸石。     

GLq(N)-covariant braided differential bialgebras

We study the possibility of defining the (braided) comultiplication for the GL _q (N)-covariant differential complexes on some quantum spaces. We discover suchdifferential bialgebras (and Hopf algebras) on the bosonic and fermionic quantum hyperplanes (with additive coproduct) and on the braided matrix algebra BM _q (N) with both multiplicative and additive coproducts. The latter case is related (forN = 2) to theq-Minkowski space andq-Poincaré algebra.     

连续双向联想记忆模型的稳定性分析

对于连续型Ｈｏｐｆｉｅｌｄ模型的平衡态特征，目前人们已经得到了很多富有意义的成果，本文说明，连续Ｈｏｐｆｉｅｌｄ模型的大部分结论都可以推广到连续双向联想记忆模型，我们重点讨论了平衡态条件、渐近稳定性以及围绕一稳定平衡点的吸引域等问题，所得到的结论对于ＢＡＭ的设计和应用都是很有意义的。