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111.
A rapid and sensitive flow-injection spectrophotometric method is proposed for the determination of sulfadiazine and sulfamethoxazole. This method is based on the diazotization of sulfonamide with sodium nitrite, and a coupling reaction of the diazo-compound with alpha-naphthylamine. The optimum experimental conditions are obtained by using the controlled and weighted centroid simplex method. The linear ranges for the determination of sulfadiazine and sulfamethoxazole are 0.2-20 microg ml(-1) and 0.1-20 microg ml(-1), and their detection limits are 0.06 microg ml(-1) and 0.05 microg ml(-1), respectively, and the sampling frequency is 130 samples per hour. The method has been used to determine sulfadiazine and sulfamethoxazole in pharmaceuticals and urine without separation. The results are in agreement with those obtained by a high-performance liquid chromatograph technique at the 95% confidence level. 相似文献
112.
Wenping Deng Gang Xu Lei Wan Anwen Liu Bo Gao Junhe Du Shuiming Hu Yang Chen 《Acta Physico》2008,24(8):1329-1334
Apparatus integrating a Fourier transform-infrared (FT-IR) spectrometer and a mid-infrared difference frequency generation (DFG) laser spectrometer was built for the study of the matrix isolation spectrum in solid molecular hydrogen. A 3-cm-long molecular hydrogen crystal was grown in a liquid-helium Dewar, and its infrared absorption spectrum in the 1-5 μm region was recorded to test the system. The W0(0) (ν=0←0, J=6←0) line around 2410 cm−1 of solid hydrogen was investigated with the DFG laser spectroscopy. High-resolution matrix isolation spectrum of CO2 co-deposited with hydrogen on a BaF2 cold plate at liquid-helium temperature was studied. 相似文献
113.
A novel algorithm, alternatively minimizing coupled vector (COV) resolution error and PARAFAC error algorithm, is proposed in this paper. This algorithm can overcome the problem of slow convergence and is insensitive to the estimation of component number, such problems are unavoidable while using the traditional parallel factors analysis (PARAFAC) algorithm. In other words, this algorithm is capable of improving the computing speed and providing accurate resolutions provided that the number of factors used in the computation is no less than that of the actual underlying ones. The characteristic performances were demonstrated with a novel fluorescence data array. 相似文献
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115.
Multimedia signal processing is more than simply “putting together” text, audio, images, and video. It is the integration and interaction among these different media that creates new systems and new research challenges and opportunities. In multimodal communication where speech is involved, audio-visual interaction is particularly significant 相似文献
116.
Chen Yongnian 《模糊系统与数学》1995,(1)
ANTIFUZZYVECTORSPACES(Ⅱ)ChenYongnian(DepartmentofMathematics,XinjiangNormalUniversity,830054,Xinjiang,P.R.China)ANTIFUZZYVECT... 相似文献
117.
A step-up/down single-phase AC-to-DC power converter without current sensor is proposed to achieve high performance and simple control logic. The power converter adopts a front-end diode rectifier so that only one active switch is required. The familiar state-space averaging technique for discontinuous mode DC-to-DC power converters is extended to model the proposed AC-to-DC converter. Unlike the existing model, which is valid only for a very low frequency range, namely below line frequency, the proposed model is applicable up to half switching frequency. The design of the controller is detailed. Selected experimental results are presented to verify the proposed theory 相似文献
118.
Two homologous series of mesogenic materials which incorporate a 1,4-tetrafluorophenylene moiety and a terminal cyano- or nitro-substituent have been synthesized by using palladiumcatalysed coupling procedures. The compounds exhibit nematic and/or smectic A phases. 相似文献
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