DYNAMIC STABILITY OF SKEW PLATES SUBJECTED TO AERODYNAMIC AND RANDOM IN-PLANE FORCES

This paper presents an investigation into the dynamic stability of skew plates acted upon simultaneously by an aerodynamic force in the chordwise direction and a random in-plane force in the spanwise direction. Due to this random in-plane force, the plate may become unstable before the aerodynamic force reaches its critical value. In this work, the finite element formulation is applied to obtain the discretized system equations. The system equations are then partially uncoupled and reduced in size by the modal truncation method. Finally, the unsmoothed and the smoothed versions of the stochastic averaging are used to calculate the system response, and the second-moment stability criterion is utilized to determine the stability boundary of the system. Numerical results show that the stability boundary obtained by the smoothed stochastic averaging is less conservative than that obtained by the unsmoothed version, and the former is the tangent of the latter at zero spectral density of the random in-plane force.     

Al-C-Ni组分的变化对Al-C-Ni与ITO层接触电阻的影响

为克服大尺寸显示面板中反应时间的延迟问题,采用低阻栅线是十分有益的,同样在小尺寸面板上也存在这种相互匹配的过程。然而,由于Al较高的氧化速度,铝合金和ITO材料接触性能并不太好。文章介绍了在室温ITO沉积过程中,通过增加ACX(Al-C-Ni)中Ni含量来减少ACX-ITO接触电阻。经室温ITO沉积后,接触电阻成功地减少到300Ω,而且没有ACX引起的问题出现。     

基于PenTile RGBWTM算法的高像素密度a-Si TFT移动液晶显示屏

采用传统的移动设备设计规则,基于PenTile RGBWTM算法开发了a-Si TFT移动液晶显示屏。将AFFS模式和PenTile RGBWTM算法相结合,制作的TFT液晶屏获得了超过200 cd/ m2的高亮度,500∶1的高对比度,以及达到VGA标准,可以清晰显示互联网网页的高分辨率。     

ON THE ACOUSTIC ABSORPTION OF MULTI-LAYER ABSORBERS WITH DIFFERENT INNER STRUCTURES

A rigorous finite element analysis procedure is developed to study the effect of the inner structures on the acoustic absorption of multi-layer absorbers. To do this, four types of basic inner structure compartments adopted in the multi-layer absorbers are selected for analysis. These compartments are composed of porous materials inlaid with perforated plates of various shapes, say, triangle, semicircle, convex rectangle and plate shapes. As it is different from the conventional finite element analysis for the acoustic system in the literature, the perforated plates are simulated by appropriate equivalent boundary conditions, depending on their thickness, hole radius, hole pitch and porosity and the air contained in the holes. A large number of total degrees of freedom generated from meshing the air in the holes of perforated plates are thus avoided. The results reveal that the inner structures of the multi-layer absorbers will influence the acoustic absorption at some frequency bands significantly. Based on those features, the multi-layer absorber with a novel inner structure is then designed and manufactured. Both the finite element and experimental results show that its acoustic absorption would be distinctly promoted.     

柔性铰链微位移机构在可调谐F-P滤波器中的应用研究

分析了由于反射镜倾斜导致的可调谐F-P(Fabry-Perot)滤波器失谐。设计了一种柔性铰链式微位移机构,由压电陶瓷驱动,采用平行四连杆机构进行传动导向。采用该机构驱动F-P腔镜扫描克服了直接使用压电陶瓷带来的腔镜倾斜问题。该机构已应用于可调谐F-P滤波器中,输出信号多周期峰值幅度均匀,重复性好。     

广州市住宅室内外大气羰基化合物的监测分析

选择代表性住宅,在其室内、外同步开展大气羰基化合物的监测分析,准确评价大气羰基化合物的污染状况,揭示其来源。用涂覆2,4-硝基苯肼(DNPH)的硅胶采样管收集羰基化合物,借助高效液相色谱完成样品分析,共检测了13种羰基化合物,其中甲醛、乙醛两种物质的平均浓度最高,占被测物质总浓度的30%~67%。甲醛、乙醛的浓度,夏季室内平均为53.47μg/m3、17.81μg/m3,室外平均为15.00μg/m3、10.97μg/m3;冬季室内平均为37.97μg/m3、11.49μg/m3,室外平均为10.44μg/m3、8.15μg/m3。大气羰基化合物呈现夏季高于冬季、室内大于室外的浓度变化规律。甲醛/乙醛和乙醛/丙醛比值结果反映城市大气羰基化合物的人为污染。     

尿素法合成高结晶度类水滑石

尿素的高温分解特性被用于控制层状化合物合成过程中的pH值。室温下尿素可与硝酸盐形成均一溶液，当其高温分解时可以保证溶液内部各点的pH值始终一致，因而可获得高结晶度的水滑石样品。利用该法可合成出Mg-Al、Zn-Al及Ni-Al类水滑石，但难以合成出Co-Al，Mn-Al及Co-Cr类水滑石，相信这与不同金属离子发生沉淀时所需的pH值有关。     

Regioselective Formation of Enediynes via Intramolecular Trapping of Allylic Cations

Enediynes are a novel class of naturally occurring antitumor antibiotics capable of causing DNA strand cleavage by hydrogen atom abstraction from the deoxyribose backbone. During the past decade, numerous synthetic methods have been developed to synthesize the naturally occurring and the "designed" enediynes for biomedical studies. Recently, we have succeeded in assembling the cis-enediynes 2 by a novel and high-yielding allylic rearrangement under mild reaction conditions (Eq 1).^1-3 This methodology has been used to synthesize a 10-membered ring enediyne³ which exhibits DNA cleavage activity.     

Novel Method of Preparation of Monolithic Columns for Fast Separation by γ-Ray Irradiation

A porous monolithic sol-gel column with the solution of methacryloxypropyltrimethoxysilane in toluene with an acid catalyst was prepared in the presence and absence of sodium dodecyl sulfate. In situ polymerization was carried out byγ-ray irradiation within the capillary. Theγ-radiation-initiated synthesis could generate radicals directly on the monomer avoiding use of any initiator. The chromatographic behavior of the capillary monolithic columns were studied in the modes of CEC, p-CEC and low pressure-driven separation, all the tests exhibited reversed-phase character. It provided a viable alternative to either thermally initiated or photo polymerization method for the preparation of monolithic columns.     

Development of an RPLC-based Method for Measurement of Indoprofen Stability and Validation of the Method

A method for quantitative measurement of the photochemical decomposition of the anti-inflammatory agent, indoprofen （INP） is descriped. An RPLC-based assay that could determine the extent of degradation of INP in a rapid, sensitive, and accurate manner was developed. The method was validated under photoirradiation. Quantitation was monitored with an Inertsil ODS-3V column using a mobile phase of acetonitril and 1% HOAc solution in deionized H2O. Statistics relevant to the system criteria, peak integrity and resolution among the parent drug and its degradation products were performed. From the intra- and inter-day tests, the coefficients of variation were found to range from 0.59% to 4.25% for the former and from 0.71% to 4.86% for the latter. The good selectivity and specificity of this RPLC-based procedure render it suitable for measurements of INP stability.