Optimization design and realization of Gaussian apodized sample gratings for narrowband wavelength selectivity filters

A sample fiber Bragg grating（SFBG） with Gaussian apodization profile is designed and optimized for the narrowband wavelength filter,and the relevant conclusions provide a guide for the further filter fabrication.With the grating length limited,a narrowband（5 GHz） grating filter used in the radio over fiber（ROF） system is fabricated,which has insertion loss of 3.463 dB,sideband suppression of 24.21dB,3 dB bandwidth of 40 pm,and 20 dB bandwidth of 106.3 pm.     

包层变化型光纤光栅传输特性研究

运用传输矩阵理论分析了一种包层半径变化的光栅结构。对包层形状变化取不同形式的光栅传输特性进行了模拟。研究发现,包层半径沿z轴非单调变化将比单调变化时具有更好的方波形反射谱;当半径变化因子g取0．1,包层形状为sin型及外加应力F为1．0N时,可以得到带宽为0．9nm,中心波长为1．55685μm的方波形反射谱。对光栅施加外力时的应变响应进行了研究,发现其对应力也是非常敏感的。     

加快Windows CE下FAT文件系统加载速度的方法及实现

针对Windows CE应用于大容量NAND FLASH时文件系统加载速度慢的问题,分析NAND FLASH驱动程序的结构和FAT文件系统的加载过程,提出以块为单位存储部分文件系统信息的创新优化方案。在Xscale PXA270的平台上测试表明,经优化后文件系统加载速度大约可以提高50%。此方案对类似的嵌入式系统研究也有借鉴作用。     

氮化硼纳米管-纳米片分级结构的制备及光学和吸附特性

将五硼酸铵、 氨硼烷络合物和氧化镁混合, 球磨均匀后, 在1200 ℃及0.6 L/min流动氨气保护条件下退火6 h, 即可在氧化铝基片上收集到白色毛状产物. 采用X射线衍射(XRD), 红外光谱(FTIR)、 扫描电子显微镜(SEM)、 透射电子显微镜(TEM)、 拉曼光谱(Raman)、 紫外-可见吸收光谱(UV-Vis)和荧光光谱(PL)对产物进行了表征. 结果表明, 样品呈一维线状分级结构, 长度大于5 mm, 中间为竹节状空心结构, 内部管径为50~350 nm, 外径范围为200~800 nm. 分级结构表面负载了大量氮化硼(BN)纳米薄片, 单个薄片厚度约为13 nm. 薄片弯曲褶皱, 相互交织, 构成1个氮化硼片层, 其厚度约为50~200 nm. UV-Vis和PL光谱测试结果表明, 氮化硼纳米管(BNNT)分级结构在紫外光材料领域具有一定的应用潜力, 且对亚甲基蓝具有良好的吸附能力(7 min即可吸附71%, 107 min时可吸附96%). 对比实验结果表明, BNNT的生长机理遵循气-液-固相(VLS)模型, 而表面负载的超薄BN片的生长机理遵循气-固相(VS)模型.     

A practicable strategy for enrichment and separation of four minor flavonoids including two isomers from barley seedlings by macroporous resin column chromatography,medium‐pressure LC,and high‐speed countercurrent chromatography

Separation of minor compounds especially with similar polarities and structures from complex samples is a challenging work. In the present study, an efficient method was successfully established by macroporous resin column chromatography, medium‐pressure liquid chromatography, and high‐speed countercurrent chromatography for separation of four minor flavonoids from barley seedlings. Macroporous resin column chromatography and medium‐pressure liquid chromatography were used for enrichment of these four flavonoids. High‐pressure liquid chromatography analysis showed the total content of these four flavonoids increased from 2.2% in the crude extract to 95.3% in the medium‐pressure liquid chromatography fraction. It was indicated that the combination of macroporous resin column chromatography and medium‐pressure liquid chromatography could be a practicable strategy for enrichment of minor compounds from complex sample. Then, high‐speed countercurrent chromatography was employed for separation of these four flavonoids using ethyl acetate/n‐butanol/water (0.1% glacial acetic acid) (4:1:5, v/v/v) as solvent system. As a result, four flavonoids including two isomers with purities higher than 98% were obtained. Interestingly, two flavonoids existing in one high‐pressure liquid chromatography peak were also successfully separated. All these indicated high‐speed countercurrent chromatography had great potential for separation of compounds with similar structures and polarities. This study provides a reference for efficient enrichment and separation of minor compounds from complex sample.     

线上线下混合式实验教学模式的改革与探索

大学化学实验课程是培养材料、化学、化工等专业人才应用基本操作和理论解决实际问题的综合性实践训练环节。文章探讨了当前大学化学实验发展由于受到仪器设备大型化、专业化、成本大、更新快等因素限制出现瓶颈,设计了线上线下混合实验教学模式,进行相应的软硬件建设,并开展线上线下混合式实验教学模式的改革与探索。该教学模式具有良好的教学效果,并且可复制可推广,为创新人才的培养和实验教学的创新提供了有益的借鉴。     

Cooling curve thermal analysis,phase constitution,and solidification characteristics of cast Mg–5Gd–2Y–xNd–Zr alloys

Journal of Thermal Analysis and Calorimetry - Mg–RE alloys are high-strength magnesium alloys with great application potential. The solidification pathways and microstructure formation of...     

Distributed machine learning load balancing strategy in cloud computing services

Wireless Networks - Mobile service computing is a new cloud computing model that provides various cloud services for mobile intelligent terminal users through mobile internet access. The quality of...     

Existence results for obstacle problems for nonlinear hemivariational inequality at resonance

In this paper, we are interested in studying the existence of solutions to obstacle problems for nonlinear hemivariational inequality at resonance driven by the p$p$-Laplacian. Using a variational approach based on the nonsmooth critical point theory for nondifferentiable functionals. We prove two existence theorems.     

Purification and Characterization of the Catalytic Domain of Protein Tyrosine Phosphatase SHP-1 and the Preparation of Anti-ΔSHP-1 Antibodies

This study is focused on the expression of an SH2 domain-truncated form of protein tyrosine phosphatase SHP-1（designated ΔSHP-1） and the preparation of its polyclonal antibodies. A cDNA fragment encoding ΔSHP-1 was amplified by PCR and then cloned into the pT7 expression vector. The recombinant pT7-ΔSHP-1 plasmid was used to transform Rosetta（DE3） E. coli cells. ΔSHP-1 was distributed in the exclusion body of E. coli cell extracts and was purified through a two-column chromatographic procedure. The purified enzyme exhibited an expected molecular weight on SDS-gels and HPLC gel filtration columns. It possesses robust tyrosine phosphatase activity and shows typical enzymatic characteristics of classic tyrosine phosphatases. To generate polyclonal anti-ΔSHP-1 antibodies, purified recombinant ΔSHP-1 was used to immunize a rabbit. The resultant anti-serum was subjected to purification on ΔSHP-1 antigen affinity chromatography. The purified polyclonal antibody displayed a high sensitivity and specificity toward ΔSHP-1. This study thus provides the essential materials for further investigating the biological function and pathological implication of SHP-1 and screening the inhibitors and activators of the enzyme for therapeutic drug development.