硅中硼离子注入校准样品的研制

本文主要介绍了硅中硼离子注入校准样品的制备与研究。分别用三台SIMS仪器对样品进行了深度剖析与比对,并对用作校准目的的样品主要参数进行了定值。     

Expert systems for HPLC in biochemistry—The knowledge base for selection of HPLC column system in the separation of amino acids,peptides and proteins

The strategy of expert system for high performance liquid chromatography was discussed, the attentions are mainly placed on the knowledge base for selection of column system, separation modes and detection modes in the analysis of amino acids, peptides and proteins.     

A wavelet-based procedure for process fault detection

To detect faults in a time-dependent process, we apply a discrete wavelet transform (DWT) to several independently replicated data sets generated by that process. The DWT can capture irregular data patterns such as sharp "jumps" better than the Fourier transform and standard statistical procedures without adding much computational complexity. Our wavelet coefficient selection method effectively balances model parsimony against data reconstruction error. The few selected wavelet coefficients serve as the "reduced-size" data set to facilitate an efficient decision-making method in situations with potentially large-volume data sets. We develop a general procedure to detect process faults based on differences between the reduced-size data sets obtained from the nominal (in-control) process and from a new instance of the target process that must be tested for an out-of-control condition. The distribution of the test statistic is constructed first using normal distribution theory and then with a new resampling procedure called "reversed jackknifing" that does not require any restrictive distributional assumptions. A Monte Carlo study demonstrates the effectiveness of these procedures. Our methods successfully detect process faults for quadrupole mass spectrometry samples collected from a rapid thermal chemical vapor deposition process     

Iterative receivers for space-time block-coded OFDM systems indispersive fading channels

We consider the design of iterative receivers for space-time block-coded orthogonal frequency-division multiplexing (STBC-OFDM) systems in unknown wireless dispersive fading channels, with or without outer channel coding. First, we propose a maximum-likelihood (ML) receiver for STBC-OFDM systems based on the expectation-maximization (EM) algorithm. By assuming that the fading processes remain constant over the duration of one STBC code word and by exploiting the orthogonality property of the STBC as well as the OFDM modulation, we show that the EM-based receiver has a very low computational complexity and that the initialization of the EM receiver is based on the linear minimum mean square error (MMSE) channel estimate for both the pilot and the data transmission. Since the actual fading processes may vary within one STBC code word, we also analyze the effect of a modeling mismatch on the receiver performance and show both analytically and through simulations that the performance degradation due to such a mismatch is negligible for practical Doppler frequencies. We further propose a turbo receiver based on the maximum a posteriori-EM algorithm for STBC-OFDM systems with outer channel coding. Compared with the previous noniterative receiver employing a decision-directed linear channel estimator, the iterative receivers proposed here significantly improve the receiver performance and can approach the ML performance in typical wireless channels with very fast fading, at a reasonable computational complexity well suited for real-time implementations     

The prediction of the peak width at half height in HPLC

The prediction of the peak width at half height is an important aspect in the optimization of the chromatographic operating conditions. In this paper, a linear relationship, between the peak widths at half height and the retention values with various isocratic elution is observed. In gradient elution, however, the relationship between the peak widths at half height and the so-called invented retention values that correspond to the mobile phase composition by eluting the solute from the column end is developed. We believe that there is almost the same band width at half height inside the column (in unit of length) for different solutes. The peak width at half height in the chromatogram (in unit of time) is mainly determined by the capacity factor of the solute when it is eluted from the column end. The larger the capacity factor of a solute eluted from the column end, the more slowly will be the solute eluted from the column end and the wider will be the peak width at half height. It is possible to predict the peak width at half height in various isocratic and gradient elutions by using this linear relationship.     

应用加权列联表分析预测汛期（4─9月）洪涝趋势

本文根据汉寿县１９６０─１９８８年洪涝灾害资料，应用加权列联表分析法，与前期气候因子建立洪涝趋势预测模式。最后对１９８９─１９９０年洪涝试报，取得了满意的效果。     

弱激发氩离子激光的振荡频率特性

通过改变激光器的相对激发,观察到了氩离子激光器振荡频率的演变特性。用模竞争效应对实验现象进行了理论解释。     

IPA模型对Hopfield模型神经网络的改进

考虑Ｈｏｐｆｉｅｌｄ模型中假态之间的布尔逻辑关系，提出利用ＩＰＡ模型对神经网络中的假态进行抑制，并和原网络的性能进行了比较，结果表明：改进后的网络性能比Ｈｏｐｆｉｅｌｄ模型和ＩＰＡ模型均有较大提高。     

(NH4)2MoS4在活性炭上浸渍过程的研究:Ⅱ.干燥机理及模型

（ＮＨ＿４）＿２ＭｏＳ＿４在活性炭上浸渍过程的研究Ⅱ．干燥机理及模型秦慧芳，张成芳，陆岗，俞丰，朱子彬（华东理工大学无机化工研究所，上海２００２３７）２３７）关键词硫代钼酸铵，活性炭，干燥，钼分布，干燥模型负载型催化剂的活性组分在载体上的分布，受浸渍...     

混沌电路同步的研究

本文叙述对混沌电路实现同步控制的实验研究之初步结果。所用的电路为蔡氏电路和锁相环电路。这项研究工作在通信系统中有应用前景。