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121.
针对压力传感器隔离式封装中的波纹膜片这一关键部件,采用有限元分析的方法研究了波纹膜片的厚度、波纹深度和波纹数目分别对最大压力约0.1 MPa下的压力传感器输出信号的影响,优化了波纹膜片结构的参数选择。通过对封装了不同波纹膜片的样品的测试与比较表明,较小的膜厚与波纹深度、较多的波纹数目有助于提高压力传感器的性能,从而验证了波纹膜片结构优化的正确性。 相似文献
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重点研究了InGaAs/InP SPAD的隧道贯穿电场、雪崩击穿电场、雪崩宽度与过偏电压的关系,提出了过偏电压的计算方法.分析了InGaAs/InP SPAD的基本特性即探测效率、暗计数率与其过偏电压、工作温度、量子效率、电场分布的依赖关系,提出了一种单光子InGaAs雪崩二极管的设计方法.设计制作了InGaAs/InP SPAD,并在门控淬灭模式下进行了单光子探测实验.结果表明:对于200m的SPAD,在过偏2 V、温度-40 ℃条件下,探测效率(PDE) 20%(1 550 nm)、暗计数率(DCR)20 kHz;对于50m的SPAD,在过偏2.5 V、温度-40 ℃条件下,探测效率(PDE) 23%(1 550 nm)、暗计数率(DCR)2 kHz.最后对实验结果进行了分析和讨论. 相似文献
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Yin Wang Yuan Fang Guohua Jiang Qi Lv Xinke Sun Miaojun Ding 《高分子科学杂志,A辑:纯化学与应用化学》2013,50(11):890-895
Shell crosslinked nanoparticles, prepared from copolymerization of styrene and disulfide crosslinker, using poly(2-(dimethylamino)ethyl methacrylate) (PDMAEMA) as stabilizer and macroinitiator, exhibited a special fission behavior during the mini-emulsion RAFT polymerization process. 相似文献
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Poly(L‐lactic acid‐co‐glycolic acid) (PLGA) was prepared from hydroxy‐acids with melt polymerization. In this way, the copoly(L‐LA/GA) (PLGA) was synthesized directly using a binary catalyst (tin chloride dihydrate/p‐toluenesulfonic acid). The thermal properties of PLGA were studied by differential scanning calorimetry (DSC) and nuclear magnetic resonance (NMR). The results show that the melting point of PLGA decreases with increasing mole fraction of GA units in the copolymer. In addition, the melting point of polymer also decreases with increasing degree of racemization of the polymer. 相似文献
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Chunxiao Lv Qing Li Yaowen Zhang Zhenyu Sui Bosai He Huarong Xu Yidi Yin Xiaohui Chen Kaishun Bi 《Journal of mass spectrometry : JMS》2013,48(8):904-913
A fast, sensitive and reliable ultra fast liquid chromatography‐tandem mass spectrometry (UFLC‐MS/MS) method has been developed and validated for simultaneous quantitation of polygalaxanthone III (POL), ginsenoside Rb1 (GRb1), ginsenoside Rd (GRd), ginsenoside Re (GRe), ginsenoside Rg1 (GRg1) and tumulosic acid (TUM) in rat plasma after oral administration of Kai‐Xin‐San, which plays an important role for the treatment of Alzheimer's disease (AD). The plasma samples were extracted by liquid–liquid extraction using ethyl acetate–isopropanol (1:1, v/v) with salidrdoside as internal standard (IS). Good chromatographic separation was achieved using gradient elution with the mobile phase consisting of methanol and 0.01% acetic acid in water. The tandem mass spectrometric detection was performed in multiple reaction monitoring mode on 4000Q UFLC‐MS/MS system with turbo ion spray source in a negative and positive switching ionization mode. The lower limits of quantification were 0.2–1.5 ng/ml for all the analytes. Both intra‐day and inter‐day precision and accuracy of analytes were well within acceptance criteria (±15%). The mean absolute extraction recoveries of analytes and IS from rat plasma were all more than 60.0%. The validated method has been successfully applied to comparing pharmacokinetic profiles of analytes in normal and AD rat plasma. The results indicated that no significant differences in pharmacokinetic parameters of GRe, GRg1 and TUM were observed between the two groups, while the absorption of POL and GRd in AD group were significantly higher than those in normal group; moreover, the GRb1 absorbed more rapidly in model group. The different characters of pharmacokinetics might be caused by pharmacological effects of the analytes. Copyright © 2013 John Wiley & Sons, Ltd. 相似文献
129.
Yuqiao Wang Huijun Zhang Dan Yao Junjie Pu Yuan Zhang Xiaorui Gao Yueming Sun 《Journal of Solid State Electrochemistry》2013,17(3):881-887
Graphene/Fe3O4 nanocomposite was prepared for the immobilization of hemoglobin (Hb) to improve the electron transfer between Hb and glass carbon electrode (GCE). The characterization of nanocomposites was described by transmission electron microscopy, Fourier transform infrared, Raman spectroscopy, and X-ray photoelectron spectroscopy, respectively. The electrochemistry of Hb on the graphene/Fe3O4-based GCE was investigated by cyclic voltammetry and amperometric measurement. The modified electrode showed a wide linear range from 0.25 μmol/L to 1.7 mmol/L with a correlation coefficient of 0.9967. The detection limit of the H2O2 biosensor was estimated at 6.0?×?10?6?mol/L at a signal-to-noise ratio of 3. 相似文献
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