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101.
Hossini I Harrad MA Ait Ali M El Firdoussi L Karim A Valerga P Puerta MC 《Molecules (Basel, Switzerland)》2011,16(7):5886-5895
Friedel-Craft acylation at 100 °C of 2,5,9,9-tetramethyl-6,7,8,9-tetrahydro-5H-benzocycloheptene [ar-himachalene], a sesquiterpenic hydrocarbon obtained by catalytic dehydrogenation of α-, β- and γ-himachalenes, produces a mixture of two compounds: (3,5,5,9-tetramethyl-6,7,8,9-tetrahydro-5H-benzocyclohepten-2-yl)-ethanone (2, in 69% yield), with a conserved reactant backbone, and 3, with a different skeleton, in 21% yield. The crystal structure of 3 reveals it to be 1-(8-ethyl-8-hydroperoxy-3,5,5-trimethyl-5,6,7,8-tetrahydronaphthalen-2-yl)-ethanone. In this compound O-H…O bonds form dimers. These hydrogen-bonds, in conjunction with weaker C-H…O interactions, form a more extended supramolecular arrangement in the crystal. 相似文献
102.
Harrad MA Valerga P Puerta MC Houssini I Ali MA El Firdoussi L Karim A 《Molecules (Basel, Switzerland)》2011,16(1):367-372
A recyclable catalyst, Ni(0)-CMC-Na, composed of nickel colloids dispersed in a water soluble bioorganic polymer, sodium carboxymethylcellulose (CMC-Na), was synthesized by a simple procedure from readily available reagents. The catalyst thus obtained is stable and highly active in alkene hydrogenations. 相似文献
103.
Hosni K Msaâda K Ben Taârit M Chahed T Marzouk B 《Natural product communications》2011,6(11):1731-1734
The chemical composition of the essential oils obtained by hydrodistillation from the aerial parts of the Tunisian Hypericum perforatum and H. ericoides ssp. roberti was elucidated by a combination of GC and GC-MS analyses. The main constituents of the oil of H. perforatum were alpha-pinene (11.8%), alpha-ylangene (10.4%), germacrene-D (9.5%), n-octane (6.5%) and alpha-selinene (5.9%). The oil of H. ericoides ssp. roberti exhibited a higher amount of aliphatic and branched hydrocarbons and the main constituents were n-octane (29.1%), alpha-pinene (10.9%), pulegone (7.7%) and acetophenone (7%). Both qualitative and quantitative differences were observed between the studied oils. This chemical variability seems likely to result from the genetic variability, since samples of both species were collected at the same location and processed under the same conditions. 相似文献
104.
Zahra Kamali Bahram Khani Robati Karim Hedayatian 《Czechoslovak Mathematical Journal》2011,61(2):551-563
In this paper, we discuss the hypercyclicity, supercyclicity and cyclicity of the adjoint of a weighted composition operator
on a Hilbert space of analytic functions. 相似文献
105.
The ruled residue theorem characterises residue field extensions for valuations on a rational function field. Under the assumption that the characteristic of the residue field is different from 2 this theorem is extended here to function fields of conics. The main result is that there is at most one extension of a valuation on the base field to the function field of a conic for which the residue field extension is transcendental but not ruled. Furthermore the situation when this valuation is present is characterised. 相似文献
106.
107.
一,SiP技术的产生背景 系统级封装SiP(System-In-Package)是将一个电子功能系统,或其子系统中的大部分内容,甚至全部都安置在一个封装内.这个概念看起来很容易理解,熟悉封装技术,又对电子装置或电子系统有所了解的人们一般都能够理解SiP的含义.但是如果试图对SiP使用严格的名词术语,进行精确的定义,却非常困难.SiP这一术语出现至今,虽然已经有好几年了,但是仍然没有,能够被广泛认同的定义;一般只是指出其包含的内容,或者指出其所具有的特征.Amkor公司认为SiP技术包括以下内容,或具有以下特征: 相似文献
108.
An asymptotic formula for the voltage potential in the case of a near-surface conductivity inclusion
Habib Ammari Hyeonbae Kang Karim Touibi 《Zeitschrift für Angewandte Mathematik und Physik (ZAMP)》2006,57(2):234-243
We rigorously derive an asymptotic expansion of the steady-state voltage potentials in the presence of a conductivity inclusion
of small volume that is close to a planar surface. This new formula is motivated by the practically important inverse problem
of imaging a conductivity inclusion near a planar interface.
Partly supported by ACI Jeunes Chercheurs (0693) from the Ministry of Education and Scientific Research, France.
Partially supported by grant R02-2003-000-10012-0 from the Korea Science and Engineering Foundation.
Received: December 2, 2003; revised: January 18, 2004 相似文献
109.
Karim Kadir Tetsuo Sakai Itsuki Uehara Lars Eriksson 《Acta Crystallographica. Section C, Structural Chemistry》2001,57(9):999-1000
Yttrium tricopper dialuminium, YCu3Al2, is isostructural with hexagonal CaCu5, in which each Cu atom at the 3g(½,0,½) position in space group P6/mmm (No. 191) is partially replaced by an Al atom. The hydrogen‐uptake properties are usually enhanced in other AB5 structures by aluminium substitution. YCu5 does not show any hydrogen absorption, and the goal of the present work is to investigate whether aluminium substitution could expand the metal‐atom lattice enough to provide better interstitial positions for hydrogen storage. However, no enthalpy change was observed up to 773 K under 3 MPa static H2 pressure by differential thermal analysis (DTA) for the title compound. The compound does not show any significant hydrogen absorption/desorption in the pressure‐composition isotherms (P–C–T diagrams) in the temperature range 298–673 K under 3.3 MPa H2 pressure. 相似文献
110.
The letter presents an identification scheme incorporating a set of relays, which lessens the online computations, for discrete-time model reference adaptive systems (MRAS). 相似文献